orthogonal experiments

正交实验
  • 文章类型: Journal Article
    风积沙分布在世界各地,表现出不良的分级,低凝聚力,和松散的结构。沙漠地区的基础设施建设有时需要稳定沙子,以水泥为主固化剂。本研究首先采用正交实验来评估关键因素,例如,固化时间,水泥用量,和水的剂量,影响水泥稳定风积砂的无侧限抗压强度(UCS)。上述每个因素都被设置为五个级别,即固化时间(7、14、28、60和90天),水泥用量(3%,5%,7%,9%,和11%),和水用量(3%,6%,9%,12%,和15%),分别。水和水泥用量为天然风沙质量的百分比。结果表明,影响ASCUCS的敏感性因素是水泥用量,固化时间,和水的用量按降序排列。ASC的UCS与养护时间和水泥用量呈正相关,随着水用量的增加,它先增加后减少。最佳条件为90天固化时间,水泥用量11%,和9%的水剂量。使用光学显微镜对ASC进行显微分析,扫描电子显微镜(SEM),和X射线衍射(XRD)表明,水化产物通过粘结松散颗粒和填充孔隙来增强强度,从而提高压实度。风积-水泥反应体系中水化产物的数量和密实度随着水泥用量和养护时间的增加而增加,低水用量抑制了水化反应。这项研究可以为风积沙的稳定机理提供见解,帮助沙漠地区的基础设施建设。
    Aeolian sand is distributed worldwide, exhibiting poor grading, low cohesion, and loose structure. Infrastructure construction in desert areas sometimes requires stabilization of the sand, with cement as the primary curing agent. This study first employed orthogonal experiments to evaluate critical factors, e.g., curing time, cement dosage, and water dosage, affecting the unconfined compressive strength (UCS) of the aeolian sand stabilized with cement (ASC). Each of the aforementioned factors were set at five levels, namely curing time (7, 14, 28, 60, and 90 days), cement dosage (3%, 5%, 7%, 9%, and 11%), and water dosage (3%, 6%, 9%, 12%, and 15%), respectively. The water and cement dosages were percentages of the mass of the natural aeolian sand. The results indicated that the sensitivity of the influencing factors on the UCS of ASC was cement dosage, curing time, and water dosage in descending order. The UCS of ASC positively correlated with curing time and cement dosage, while it first increased and then decreased with the water dosage increase. The optimal conditions were 90 days\' curing time, 11% cement dosage, and 9% water dosage. The microscopic analyses of ASC using optical microscopy, scanning electron microscopy (SEM), and X-ray diffraction (XRD) revealed that hydration products enhanced strength by bonding loose particles and filling pores, thereby improving compaction. The quantity and compactness of hydration products in the aeolian-cement reaction system increased with the increases in cement dosage and curing time, and low water dosage inhibited the hydration reaction. This study can provide insights into the stabilization mechanism of aeolian sand, aiding infrastructure development in desert regions.
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  • 文章类型: Journal Article
    白菜是B.striata(Thund。)Reichb.f.,具有抗菌性,抗炎,抗肿瘤,抗氧化和伤口愈合效果。传统上,它已被用于止血治疗,以及治疗疮,皮肤肿胀和干裂。在这项研究中,我们以纹状体芽孢杆菌提取物的紫外线(UV)吸收率为指标,并且提取根据固液比而变化,乙醇浓度,超声时间和温度,以优化其防晒成分的提取工艺。百济防晒成分中的主要化合物(B.纹状体)使用超高效液相色谱结合四极杆飞行时间串联质谱进行分析。随后使用3M胶带方法在体外评价防晒性能。结果表明,纹状体防晒成分的最佳提取条件为料液比1:40(g/mL),乙醇浓度为50%,超声时间为50分钟,温度为60°C。在整个实验中使用100W的功率和40Hz的超声频率。在这些优化条件下,分离的防晒成分在UVB区域的紫外线吸收率达到84.38%,RSD为0.11%。鉴定出18种化合物,包括11种2-异丁基苹果酸葡萄糖氧苄酯,四种菲,两个联苄和一个α-异丁基苹果酸。对防晒剂性质的评估显示,来自不同批次的纹状体芽孢杆菌的防晒剂样品的平均UVB吸收值在0.727至1.201的范围内。纹状体提取物的防晒成分在UVB区域具有良好的紫外线吸收能力,它们在中等强度的阳光下具有有效的防晒效果。因此,这项研究将为从B.striata植物中提取防晒成分提供实验参考,它为B.striata作为具有UVB保护性能的候选化妆品原料的未来发展提供了证据。
    Bletilla striata is the dried tuber of B. striata (Thund.) Reichb.f., which has antibacterial, anti-inflammatory, anti-tumor, antioxidant and wound healing effects. Traditionally, it has been used for hemostasis therapy, as well as to treat sores, swelling and chapped skin. In this study, we used the ultraviolet (UV) absorbance rate of B. striata extracts as the index, and the extraction was varied with respect to the solid-liquid ratio, ethanol concentration, ultrasonic time and temperature in order to optimize the extraction process for its sunscreen components. The main compounds in the sunscreen ingredients of Baiji (B. striata) were analyzed using ultra-high-performance liquid chromatography combined with quadrupole time-of-flight tandem mass spectrometry. The sunscreen properties were subsequently evaluated in vitro using the 3M tape method. The results show that the optimal extraction conditions for the sunscreen components of B. striata were a solid-liquid ratio of 1:40 (g/mL), an ethanol concentration of 50%, an ultrasonic time of 50 min and a temperature of 60 °C. A power of 100 W and an ultrasonic frequency of 40 Hz were used throughout the experiments. Under these optimized conditions, the UV absorption rate of the isolated sunscreen components in the UVB region reached 84.38%, and the RSD was 0.11%. Eighteen compounds were identified, including eleven 2-isobutyl malic acid glucose oxybenzyl esters, four phenanthrenes, two bibenzyl and one α-isobutylmalic acid. An evaluation of the sunscreen properties showed that the average UVB absorption values for the sunscreen samples from different batches of B. striata ranged from 0.727 to 1.201. The sunscreen ingredients of the extracts from B. striata had a good UV absorption capacity in the UVB area, and they were effective in their sunscreen effects under medium-intensity sunlight. Therefore, this study will be an experimental reference for the extraction of sunscreen ingredients from the B. striata plant, and it provides evidence for the future development of B. striata as a candidate cosmetic raw material with UVB protection properties.
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  • 文章类型: Journal Article
    评估了中试规模的食品垃圾(FW)膜覆盖堆肥(MCC)过程中不同操作参数对堆肥效率和堆肥质量的影响。在正交实验中,在三个不同的水平上评估了四个因素:初始混合物水分(IMM,55%,60%,和65%),曝气时间(AT,6、9和12h/d),曝气速率(AR,0.2、0.4和0.6m3/h)和成熟堆肥添加比(MC,2%,4%,和6%)。结果表明,55%的IMM,6h/dAT,0.4m3/hAR,和4%MC添加比例同时为堆肥提供了最大累积温度和最小水分。结果表明,IMM是这种最佳堆肥过程的驱动因素。相反,减少碳和氮损失的最佳参数为65%IMM,6h/dAT,0.4m3/hAR,和2%的MC添加比例。与所有其他因素相比,AR对减少碳和氮损失的影响最大。堆肥成熟度的最佳条件是55%IMM,9h/dAT,0.2m3/hAR,和6%的MC添加比例。影响pH值和电导率值的主要元素是AR,而发芽指数受IMM影响。蛋白质是限制堆肥效率的主要有机物。本研究结果将为餐厨垃圾MCC技术的推广应用提供指导,并有助于更好地了解MCC处理有机固体废物的机制。
    The impact of different operational parameters on the composting efficiency and compost quality during pilot-scale membrane-covered composting (MCC) of food waste (FW) was evaluated. Four factors were assessed in an orthogonal experiment at three different levels: initial mixture moisture (IMM, 55 %, 60 %, and 65 %), aeration time (AT, 6, 9, and 12 h/d), aeration rate (AR, 0.2, 0.4, and 0.6 m3/h) and mature compost addition ratio (MC, 2 %, 4 %, and 6 %). Results indicated that 55 % IMM, 6 h/d AT, 0.4 m3/h AR, and 4 % MC addition ratio simultaneously provided the compost with the maximum cumulative temperature and the minimum moisture. It was shown that the IMM was the driving factor of this optimum composting process. On contrary, the optimal parameters for reducing carbon and nitrogen loss were 65 % IMM, 6 h/d AT, 0.4 m3/h AR, and 2 % MC addition ratio. The AR had the most influence on reducing carbon and nitrogen losses compared to all other factors. The optimal conditions for compost maturity were 55 % IMM, 9 h/d AT, 0.2 m3/h AR, and 6 % MC addition ratio. The primary element influencing the pH and electrical conductivity values was the AR, while the germination index was influenced by IMM. Protein was the main organic matter limiting the composting efficiency. The results of this study will provide guidance for the promotion and application of food waste MCC technology, and contribute to a better understanding of the mechanisms involved in MCC for organic solid waste treatment.
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  • 文章类型: Journal Article
    一种新型的神经酰胺化合物,命名为AspercalsideA(AcA),从海洋共生真菌曲霉的乙酸乙酯层中成功分离。AcA通过在30μg/mL和40μg/mL的浓度下有效抑制RAW264.7细胞中一氧化氮(NO)的产生而表现出显著的抗炎活性。为治疗炎症性疾病提供了一条有希望的途径。优化糖基神经酰胺(AcA)的收率,一系列的技术,包括单因素实验,正交实验,和响应面优化,系统地用于微调发酵培养基的组成。最初,最佳碳源(蔗糖),氮源(酵母提取物粉末),通过单因素实验确定了最合适的中等盐度(14ppt)。随后,正交实验,采用正交表来规划和分析多因素实验,进行了。最后,一个数学模型,使用Box-Behnken设计建立,综合分析各因素之间的相互作用,确定发酵培养基的最佳组成。根据模型的预测,当蔗糖浓度设定为37.47g/L时,酵母提取物粉末浓度为19.66g/L,和13.31ppt的中等盐度,糖基神经酰胺的预测浓度为171.084μg/mL。实验结果证实了模型的准确性,在这些条件下测得的糖基神经酰胺的实际平均浓度为171.670μg/mL,与预测值紧密一致。
    A novel ceramide compound, named Aspercerebroside A (AcA), was successfully isolated from the ethyl acetate layer of the marine symbiotic fungus Aspergillus sp. AcA exhibited notable anti-inflammatory activity by effectively inhibiting the production of nitric oxide (NO) in RAW 264.7 cells at concentrations of 30 μg/mL and 40 μg/mL, offering a promising avenue for the treatment of inflammatory diseases. To optimize the yield of glycosylceramide (AcA), a series of techniques, including single-factor experiments, orthogonal experiments, and response surface optimization, were systematically employed to fine-tune the composition of the fermentation medium. Initially, the optimal carbon source (sucrose), nitrogen source (yeast extract powder), and the most suitable medium salinity (14 ppt) were identified through single-factor experiments. Subsequently, orthogonal experiments, employing an orthogonal table for planning and analyzing multifactor experiments, were conducted. Finally, a mathematical model, established using a Box-Behnken design, comprehensively analyzed the interactions between the various factors to determine the optimal composition of the fermentation medium. According to the model\'s prediction, when the sucrose concentration was set at 37.47 g/L, yeast extract powder concentration at 19.66 g/L, and medium salinity at 13.31 ppt, the predicted concentration of glycosylceramide was 171.084 μg/mL. The experimental results confirmed the model\'s accuracy, with the actual average concentration of glycosylceramide under these conditions measured at 171.670 μg/mL, aligning closely with the predicted value.
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  • 文章类型: Journal Article
    建筑业和煤炭工业产生大量工业废物,包括煤矸石和建筑和拆除(C&D)废物,导致环境污染和高处置成本。将再生骨料(RA)和煤矸石粉(CGP)集成到混凝土中是一种有效的废物管理方法。然而,CGP会影响传统再生混凝土的性能。本研究主要旨在优化RA和CGP的利用,同时保持混凝土性能。他们利用正交实验设计和微观表征技术,包括扫描电子显微镜(SEM),能量色散X射线光谱(EDS),和X射线衍射(XRD)。正交实验分析表明,水灰比(WCR)为0.5,CGP和RA的置换率为10%,RA的置换率为60%,抗压强度和劈裂抗拉强度达到普通C30混凝土的73.6%和77.4%,分别。这种混合比例可最大程度地减少煤矸石粉再生骨料混凝土(CGP-RAC)的强度下降,同时最大程度地替代再生材料。微观分析表明,CGP增加了水泥浆中的Ca/Si比,阻碍水合反应,导致内部结构松动,混凝土强度降低。这些发现有望为固体废物的回收和利用提供新的理论见解。
    The construction and coal industries generate substantial industrial waste, including coal gangue and construction and demolition (C&D) waste, leading to environmental pollution and high disposal costs. Integrating recycled aggregates (RAs) and coal gangue powder (CGP) into concrete is an effective approach for waste management. However, CGP can affect the performance of traditional recycled concrete. This study primarily aims to optimize the utilization of RAs and CGP while maintaining concrete performance. They utilized orthogonal experimental designs and microscopic characterization techniques, including scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), and X-ray diffraction (XRD). Orthogonal experimental analysis indicated that with a water-cement ratio (WCR) of 0.5 and replacement rates of 10% for CGP and 60% for RA, compressive and splitting tensile strengths reached 73.6% and 77.4% of ordinary C30 concrete, respectively. This mix proportion minimizes strength decline in coal gangue powder-recycled aggregate concrete (CGP-RAC) while maximizing recycled material replacement. Microscopic analysis revealed that CGP increased the Ca/Si ratio in cement paste, impeding hydration reactions, resulting in a looser internal structure and reduced concrete strength. These findings are anticipated to provide fresh theoretical insights for solid waste recycling and utilization.
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  • 文章类型: Journal Article
    水泥基复合材料是典型的多尺度复合材料,失效过程具有渐进的特点,多尺度、多阶段损伤。为了延缓水泥基复合材料的多级损伤过程,通过使用不同尺度的纤维和粉煤灰(FA)来抑制不同尺度的缺陷,水泥基复合材料的整体性能得到改善,一种由毫米级聚乙烯醇纤维(PVA)组成的新型多尺度纤维增强水泥基复合材料,微米级碳酸钙晶须(CW),并设计了纳米级碳纳米管(CNTs)。抗压强度,抗弯强度,劈裂抗拉强度,以氯离子渗透系数为评价指标,采用正交试验设计。检查了三种纤维鳞片和粉煤灰对每个单独指标的影响,然后使用灰色关联分析对多尺度纤维增强胶凝材料(MSFRCC)的整体性能进行了优化。综合性能的优化配合比为PVA:1.5%,CW:2%,CNT:0.1%,FA:40%。与每组的最佳结果相比,最终优化的MSFRCC组的抗压强度下降了8.9%,抗弯强度提高了28.4%,劈裂抗拉强度提高了10%,氯离子渗透系数下降了5.7%。结果表明,在正交试验中,优化组的压缩性能和抗氯离子渗透性能略差于最优组,但其弯曲性能和劈裂拉伸性能均有显著提高。
    Cement-matrix composite are typical multi-scale composite materials, the failure process has the characteristics of gradual, multi-scale and multi-stage damage. In order to delay the multi-stage damage process of cement-matrix composites, the defects of different scales are suppressed by using different scales of fibres and fly ash (FA), and the overall performance of cement-matrix composites is improved, a new multi-scale fibre-reinforced cement-based composite composed of millimetre-scale polyvinyl alcohol fibre (PVA), micron-scale calcium carbonate whisker (CW), and nano-scale carbon nanotubes (CNTs) was designed in this study. The compressive strength, flexural strength, splitting tensile strength, and chloride ion permeability coefficient were used as assessment indices by the orthogonal test design. The impacts of the three fibre scales and fly ash on each individual index were examined, and the overall performance of the multi-scale fibre-reinforced cementitious materials (MSFRCC) was then optimized using grey correlation analysis. The optimized mix ratio for overall performance was PVA: 1.5%, CW: 2%, CNTs: 0.1%, FA: 40%. Compared with the optimal results for each group, the compressive strength of the final optimized MSFRCC group decreased by 8.9%, the flexural strength increased by 28.4%, the splitting tensile strength increased by 10%, and the chloride ion permeability coefficient decreased by 5.7%. The results show that the compressive performance and resistance to chloride ion penetration of the optimized group are slightly worse than those of the optimal group in the orthogonal test, but its flexural performance and splitting tensile performance are significantly improved.
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  • 文章类型: Journal Article
    纯自密实混凝土有许多缺点,如早期收缩和开裂。纤维的加入可以有效提高自密实混凝土的抗拉伸性能和抗开裂性能,从而可以达到提高其强度和韧性的效果。玄武岩纤维是一种“绿色工业新材料”,具有独特的优势,如抗裂性高,与其他纤维材料相比重量轻。为了深入研究玄武岩纤维自密实高强混凝土的力学性能和抗裂性能,采用多比例绝对体积法设计并获得了C50的自密实高强混凝土。采用正交试验方法研究了水胶比的影响,纤维体积分数,纤维长度,粉煤灰掺量对玄武岩纤维自密实高强混凝土力学性能的影响。同时,效率系数法确定最佳实验方案(水胶比0.3,纤维体积比0.2%,纤维长度12毫米,粉煤灰含量30%),采用改进的平板约束实验研究了纤维体积分数和纤维长度对自密实高性能混凝土抗裂性能的影响。结果表明:(1)水胶比对玄武岩纤维自密实高强混凝土的抗压强度影响最大,随着纤维体积分数的增加,拉伸强度和弯曲强度均增加;(2)纤维长度对力学性能的影响存在最优值;(3)随着纤维体积分数的增加,纤维自密实高强混凝土的总裂缝面积显著减小。当纤维长度增加时,最大裂缝宽度先减小后缓慢增大。当纤维体积分数为0.3%,纤维长度为12mm时,抗裂效果最好。因此,玄武岩纤维自密实高强混凝土可广泛应用于工程领域,如国防建设,交通运输,以及建筑结构的加固和修复,由于其优异的机械性能和抗裂性。
    Pure self-compacting concrete has many disadvantages, such as early shrinkage and cracking. The addition of fibers can effectively improve the properties of resistance to tension and cracking of self-compacting concrete, thereby the effect of improving its strength and toughness can be achieved. Basalt fiber is a \"new green industrial material\" that has unique advantages, such as high crack resistance and being lightweight compared with other fiber materials. In order to study the mechanical properties and crack resistance of basalt fiber self-compacting high-strength concrete intensively, the self-compacting high-strength concrete of C50 was designed and obtained using the absolute volume method with multiple proportions. Orthogonal experimental methods were used to study the influence of the water binder ratio, fiber volume fraction, fiber length, and fly ash content on the mechanical properties of the basalt fiber self-compacting high-strength concrete. Meanwhile, the efficiency coefficient method was used to determine the best experiment plan (water binder ratio 0.3, fiber volume ratio 0.2%, fiber length 12 mm, fly ash content 30%), and the effect of fiber volume fraction and fiber length on the crack resistance of the self-compacting high-performance concrete was investigated using improved plate confinement experiments. The results show that (1) the water binder ratio had the greatest impact on the compressive strength of basalt fiber self-compacting high-strength concrete, and as the fiber volume fraction increased, the splitting tensile strength and flexural strength both increased; (2) there was an optimal value for the effect of the fiber length on the mechanical properties; (3) with the increase in fiber volume fraction, the total crack area of the fiber self-compacting high-strength concrete significantly decreased. When the fiber length increased, the maximum crack width first decreased and then slowly increased. The best crack resistance effect was achieved when the fiber volume fraction was 0.3% and the fiber length was 12 mm. Therefore, basalt fiber self-compacting high-strength concrete can be widely used in engineering fields, such as national defense construction, transportation, and building structure reinforcement and repair, due to its excellent mechanical and crack resistance properties.
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  • 文章类型: Journal Article
    随着一次性口罩造成的环境污染日益加剧,开发新型医用口罩可降解过滤材料至关重要。利用纳米ZnO和L-丙交酯制备的ZnO-PLLA/PLLA(L-丙交酯)共聚物通过静电纺丝技术制备用于空气过滤的纤维膜。ZnO-PLLA的H-NMR结构表征,XPS,XRD和XRD表明ZnO成功接枝到PLLA上。采用L9(43)标准正交阵列来评估ZnO-PLLA浓度的影响,ZnO-PLLA/PLLA含量,DCM(二氯甲烷)至DMF(N,N-二甲基甲酰胺)比,和纺丝时间对ZnO-PLLA/PLLA纳米纤维薄膜的空气过滤能力的影响。值得注意的是,ZnO的引入对品质因数(QF)的增强很重要。获得的最佳组是样品编号。在QF为0.1403Pa-1的情况下,颗粒过滤效率(PFE)为98.3%,细菌过滤效率(BFE)为98.42%,气流阻力(Δp)为29.2Pa。因此,所制备的ZnO-PLLA/PLLA薄膜具有开发可降解掩模的潜力。
    With the increasing environmental pollution caused by disposable masks, it is crucial to develop new degradable filtration materials for medical masks. ZnO-PLLA/PLLA (L-lactide) copolymers prepared from nano ZnO and L-lactide were used to prepare fiber films for air filtration by electrospinning technology. Structural characterization of ZnO-PLLA by H-NMR, XPS, and XRD demonstrated that ZnO was successfully grafted onto PLLA. An L9(43) standard orthogonal array was employed to evaluate the effects of the ZnO-PLLA concentration, ZnO-PLLA/PLLA content, DCM(dichloromethane) to DMF(N,N-dimethylformamide) ratio, and spinning time on the air filtration capacity of ZnO-PLLA/PLLA nanofiber films. It is noteworthy that the introduction of ZnO is important for the enhancement of the quality factor (QF). The optimal group obtained was sample No. 7, where the QF was 0.1403 Pa-1, the particle filtration efficiency (PFE) was 98.3%, the bacteria filtration efficiency (BFE) was 98.42%, and the airflow resistance (Δp) was 29.2 Pa. Therefore, the as-prepared ZnO-PLLA/PLLA film has potential for the development of degradable masks.
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  • 文章类型: Journal Article
    在这项研究中,采用水射流引导激光(WJGL)方法切割耐高温Inconel718合金。通过田口正交实验研究了水射流引导激光加工方法的关键参数对切割深度的影响。此外,采用响应面法建立了切削深度的数学预测模型。验证实验表明,该数学模型对切削深度具有较高的预测能力。通过模型预测得到最优切削深度,与实验结果相比误差为5.5%。与传统的干式激光切割相比,水传导激光法减少了热损伤,提高了切割质量。该研究为水射流引导激光精密加工Inconel718提供了参考。
    In this study, the water-jet-guided laser (WJGL) method was used to cut Inconel 718 alloy with high temperature resistance. The effect of critical parameters of the water-jet-guided laser machining method on the cutting depth was studied by a Taguchi orthogonal experiment. Furthermore, the mathematical prediction model of cutting depth was established by the response surface method (RSM). The validation experiments showed that the mathematical model had a high predictive ability for cutting depth. The optimal cutting depth was obtained by model prediction, and the error was 5.5% compared with the experimental results. Compared with the traditional dry laser cutting, the water conducting laser method reduced the thermal damage and improved the cutting quality. This study provides a reference for the precision machining of Inconel 718 with a water-jet-guided laser.
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  • 文章类型: Journal Article
    本文旨在制备一种基于MXene材料的双氯芬酸钠(DCF)吸附剂。在本文中,通过用氢氟酸(HF)蚀刻Ti3AlC2来制备Ti3C2-MXene。对Ti3C2进行方便且简单的溶剂热处理。在溶剂热法过程中形成了TiO2和Ti2C。根据FT-IR和XRD的结果,TiO2和Ti2C的形成将增加制备的Ti3C2-12h的层间间距,从而提高了MXenes的吸附性能。影响吸附剂的主要因素,最大吸附能力,通过单因素试验分析两因素之间的交互作用,正交实验,和响应面分析。Ti3C2和Ti3C2-12h的最大DCF吸附容量分别为201mg/g和395mg/g,分别。由HF制成的MXene可以在各种pH条件下吸收DCF并保持较高的吸附率,在环境保护中具有重要的应用。
    This paper aims to prepare an adsorbent based on MXene material for adsorbing diclofenac sodium (DCF). In this paper, Ti3C2-MXene was prepared by etching Ti3AlC2 with hydrofluoric acid (HF). Ti3C2 was subjected to a convenient and simple solvothermal treatment. TiO2 and Ti2C were formed during the solvothermal process. According to the results of FT-IR and XRD, the formation of TiO2 and Ti2C will increase the interlayer spacing of the prepared Ti3C2-12 h, thereby improving the adsorption performance of MXenes. The main factors affecting the adsorbent, the maximum adsorption capacity, and the interaction between the two factors were analyzed by single-factor experiment, orthogonal experiment, and response surface analysis. The maximum DCF adsorption capacities of Ti3C2 and Ti3C2-12 h are 201 mg/g and 395 mg/g, respectively. MXene made from HF can absorb DCF under various pH conditions and maintain a high adsorption rate, which has important applications in environmental protection.
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