Dental Alloys

牙科合金
  • 文章类型: Journal Article
    背景:直流电的应用会对牙齿移动速度和周围牙周膜胶原周转产生重大影响。本研究旨在深入了解施加电流的最佳特性,以实现增强的组织反应。
    方法:18只雄性Wistar大鼠分为三组(I,II,andIII).使用了裂口设计,每侧分为实验组或对照组。第一组的实验侧,II,III接受20、10和15μA的电流(15分钟,每天两次,共3天)。实验组和对照组都通过NiTi闭合螺旋弹簧接收正畸力。每天确定牙齿移动的量。使用免疫反应性评分(IRS)系统对I型和III型胶原蛋白进行免疫组织化学切片评分。单因素方差分析(ANOVA)和Tukey事后检验用于分析牙齿移动的速度,而Mann-Whitney检验用于分析对照组和实验组之间的IRS分布。
    结果:与对照组相比,所有实验组的牙齿移动有统计学上的显著差异,第3组显示第2天和第3天的最大比率。这得到I型和III型胶原的免疫反应性评分的支持。
    结论:72小时后,III组1型和3型胶原蛋白的表达显着增加。这一发现与牙齿移动的速度一致,与其他组相比,第3组(15μA)最大。
    BACKGROUND: The application of direct current can have a significant impact on the rate of tooth movement and surrounding periodontal ligament collagen turnover. This study aims to provide insight into the optimal characteristics of applied current to achieve enhanced tissue response.
    METHODS: Eighteen male Wistar rats were divided into three groups (I, II, and III). Split mouth design was used, and each side was allocated into an experimental group or control group. Experimental sides of groups I, II, and III received 20, 10, and 15 μA of current (15 min, twice daily for 3 days). Both the experimental and control groups receive an orthodontic force via the NiTi closed coil spring. The amount of tooth movement was determined daily. Immunohistochemistry slides were scored using the immunoreactive scoring (IRS) system for collagen types I and III. One-way Analysis of Variance (ANOVA) and Tukey post hoc test were used to analyse the rate of tooth movement, while Mann-Whitney test was used to analyse IRS distribution between control and experimental groups.
    RESULTS: Compared with the control group, there was a statistically significant difference in tooth movement in all the experimental groups, with group 3 showing the maximum rate on days 2 and 3. This was supported by immunoreactive scores for both collagen types I and III.
    CONCLUSIONS: After 72 hours, the expression of collagen types 1 and 3 increased significantly for group III. This finding was in harmony with the rate of tooth movement, which was maximum for group 3 (15 μA) as compared to other groups.
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  • 文章类型: Journal Article
    背景:正畸治疗过程中常见的情况是正畸托槽粘结失败。这项研究调查了基于Er:YAG激光从金属和陶瓷支架的底座上去除粘合剂以进行重新粘合的影响。
    方法:从患者中收集168颗前磨牙。在第1、2、3和4组中,使用84个金属托槽粘合在前磨牙的颊表面上,而在第1组中应用了84个陶瓷托槽,II,III和IV。组1/I代表初始键合基团,第2/II组是带有新括号的重新结合组,而第3/III组和第4/IV组分别接受Er:YAG激光或火焰处理的回收支架。使用通用试验机在所有样品中进行第一和第二脱粘,以确定剪切粘结强度(SBS)。使用立体显微镜评价粘合剂残留指数(ARI)。使用扫描电子显微镜(SEM)评估新的和处理过的托槽底座。通过单向方差分析了初始键合和重新键合能力的差异,ARI的差异用Kruskal-Wallis检验进行评估.
    结果:在激光处理的陶瓷托槽上观察到更大量的粘合剂残留物。第3组(26.13MPa)的回收金属支架的SBS值与第1组(23.62MPa)相当,而与第4组(12.54MPa)则有显着差异。当使用陶瓷托槽比较4组时,没有观察到这些值的显著差异。第4组ARI评分(2~3分)与其他3组比较差异有统计学意义(P<0.05)。对于第一组,II,III和IV,ARI评分相似(P>0.05).SEM分析未显示由Er:YAG激光处理的金属或陶瓷材料组成的支架底座明显损坏。
    结论:Er:YAG激光治疗作为一种去除粘合剂而不损坏支架的方法,优于火焰治疗。Er:YAG激光治疗后的SBS值和ARI评分与新支架相似,为Er:YAG激光治疗提供进一步的支持,作为回收脱粘支架的可行手段。
    BACKGROUND: Failure of orthodontic bracket bonds is a common occurrence during orthodontic treatment. This study investigated the impact of Er: YAG laser-based removal of adhesive from the bases of metal and ceramic brackets for re-bonding.
    METHODS: A total of 168 extracted premolars were collected from patients. 84 metal brackets were used to be bonded on the buccal surface of the premolars in Groups 1, 2, 3 and 4, while 84 ceramic brackets were applied in Groups I, II, III and IV. Group 1/I represented the initial bonding group, with Group 2/II being the re-bonding group with new brackets, while Groups 3/III and 4/ IV received recycled brackets treated by Er: YAG laser or flaming respectively. Both the first and second de-bonding were performed in all samples using a universal testing machine to determine the shear bond strength (SBS). The adhesive remnant index (ARI) was evaluated using a stereo-microscope. The new and the treated bracket bases were evaluated using scanning electron microscopy (SEM). Differences in initial bonding and re-bonding ability were analyzed through one-way ANOVAs, and differences in ARI were assessed with the Kruskal-Wallis test.
    RESULTS: Greater amounts of adhesive residue were observed on ceramic brackets treated by laser. The SBS values for recycled metal brackets in Group 3 (26.13 MPa) were comparable to Group 1 (23.62 MPa) whereas they differed significantly from Group 4 (12.54 MPa). No significant differences in these values were observed when comparing the 4 groups with ceramic brackets. ARI score in Group 4 (2-3 points) differed significantly from the three other groups (P < 0.05). For Group I, II, III and IV, similar ARI scores were observed (P > 0.05). SEM analysis didn\'t show apparent damage of bracket bases consisting of either metal or ceramic material treated by Er: YAG laser.
    CONCLUSIONS: Er: YAG laser treatment was superior to flame treatment as a means of removing adhesive without damaging the brackets. SBS values and ARI scores following Er: YAG laser treatment were similar to those for new brackets, offering further support for Er: YAG laser treatment as a viable means of recycling debonded brackets.
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  • 文章类型: Journal Article
    铬和钴基合金,以及铬镍钢,最常用于牙科修复术。不幸的是,这些合金,尤其是镍基合金,会引起过敏反应。这些合金的缺点还在于耐腐蚀性不足。为了提高这些合金的性能,非晶Si(C,N)涂层沉积在金属试样的表面上。本文表征了碳化硅氮化物涂层,通过磁控溅射法在牙科修复中使用的镍铬合金表面上沉积。根据沉积参数,获得了不同碳氮比的涂层。该研究分析了它们的结构以及化学和相组成。此外,进行了表面润湿性和表面粗糙度的研究。根据获得的结果,发现Si(C,获得厚度为2至4.5µm的N)型。所有获得的涂层都增加了表面自由能的值。研究表明,Si(C,N)型薄膜可用于牙科修复中作为保护涂层。
    Chromium- and cobalt-based alloys, as well as chrome-nickel steels, are most used in dental prosthetics. Unfortunately, these alloys, especially nickel-based alloys, can cause allergic reactions. A disadvantage of these alloys is also insufficient corrosion resistance. To improve the properties of these alloys, amorphous Si (C,N) coatings were deposited on the surfaces of metal specimens. This paper characterizes coatings of silicon carbide nitrides, deposited by the magnetron sputtering method on the surface of nickel-chromium alloys used in dental prosthetics. Depending on the deposition parameters, coatings with varying carbon to nitrogen ratios were obtained. The study analyzed their structure and chemical and phase composition. In addition, a study of surface wettability and surface roughness was performed. Based on the results obtained, it was found that amorphous coatings of Si (C,N) type with thicknesses of 2 to 4.5 µm were obtained. All obtained coatings increase the value of surface free energy. The study showed that Si (C,N)-type films can be used in dental prosthetics as protective coatings.
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  • 文章类型: Journal Article
    目的:本研究旨在比较插入扭矩(IT),不锈钢(SS-MIs)和钛合金(Ti-MIs)正畸微型植入物之间的弯曲强度(FS)和表面变化。
    方法:二十四个MIs(2x10mm;SS-MIs,n=12;Ti-MIs,n=12)插入20lb/ft3(20PCF)和40lb/ft3(40PCF)密度的人工骨块上。使用数字扭矩计记录最大IT。在2、3和4mm偏转下评估FS。通过扫描电子显微镜(SEM)和能量色散X射线光谱(EDS)评估了MI的表面形貌和化学组成。一般线性和混合模型用于评估MI类型的影响,骨密度和偏转对评估结果的影响。
    结果:Ti-MIs的IT比SS-MIs的IT高1.1Ncm(p=0.018)。在40个PCF测试块中插入的MI的IT比在20个PCF测试块中插入的MI的IT大5.4Ncm(p<0.001)。插入高密度骨(40PCF)的SS-MIs的抗弯强度明显高于其他组,在2mm(98.7±5.1Ncm),3mm(112.0±3.9Ncm)和4mm(120.0±3.4Ncm)的偏转(p<0.001)。SEM证实了Ti-MIs中的断裂。EDS显示在加载的SS-MIs中掺入了18%的C和2.06%的O,和3.91%的C在负载的Ti-MIs中。
    结论:根据这项体外研究的结果,似乎SS-MIs提供足够的稳定性并表现出更大的机械强度,与Ti-MI相比,当插入更高密度的骨骼。
    OBJECTIVE: This study aimed to compare the insertion torque (IT), flexural strength (FS) and surface alterations between stainless steel (SS-MIs) and titanium alloy (Ti-MIs) orthodontic mini-implants.
    METHODS: Twenty-four MIs (2 x 10 mm; SS-MIs, n = 12; Ti-MIs, n = 12) were inserted on artificial bone blocks of 20 lb/ft3 (20 PCF) and 40 lb/ft3 (40 PCF) density. The maximum IT was recorded using a digital torque meter. FS was evaluated at 2, 3 and 4 mm-deflection. Surface topography and chemical composition of MIs were assessed by scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). General linear and mixed models were used to assess the effect of the MI type, bone density and deflection on the evaluated outcomes.
    RESULTS: The IT of Ti-MIs was 1.1 Ncm greater than that obtained for the SS-MIs (p= 0.018). The IT for MIs inserted in 40 PCF test blocks was 5.4 Ncm greater than that for those inserted in 20 PCF test blocks (p < 0.001). SS-MIs inserted in higher density bone (40 PCF) had significantly higher flexural strength than the other groups, at 2 mm (98.7 ± 5.1 Ncm), 3 mm (112.0 ± 3.9 Ncm) and 4 mm (120.0 ± 3.4 Ncm) of deflection (p< 0.001). SEM evidenced fractures in the Ti-MIs. EDS revealed incorporation of 18% of C and 2.06% of O in the loaded SS-MIs, and 3.91% of C in the loaded Ti-MIs.
    CONCLUSIONS: Based on the findings of this in vitro study, it seems that SS-MIs offer sufficient stability and exhibit greater mechanical strength, compared to Ti-MIs when inserted into higher density bone.
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  • 文章类型: Journal Article
    目的:本研究回顾了目前有关扩展有限元方法(XFEM)在临床和实验性牙髓研究中的应用以及XFEM在旋转牙髓镍钛(NiTi)器械循环疲劳评估中的适用性的文献。
    方法:使用适当的搜索词进行电子文献检索,并对标题和摘要进行了相关性筛选。删除重复项后,搜索产生了13次命中,4项研究符合纳入标准.
    结果:迄今为止还没有研究利用XFEM来研究旋转牙髓NiTi器械中的循环疲劳或裂纹扩展。诸如建模材料输入和疲劳标准之类的挑战可以解释在NiTi仪器的机械行为分析中缺乏XFEM的利用。
    结论:综述显示XFEM很少用于牙髓学文献。最近的工作表明,使用XFEM对NiTi结构进行建模的潜在希望。
    OBJECTIVE: The present study reviews the current literature regarding the utilization of the extended finite element method (XFEM) in clinical and experimental endodontic studies and the suitability of XFEM in the assessment of cyclic fatigue in rotary endodontic nickel-titanium (NiTi) instruments.
    METHODS: An electronic literature search was conducted using the appropriate search terms, and the titles and abstracts were screened for relevance. The search yielded 13 hits after duplicates were removed, and four studies met the inclusion criteria for review.
    RESULTS: No studies to date have utilized XFEM to study cyclic fatigue or crack propagation in rotary endodontic NiTi instruments. Challenges such as modelling material inputs and fatigue criteria could explain the lack of utilization of XFEM in the analysis of mechanical behavior in NiTi instruments.
    CONCLUSIONS: The review showed that XFEM was seldom employed in endodontic literature. Recent work suggests potential promise in using XFEM for modelling NiTi structures.
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  • 文章类型: Journal Article
    背景:正畸矫正器中使用的材料的机械性能的变化可能会影响矫正器的工作性能,从而影响临床进展和预后。大量研究证实了合金腐蚀与表面粗糙度升高之间的相关性,直接影响正畸弓丝的工作特性。
    方法:本研究使用了30根镍钛(NiTi)正畸弓丝。随机选择患者并根据随机计划分为三组;(对照组):受试者进行定期口腔卫生;(氟化物组):受试者使用氟化物进行强化预防;(氯己定组):受试者使用氯己定。通过SEM评估代表性样品,然后使用ImageJ软件检查高分辨率的SEM图像以确定表面粗糙度并获得结果进行进一步的统计分析。
    结果:我们的发现表明,在对照组和其他两组之间,三组的前部和后部之间存在显着差异,而在NaF和CHX组之间没有显着差异。总的来说,两组比较的p值为0.000,表明特别是在对照组和NaF组之间存在非常显着的差异。
    结论:含氟化钠的漱口水比对照组和CHX组显示出更明显的表面变化,应根据正畸材料处方以减少副作用。
    BACKGROUND: Alterations in the mechanical properties of the materials utilized in orthodontic appliances could affect the working properties of the appliances, thereby affecting clinical progress and outcome. Numerous studies have confirmed the correlation between alloy corrosion and raised surface roughness, which has a direct impact on the working characteristics of orthodontic archwires.
    METHODS: Thirty nickel-titanium (NiTi) orthodontic archwires were utilized in this study. Patients were randomly selected and allocated into three groups according to the randomization plan; (The control group): subjects practiced regular oral hygiene; (The fluoride group): subjects used fluoride for intensive prophylaxis; (The chlorhexidine group): subjects used chlorhexidine. Representative samples were evaluated by SEM, and then SEM images with high resolution were examined using Image J software to determine the surface roughness and obtain the results for further statistical analysis.
    RESULTS: Our findings indicated a significant difference was found between the three groups regarding the anterior and posterior parts between the control and the two other groups and a non-significant difference between NaF and CHX groups. Overall, the p-value for group comparisons was 0.000 for both parts, indicating a highly significant difference especially between the control and NaF groups.
    CONCLUSIONS: Mouthwashes containing sodium fluoride demonstrated more significant surface alterations than the control and CHX groups and should be prescribed in accordance with orthodontic materials to reduce side effects.
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  • 文章类型: Journal Article
    目的:使用Hedstrom文件评估和比较牙本质缺损的形成,XP-Shaper,TruNatomy,和ReciprocBlue文件系统用于椭圆形根管时。
    方法:选择单根和卵圆管的一百一十五个人下颌前磨牙进行研究。21颗牙齿未经准备(对照),剩下的牙齿被分为准备组(n=21),也就是说,GroupH-Files,组XP-Shaper,TruNatomy集团,和组Reciproc蓝色。通过使用带有水冷的金刚石涂层圆盘,垂直于牙齿的长轴对所有选定的牙齿进行去冠状处理,留下根节约16毫米长。每组均按上述文件系统编制。然后在连续水流下使用金刚石涂层的圆盘在距顶点3、6和9mm处垂直于其长轴剖切所有根。然后检查每个试样是否存在牙本质缺陷/微裂纹。
    结果:XP-Endo整形器组的缺陷数量最低(01/21根)4.7%;TN(04/21)19%,H文件(04/21)19%,而RCBlue(05/21)的缺陷发生率最高,为23.8%。然而,各组间差异无统计学意义(P>0.05)。
    结论:带有旋转和往复牙套以及手动牙套的电机驱动根管器械可能会在牙根牙本质中产生微裂纹,而与其他经过测试的旋转文件系统和H文件仪器相比,XP-Shaper文件系统产生的裂纹最少或更少。
    OBJECTIVE: To evaluate and compare the formation of dentinal defects using hand Hedstrom files, XP-Shaper, TruNatomy, and Reciproc Blue file systems when used for oval shaped root canals.
    METHODS: One hundred and five extracted human mandibular premolars with single root and oval canals were selected for the study. Twenty-one teeth were unprepared (control), and the remaining teeth were divided into the prepared groups (n = 21), that is, Group H-Files, Group XP-Shaper, Group TruNatomy, and Group Reciproc Blue. All selected teeth were de-coronated perpendicular to the long axis of the tooth by using a diamond-coated disk with water cooling, leaving root segments approximately 16 mm in length. Each group was prepared according to the above file system. Then all roots were sectioned perpendicular to their long axes at 3, 6, and 9 mm from the apex using a diamond-coated disk under a continuous water stream. Each specimen was then checked for the presence of dentinal defects/microcracks.
    RESULTS: The XP-Endo shaper group had the lowest number of defects (01/21 roots) 4.7%; TN (04/21) 19%, H-Files (04/21) 19%, and RC Blue (05/21) 23.8% had the highest incidence of defects. However, no significant difference was detected among these groups (P > 0.05).
    CONCLUSIONS: The motor-driven root canal instrumentation with rotary and reciprocating files and hand files may create microcracks in the radicular dentine, whereas the XP-Shaper file system produces minimal or less cracks compared to other tested rotary file systems and H-file instrumentation.
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  • 文章类型: Journal Article
    背景:金属离子的释放可能涉及过敏反应,作为不锈钢(SS304)正畸丝腐蚀的负面影响。这项研究的目的是评估镀锌(Zn涂层)SS正畸丝的耐腐蚀性。
    方法:通过PVD方法在SS线上施加锌涂层。电化学阻抗谱(EIS),使用动电位极化测试和Tafel分析方法来预测Zn涂层和未涂层SS线在中性和酸性环境中的腐蚀行为。
    结果:Ecorr的值,icorr和Rct,电化学腐蚀特性,据报道,在人造唾液和含氟环境中,Zn涂层SS线对未涂层SS线的腐蚀行为更好。Tafel图分析的实验结果与两种生物溶液的电化学阻抗谱分析的实验结果一致。
    结论:通过PVD方法在裸露的SS正畸丝上施加Zn涂层可能会增加下层不锈钢基材的耐腐蚀性。
    BACKGROUND: Releasing of metal ions might implicate in allergic reaction as a negative subsequent of the corrosion of Stainless Steel (SS304) orthodontic wires. The aim of this study was to evaluate the corrosion resistance of zinc-coated (Zn-coated) SS orthodontic wires.
    METHODS: Zinc coating was applied on SS wires by PVD method. Electrochemical impedance spectroscopy (EIS), Potentiodynamic polarization tests and Tafel analysis methods were used to predict the corrosion behavior of Zn-coated and uncoated SS wires in both neutral and acidic environments.
    RESULTS: The values of Ecorr ,icorr and Rct ,which were the electrochemical corrosion characteristics, reported better corrosion behavior of Zn-coated SS wires against uncoated ones in both artificial saliva and fluoride-containing environments. Experimental results of the Tafel plot analyses were consistent with that of electrochemical impedance spectroscopy analyses for both biological solutions.
    CONCLUSIONS: Applying Zn coating on bare SS orthodontic wire by PVD method might increase the corrosion resistance of the underlying stainless-steel substrate.
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  • 文章类型: Journal Article
    背景:这项研究的目的是评估切削槽的侧面展平对镍钛文件的循环阻力和扭转阻力的影响。
    方法:测试了新型的扁平铂金V.EU(PL)和标准的非扁平CCPremiumV.EU(CC)旋转。对于循环疲劳试验,所有的牙根管在人工根管中旋转,曲率为45°,半径为6.06mm,转速为300rpm(每组n=15)。计算故障循环次数(NCF)。对于扭转试验,文件以2rpm顺时针旋转,直到断裂发生。测量断裂时的最大扭矩值,并计算韧性和变形角。随后,在每个实验中随机选择五个片段,使用扫描电子显微镜拍摄碎片的横截面和纵向。在95%的显著性水平下进行非配对t检验。
    结果:CC和PL之间的NCF差异有统计学意义(P<0.05)。CC显示NCF高于PL。在与扭转阻力相关的参数方面,CC和PL之间没有统计学上的显着差异(畸变角,极限强度,和韧性)(P>.05)。
    结论:在本研究的局限性内,档案的侧面展平并没有改善档案的循环阻力或扭转阻力。由于侧面平整可能会降低文件的循环阻力,在临床实践中应谨慎使用此类文件。
    BACKGROUND: The purpose of this study was to evaluate the effect of side flattening of cutting flutes on the cyclic resistance and torsional resistance of nickel-titanium files.
    METHODS: Both novel flattened Platinum V.EU (PL) and standard nonflattened CC Premium V.EU (CC) rotaries were tested. For cyclic fatigue tests, all the files were rotated in an artificial root canal with a curvature of 45° and a radius of 6.06 mm at 300 rpm (n = 15 in each group). The number of cycles to failure (NCF) was calculated. For torsional tests, the files were rotated at 2 rpm clockwise until fracture occurred. The maximum torque value at fracture was measured and the toughness and distortion angle were computed. Subsequently, 5 fragments were randomly selected in each experiment, the cross-section and longitudinal direction of the fragments were photographed using a scanning electron microscope. An unpaired t-test was performed at a significance level of 95%.
    RESULTS: There was a statistically significant difference in NCF between CC and PL (P < .05). CC showed higher NCF than PL. There was no statistically significant difference between CC and PL with regards to the parameters related to torsional resistance (distortion angle, ultimate strength, and toughness) (P > .05).
    CONCLUSIONS: Within the limitations of this study, side flattening of the file did not improve cyclic resistance or torsional resistance of the files. As side flattening may reduce a file\'s cyclic resistance, such files should be used with caution in clinical practice.
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