SEM morphology

  • 文章类型: Journal Article
    探索合金中增强物浓度较高的高强度材料被证明是一项具有挑战性的任务。这项研究探索了具有碳化钨增强剂的镁基复合材料(AZ31B合金),通过联赛冠军优化来增强医疗关节置换的实力。主要目标是使用镁基复合材料增强医疗关节置换生物材料,强调含碳化钨增强剂的AZ31B合金。搅拌铸造方法用于制造镁基复合材料(MMC),包括不同百分比的碳化钨(WC)。机械特性,如显微硬度,抗拉强度,和屈服强度,已经进行了评估,并与计算模拟进行了比较。已经进行了磨损研究以分析复合材料的摩擦学行为。此外,这项研究调查了骨和关节结构内部的应力和力分布的预测,因此,为生物医学研究领域做出了重大贡献。这项研究考虑使用镁基MMC来发现适用于医疗关节置换的生物材料。研究重点是镁合金AZ31B,颗粒的大小范围从40到60微米用作基质材料。此外,结果表明,当与基于AZ31B-镁基质的MMC结合使用时,WC颗粒成为轻质制造的高效增强材料,高强度生物医学复合材料。本研究使用联赛冠军优化(LCO)方法来确定影响AZ31B基镁合金MgMMCs合成的关键变量。仔细分析了扫描电子显微镜(SEM)图像,以描绘WC颗粒的分散以及镁(Mg)基体和WC增强体之间的界面。SEM分析探索了粒子拔出的潜在机制,粒子间区域的特征,和AZ31B基体对增强复合材料力学特性的影响。正在使用有限元分析(FEA)的应用来预测髋关节模型中的应力分布和力的相互作用。这项研究比较了WC的物理力学和摩擦学特征与0%的不同组合,5%,10%和15%,及其对性能改进的影响。SEM分析证实了这一发现,提高了强度和硬度,特别是当加入10%-15%的WC时。在镁合金基体中掺入10%的WC颗粒后,研究结果表明,强度和硬度都有所提高,此外,通过利用SEM分析已经很明显。使用ANSYS,预测结构变形和应力水平,连同强度特性,如71HRC的附加硬度,拉伸强度为140-150MPa,和屈服强度接近100-110兆帕。这些模拟对关节在各种载荷条件下的行为产生了重要的见解,从而增强了这项研究在生物医学环境中的意义。
    Exploring high strength materials with a higher concentration of reinforcements in the alloy proves to be a challenging task. This research has explored magnesium-based composites (AZ31B alloy) with tungsten carbide reinforcements, enhancing strength for medical joint replacements via league championship optimisation. The primary objective is to enhance medical joint replacement biomaterials employing magnesium-based composites, emphasising the AZ31B alloy with tungsten carbide reinforcements. The stir casting method is utilised in the manufacture of magnesium matrix composites (MMCs), including varied percentages of tungsten carbide (WC). The mechanical characteristics, such as micro-hardness, tensile strength, and yield strength, have been assessed and compared with computational simulations. The wear studies have been carried out to analyse the tribological behaviour of the composites. Additionally, this study investigates the prediction of stress and the distribution of forces inside bone and joint structures, therefore offering significant contributions to the field of biomedical research. This research contemplates the use of magnesium-based MMCs for the discovery of biomaterials suitable for medical joint replacement. The study focuses on the magnesium alloy AZ31B, with particles ranging in size from 40 to 60 microns used as the matrix material. Moreover, the outcomes have revealed that when combined with MMCs based on AZ31B-magnesium matrix, the WC particle emerges as highly effective reinforcements for the fabrication of lightweight, high-strength biomedical composites. This study uses the league championship optimisation (LCO) approach to identify critical variables impacting the synthesis of Mg MMCs from an AZ31B-based magnesium alloy. The scanning electron microscopy (SEM) images are meticulously analysed to depict the dispersion of WC particulates and the interface among the magnesium (Mg) matrix and WC reinforcement. The SEM analysis has explored the mechanisms underlying particle pull-out, the characteristics of inter-particle zones, and the influence of the AZ31B matrix on the enhancement of the mechanical characteristics of the composites. The application of finite element analysis (FEA) is being used in order to make predictions regarding the distribution of stress and the interactions of forces within the model of the hip joint. This study has compared the physico-mechanical and tribological characteristics of WC to distinct combinations of 0%, 5%, 10% and 15%, and its impact on the performance improvements. SEM analysis has confirmed the findings\' improved strength and hardness, particularly when 10%-15% of WC was incorporated. Following the incorporation of 10% of WC particles within Mg-alloy matrix, the outcomes of the study has exhibited enhanced strength and hardness, which furthermore has been evident by utilising SEM analysis. Using ANSYS, structural deformation and stress levels are predicted, along with strength characteristics such as additional hardness of 71 HRC, tensile strength of 140-150 MPa, and yield strength closer to 100-110 MPa. The simulations yield significant insights into the behaviour of the joint under various loading conditions, thus enhancing the study\'s significance in biomedical environments.
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  • 文章类型: Journal Article
    考虑到最近的气候变化,特别重视任何试图去污染和保护环境的行为。循环经济似乎是矿物废物增值的理想解决方案,来自各个工业部门,通过在获得替代建筑材料的过程中重新引入它们,对环境更友好。与波特兰水泥相比,地质聚合物可以被认为是一种有前途的选择。有关前体成分影响的信息,活化体系对机械性能或凝固时间的影响可能导致预期新配方的地质聚合物或改善其某些性能。钢筋组件,不同的聚合物和膨胀剂可以在短期或长期内积极或消极地影响地质聚合物的性能。
    Considering recent climate changes, special importance is given to any attempt to depollute and protect the environment. A circular economy seems to be the ideal solution for the valorization of mineral waste, resulting from various industrial branches, by reintroducing them in the process of obtaining alternative building materials, more friendly to the environment. Geopolymers can be considered as a promising option compared to Portland cement. Information about the influence of the composition of the precursors, the influence of the activation system on the mechanical properties or the setting time could lead to the anticipation of new formulations of geopolymers or to the improvement of some of their properties. Reinforcement components, different polymers and expansion agents can positively or negatively influence the properties of geopolymers in the short or long term.
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  • 文章类型: Journal Article
    本文提出了热成像作为非接触式诊断工具,用于评估驱动器的可靠性。介绍了该技术在用热焊接热塑性聚氨酯三角带进行皮带传动的过程中的应用。V带温度根据主动皮带轮转速的不同值下的制动扭矩负载而变化,作为诊断特征。在本文中,在微观和硬度测试的基础上评估聚氨酯(PU)带的表面形态。使用表面粗糙度测试仪来评估表面磨损。通过扫描电子显微镜(SEM)和光学显微镜确定材料的表面形态和形貌。发现最有利的操作条件发生在有源和无源连接器的温度值相似且它们之间的温差小时。机械和结构结果表明,PU带的磨损很小,这为V型皮带传动提供了稳定性和运行可靠性。显微图像表面缺乏清晰的裂纹和划痕痕迹,SEM观察证实了这一点。
    This article proposes thermography as a non-contact diagnostic tool for assessing drive reliability. The application of this technique during the operation of the belt transmission with a heat-welded thermoplastic polyurethane V-belt was presented. The V-belt temperature changes depending on the braking torque load at different values of the rotational speed of the active pulley, which were adopted as diagnostic characteristics. In this paper, the surface morphology of the polyurethane (PU) belts was assessed on the basis of microscopic and hardness tests. A surface roughness tester was used to evaluate the surface wear. The surface morphology and topography of the materials was determined by scanning electron microscopy (SEM) and optical microscopy. It was found that the most favorable operating conditions occurred when the temperature values of active and passive connectors were similar and the temperature difference between them was small. The mechanical and structure results indicate that the wear of the PU belt was slight, which provided stability and operational reliability for V-belt transmission. The microscopic images lacked clear traces of cracks and scratches on the surface, which was confirmed by the SEM observations.
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  • 文章类型: Journal Article
    Microalgae have an excellent potential for producing valuable natural products, including biofuels. Therefore, it is imperative to explore and document the existing microalgal flora and utilize their potentials to cope the increasing human needs. The present work aims at exploring and characterizing newly isolated microalgae from desert Cholistan, a habitat with myriad algal diversity. Light microscopy, scanning electron microscopy, and molecular phylogenetic approaches were used for species-level identification. Characterization and growth optimization of Scendesmus sp. were analyzed under three different growth modes to determine the most favorable conditions for increasing biomass, growth rate, and lipid content. The results revealed that mixotrophic (MT) mode significantly increases photosynthetic activity, growth rate, and lipid content with glycerol as supplement carbon source. The investigated Scenedesmus dimorphous produced a maximum dry weight of 1.73 g L-1 , improved fatty acid methyl esters profile and yield lipid up to 40% of DCW (68 g L-1 ) under MT mode, which is almost double to that of photoautotrophic cultivation. The glycerol availability in medium has been identified as the critical element for boosting growth and lipid content. Thus, it can reduce the cost of biofuel production.
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  • 文章类型: Journal Article
    Morpho-biological notes and histopathology, based on LM and SEM observations, of the fig cyst nematode Heteroderafici isolated from Ficuscarica roots, collected in home and public gardens of Apulia region, southern Italy, are described and illustrated. Seventy-five localities throughout the Apulia region were sampled and one-quarter of the sampled localities had fig roots infested with H.fici, with population densities ranging from 44 to 180 cysts/100 ml of soil. All attempts to detect H.fici on ornamental Ficus spp. as well as on imported bonsai in Italy were unsuccessful. Morphometric characters of the Italian population conform to those of the type and re-description populations reported for H.fici. Molecular analysis using ITS, D2-D3 expansion domains of the 28S rRNA, and the partial 18S rRNA sequences of H.fici newly obtained in this study matched well with the corresponding sequences of H.fici present in the GenBank database. Phylogenetic trees confirmed and supported the grouping of H.fici in the Humuli group. Heteroderafici completes its embryogenic development in 14-16 days at 25 °C. Post-invasion development and maturity in the roots of F.carica seedlings is completed in 64-68 days at 25-28 °C with juveniles and adults showing different parasitic habits, being endoparasitic and semi-endoparasitic respectively. The establishment of permanent feeding sites that consist of the formation of large syncytia causes anatomical modification of vascular elements and general disorder in the root stelar structures. Syncytia structures associated with mature females showed different degrees of vacuolisation, numbers of syncytial cells, and contained nuclei and nucleoli which were constantly hypertrophied.
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  • 文章类型: Journal Article
    BACKGROUND: Early observations of enamel surfaces prepared by erbium lasers motivated clinicians to use laser as an alternative to chemical etching.
    OBJECTIVE: Evaluate shear bond strength (SBS) values of different dental adhesives on Erbium:Yttrium Aluminum Garnet (Er:YAG) laser prepared enamel and to evaluate possible etching patterns correlations between dental adhesives and SBS values.
    METHODS: One hundred bovine incisors were randomly assigned to SBS tests on enamel (n = 15) and to enamel morphology analysis (n = 5) after Er:YAG laser preparation as follows: Group I - 37% phosphoric acid (PA)+ ExciTE(®); Group II - ExciTE(®); Group III - AdheSE(®) self-etching; Group IV - FuturaBond(®) no-rinse. NR; Group V - Xeno(®) V. Teeth were treated with the adhesive systems and subjected to thermal cycling. SBS were performed in a universal testing machine at 5 mm/min.
    METHODS: One-way ANOVA and post-hoc tests (P < 0.05). For the morphology evaluation, specimens were immersed in Ethylenediamine tetraacetic acid (EDTA) and the etching pattern analyzed under Scanning Electron Microscope (SEM).
    RESULTS: Mean bond strengths were Group I - 47.17 ± 1.61 MPa (type I etching pattern); Group II - 32.56 ± 1.64 MPa, Group III - 29.10 ± 1.34 MPa, Group IV - 23.32 ± 1.53 MPa (type III etching pattern); Group V - 24.43 MPa ± 1.55 (type II etching pattern).
    CONCLUSIONS: Different adhesive systems yielded significantly different SBSs. Acid etching significantly increased the adhesion in laser treated enamel. No differences in SBS values were obtained between AdheSE(®) and ExciTE(®) without condition with PA. FuturaBond(®) NR and Xeno(®) V showed similar SBS, which was lower in comparison to the others adhesives. No correlation between enamel surface morphology and SBS values was observed, except when PA was used.
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