Ti-6Al-4V

Ti - 6Al - 4V
  • 文章类型: Journal Article
    在航空领域中使用的钛合金部件通常尺寸大并且具有复杂的结构。通过利用多种增材制造工艺,能满足生产的精度和效率要求。我们使用冷金属转移增材制造(CMTAM)和激光金属沉积(LMD)的组合研究了Ti-6Al-4V的混合增材制造,以及使用CMT-LMD混合增材制造工艺制造Ti-6Al-4V组件的可行性。显微结构检查,拉伸测试与数字图像相关和动态压缩实验(通过分离式霍普金森压杆(SHPB)系统)用于评估零件。结果表明,LMD和CMTAM区的界面形成了紧密的冶金结合。在CMTAM和LMD区域中,先验β晶粒表现出外延生长,形成柱状的先验β晶粒。由于激光重熔,CMT-LMD混合添加剂区经历晶粒细化,在界面处产生等轴的先验β晶粒,其平均晶粒尺寸小于CMTAM和LMD区域的晶粒尺寸。微观结构揭示了晶粒取向和形态在区域之间的显着差异,在每个区域形成不同的纹理。在CMT-LMD混合带,由于界面强化,应变集中发生在电弧添加剂区在拉伸试验,导致CMTAM区断裂。在高应变率动态冲击条件下,LMD区域表现出韧性断裂,而CMTAM区显示脆性断裂。混合带结合了韧性和脆性断裂模式,与单个沉积区相比,CMT-LMD杂化材料表现出优异的动态冲击性能。
    The titanium alloy components utilized in the aviation field are typically large in size and possess complex structures. By utilizing multiple additive manufacturing processes, the precision and efficiency requirements of production can be met. We investigated the hybrid additive manufacturing of Ti-6Al-4V using a combination of cold metal transfer additive manufacturing (CMTAM) and laser metal deposition (LMD), as well as the feasibility of using the CMT-LMD hybrid additive manufacturing process for fabricating Ti-6Al-4V components. Microstructural examinations, tensile testing coupled with digital image correlation and dynamic compressive experiments (by the split Hopkinson pressure bar (SHPB) system) were employed to assess the parts. The results indicate that the interface of the LMD and CMTAM zone formed a compact metallurgical bonding. In the CMTAM and LMD zone, the prior-β grains exhibit epitaxial growth, forming columnar prior-β grains. Due to laser remelting, the CMT-LMD hybrid additive zone experiences grain refinement, resulting in equiaxed prior-β grains at the interface with an average grain size smaller than that of the CMTAM and LMD regions. The microstructures reveal significant differences in grain orientation and morphology among the zones, with distinct textures forming in each zone. In the CMT-LMD hybrid zone, due to interfacial strengthening, strain concentration occurs in the arc additive zone during tensile testing, leading to fracture on the CMTAM zone. Under high-strain-rate dynamic impact conditions, the LMD region exhibits ductile fracture, while the CMTAM zone demonstrates brittle fracture. The hybrid zone combines ductile and brittle fracture modes, and the CMT-LMD hybrid material exhibits superior dynamic impact performance compared to the single deposition zone.
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  • 文章类型: Journal Article
    选择性激光熔化(SLM)可以有效地替代传统的加工方法,通过逐层堆积制备具有任意复杂形状的零件。然而,SLMTi-6Al-4V合金通常表现出低延展性和显著的机械性能各向异性,由于针状α\'马氏体和柱状先验β晶粒的存在。后热处理通常用于通过将针状α\'马氏体分解为平衡的αβ相来获得优异的机械性能。在这项研究中,系统研究了SLMTi-6Al-4V合金热处理前后的显微组织和拉伸性能。制造的Ti-6Al-4V样品的微观结构由柱状β晶粒和针状α马氏体组成,这导致高强度(〜1400MPa),但低延展性(〜5%)以及显着的拉伸各向异性。具有层状αβ微观结构的单一热处理样品表现出改善的伸长率为6.8-13.1%,强度为100-200MPa的牺牲,而拉伸各向异性减弱。通过多步高低温(HLT)热处理实现了三峰微观结构,导致强度(〜1090MPa)和延展性(〜17%)的优异组合,而拉伸各向异性几乎被消除。HLT样品的综合力学性能优于常规制造的Ti-6Al-4V合金。
    Selective laser melting (SLM) can effectively replace traditional processing methods to prepare parts with arbitrary complex shapes through layer-by-layer accumulation. However, SLM Ti-6Al-4V alloy typically exhibits low ductility and significant mechanical properties anisotropy due to the presence of acicular α\' martensite and columnar prior β grains. Post-heat treatment is frequently used to obtain superior mechanical properties by decomposing acicular α\' martensite into an equilibrium α + β phase. In this study, the microstructure and tensile properties of SLM Ti-6Al-4V alloy before and after various heat treatments were systematically investigated. The microstructure of the as-fabricated Ti-6Al-4V sample was composed of columnar prior β grains and acicular α\' martensite, which led to high strength (~1400 MPa) but low ductility (~5%) as well as significantly tensile anisotropy. The single heat treatment samples with lamellar α + β microstructure exhibited improved elongation to 6.8-13.1% with a sacrifice of strength of 100-200 MPa, while the tensile anisotropy was weakened. A trimodal microstructure was achieved through multi-step high-to-low-temperature (HLT) heat treatment, resulting in an excellent combination of strength (~1090 MPa) and ductility (~17%), while the tensile anisotropy was almost eliminated. The comprehensive mechanical properties of the HLT samples were superior to that of the conventional manufactured Ti-6Al-4V alloy.
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  • 文章类型: Journal Article
    有限元(FE)方法用于表征热梯度,凝固速率,和Ti-6Al-4V板在选择性激光熔化(SLM)过程中的熔池尺寸。使用计算流体动力学(CFD)模拟验证了结果。建议的FE模型包含一系列直接从G代码文件转换的刀具路径信息,包括舱口间距,激光功率,层厚度,停留时间,和使用Slic3r软件从CAD文件生成的扫描速度。建议的多层,多轨迹有限元模型用于研究激光功率的影响,扫描速度,和扫描路径在通过SLM构建的Ti-6Al-4V板中的微观结构上。还基于所提出的FE模型来确定处理窗口。有限元结果表明,随着激光功率的减小和扫描速度的增加,晶粒的形态,显示出完全柱状的晶体,逐渐偏离完全等轴区域。形成的晶粒取决于激光功率,扫描速度,和沉积位置,但是它们对扫描路径不敏感,从底层到顶层的沉积,形成的晶粒的尺寸逐渐增加,与实验结果吻合较好。
    The finite element (FE) method is used to characterize the thermal gradient, solidification rate, and molten pool sizes of Ti-6Al-4V plates in the process of selective laser melting (SLM). The results are verified by using the computational fluid dynamics (CFD) simulation. The proposed FE model contains a series of toolpath information that is directly converted from a G-code file, including hatch spacing, laser power, layer thickness, dwell time, and scanning speed generated by using Slic3r software from a CAD file. A proposed multi-layer, multi-track FE model is used to investigate the influence of the laser power, scanning speed, and scanning path on the microstructure in the Ti-6Al-4V plate built via SLM. The processing window is also determined based on the proposed FE model. The FE results indicate that, with a decrease in the laser power and an increase in the scanning speed, the morphology of the crystal grains, showing fully columnar crystals, gradually deviates from the fully equiaxed region. The formed grains are dependent on the laser power, scanning speed, and deposition position, but they are not sensitive to the scanning path, and with the deposition from the bottom layer to the top layer, the size of the formed grains is gradually increasing, which shows a good agreement with the experimental results.
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  • 文章类型: Journal Article
    TiAlN涂层硬质合金刀具已用于在航空车间加工Ti-6Al-4V合金。然而,TiAlN涂层对Ti-6Al-4V合金在各种冷却条件下加工中表面形貌和刀具磨损的影响尚未在公开发表的文献中报道。在我们目前的研究中,Ti-6Al-4V与无涂层和TiAlN工具在干燥下的车削实验,MQL,洪水冷却,和低温喷雾射流冷却条件进行。选取加工表面粗糙度和刀具寿命作为评价TiAlN涂层在各种冷却条件下对Ti-6Al-4V切削性能影响的两个主要定量指标。结果表明,与未涂覆的刀具相比,TiAlN涂层难以在75m/min的低速下改善切削钛合金的加工表面粗糙度和刀具磨损。与未涂覆的刀具相比,TiAlN刀具在150m/min的高速下车削Ti-6Al-4V时具有出色的刀具寿命。从在高速车削Ti-6Al-4V中获得成品表面粗糙度和优越的刀具寿命的角度来看,在低温喷雾射流冷却条件下,选择TiAlN刀具是可行的、合理的。本研究的研究成果和结论可指导航空工业Ti-6Al-4V切削刀具的优化选择。
    TiAlN-coated carbide tools have been used to machine Ti-6Al-4V alloys in aviation workshops. However, the effect of TiAlN coating on surface morphology and tool wear in the processing of Ti-6Al-4V alloys under various cooling conditions has not been reported in the public published literature. In our current research, turning experiments of Ti-6Al-4V with uncoated and TiAlN tools under dry, MQL, flood cooling, and cryogenic spray jet cooling conditions were carried out. The machined surface roughness and tool life were selected as the two main quantitative indexes for estimating the effects of TiAlN coating on the cutting performance of Ti-6Al-4V under various cooling conditions. The results showed that TiAlN coating makes it hard to improve the machined surface roughness and tool wear of a cutting titanium alloy at a low speed of 75 m/min compared to that achieved by uncoated tools. The TiAlN tools presented excellent tool life in turning Ti-6Al-4V at a high speed of 150 m/min compared to that achieved by uncoated tools. From the perspective of obtaining finished surface roughness and superior tool life in high-speed turning Ti-6Al-4V, the selection of TiAlN tools is feasible and reasonable under the cryogenic spray jet cooling condition. The dedicative results and conclusions of this research could guide the optimized selection of cutting tools in machining Ti-6Al-4V for the aviation industry.
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  • 文章类型: Journal Article
    为了研究激光金属沉积增材制造Ti-6Al-4V(LMDTi64)在宽范围的应力状态和应变速率下的机械性能和失效行为,在0.001-5000/s的应变速率下测试了不同类型的标本。进行数值模拟以收集所有试样发生破坏的临界位置处的局部断裂应变。通过与不同工艺制造的Ti64合金进行比较,LMDTi64合金的失效行为对Lode角参数和应变速率具有较强的敏感性。讨论了初始缺陷在失效中的作用。发现高激光功率和重叠比可以通过减少初始缺陷的数量来改善失效行为。在更高的应变率下观察到断裂表面上的初始缺陷,表明初始裂纹而不是初始空隙作为裂纹扩展点导致最终断裂在较高的应变率。断裂面的扫描电子显微镜观察表明,LMDTi64合金的失效机理因不同的应力状态和应变速率而有所不同。破坏机制的特征是负应力三轴时的剪切断裂,而在准静态加载条件下,在高应力三轴性下,空隙生长断裂在LMDTi64合金的失效机理中起着主导作用。
    To investigate the mechanical property and failure behavior of laser metal deposited additive manufacturing Ti-6Al-4V (LMD Ti64) in a wide range of stress states and strain rates, different types of specimens were tested at strain rates of 0.001-5000/s. Numerical simulations were conducted to collect the local fracture strain at the critical position where the failure happened for all specimens. By comparing with Ti64 alloy manufactured by different techniques, the failure behavior of LMD Ti64 alloy shows a stronger sensitivity to Lode angle parameter and strain rate. The role of initial defects in failure was discussed. It is found that high laser power and overlap ratio can improve the failure behavior by reducing the number of initial defects. The initial defects on the fracture surface at much higher strain rates were observed, indicating that the initial crack rather than initial void acts as the crack growth point leading to the final fracture at higher strain rates. The scanning electron microscope observation of the fracture surface shows that the failure mechanism of LMD Ti64 alloy varies from different stress states and strain rates. The failure mechanism is characterized by the shear fracture at the negative stress triaxiality, whereas the void growth fracture plays a dominant role in the failure mechanism of LMD Ti64 alloy at a high stress triaxiality on the quasi-static loading condition.
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  • 文章类型: Journal Article
    在本文中,提出了垂直于加载方向具有不同密度的五种梯度功能梯度晶格结构,和表面形态,变形行为,研究了以Ti-6Al-4V为建筑材料,通过选择性激光熔化(SLM)制备的功能梯度晶格结构的压缩性能。结果表明,SLM成型过程的激光能量分布特性使球形金属粉末粘附在晶格结构支柱的表面,导致晶格结构的实际相对密度高于设计的理论相对密度,但最大误差不超过3.33%。在相同的相对密度下,密度梯度垂直于加载方向的所有晶格结构都比均匀晶格结构具有更好的机械性能,特别是,LF的弹性模量,线性的屈服强度,指数的第一个最大压缩强度为28.99%,16.77%,比UNIFORM高14.46%。此外,指数和线性单位体积的能量吸收分别高出38.38%和48.29%,分别,而不是制服。断口形貌分析表明,这些晶格结构的断口形貌表现为凹坑和光滑平面,表明晶格结构在压缩载荷下表现出混合的脆性和延性破坏机制。有限元分析结果表明,当加载方向垂直于密度梯度形成方向时,晶格结构的高密度部分是主要的承载部分,晶格结构两端的密度差越大,弹性模量越大。
    In this paper, five grading functional gradient lattice structures with a different density perpendicular to the loading direction were proposed, and the surface morphology, deformation behavior, and compression properties of the functional gradient lattice structures prepared by selective laser melting (SLM) with Ti-6Al-4V as the building material were investigated. The results show that the characteristics of the laser energy distribution of the SLM molding process make the spherical metal powder adhere to the surface of the lattice structure struts, resulting in the actual relative density of the lattice structure being higher than the designed theoretical relative density, but the maximum error does not exceed 3.33%. With the same relative density, all lattice structures with density gradients perpendicular to the loading direction have better mechanical properties than the uniform lattice structure, in particular, the elastic modulus of LF, the yield strength of LINEAR, and the first maximum compression strength of INDEX are 28.99%, 16.77%, and 14.46% higher than that of the UNIFORM. In addition, the energy absorption per unit volume of the INDEX and LINEAR is 38.38% and 48.29% higher, respectively, than that of the UNIFORM. Fracture morphology analysis shows that the fracture morphology of these lattice structures shows dimples and smooth planes, indicating that the lattice structure exhibits a mixed brittle and ductile failure mechanism under compressive loading. Finite element analysis results show that when the loading direction is perpendicular to the density gradient-forming direction, the higher density part of the lattice structure is the main bearing part, and the greater the density difference between the two ends of the lattice structure, the greater the elastic modulus.
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  • 文章类型: Journal Article
    在固液界面,电双层(EDL)内的带电粒子受到静电力的作用,这可能会影响细胞吸收和表面润湿性。在这项研究中,提出了纹理表面的静电力和表面张力模型。然后,研究了鼠成骨细胞(MC3T3-E1)细胞在激光烧蚀的微正方形纹理Ti-6Al-4V表面上的生长和粘附,以证明使用激光处理的纹理可以有效地提高生物活性。三种不同的微正方形纹理亲水表面,呈现19°的较低接触角,22.5°,与光滑表面(56.5°)相比,为31.75°,是用光纤激光器制造的。通过场发射扫描电子显微镜(SEM)和荧光显微镜分析细胞形态和初始细胞附着,分别。结果表明,静电力不仅使纹理表面更亲水,而且使细胞倾向于粘附到突出的凸起的边缘和角落。细胞形态分析还显示细胞更喜欢在每个微正方形凸状突起的边缘和拐角处生长。激光处理的表面更有利于细胞的快速生长和粘附,并且细胞优先附着在亲水性纹理表面上。静电力可能是有效提高Ti-6Al-4V表面生物活性的重要因素,更多的表面沟槽的存在将更有利于提高细胞的生物活性。
    At solid-liquid interfaces, charged particles within the electric double layer (EDL) are acted on by the electrostatic force, which may affect cell absorption and surface wettability. In this study, a model of the electrostatic force and surface tension of textured surfaces was presented. Then, the growth and adhesion of Murine osteoblasts (MC3T3-E1) cells on laser-ablated micro-square-textured Ti-6Al-4V surfaces were studied to demonstrate the use of a laser-processed texture to effectively improve bioactivity. Three different micro-square-textured hydrophilic surfaces, presenting lower contact angles of 19°, 22.5°, and 31.75° compared with that of a smooth surface (56.5°), were fabricated using a fiber-optic laser. Cellular morphology and initial cell attachment were analyzed by field emission scanning electron microscopy (SEM) and fluorescence microscopy, respectively. The results show that the electrostatic force not only made the textured surface more hydrophilic but also made the cells tend to adhere to the edges and corners of the protruding convexes. Cell morphology analysis also showed that cells would prefer to grow at the edges and corners of each micro-square convex protrusion. The laser-treated surfaces were more conducive to rapid cell growth and adhesion, and cells were preferentially attached on the hydrophilic-textured surfaces. Electrostatic force may be an important factor in effectively improving the bioactivity of Ti-6Al-4V surfaces, and the presence of more surface grooves would be more conducive to improving the bioactivity of cells.
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  • 文章类型: Journal Article
    钛合金材料在航空航天中的各种工程应用,飞机,电子,和造船工业,由于当代的不断进步,表面完整性需要提高工程应用。砂带磨削参数和水平直接影响钛合金(TC4)的表面完整性,这进一步影响了钛合金在使用过程中的疲劳寿命。为了研究钛合金在不同粗糙度水平下的表面完整性,用相同类型和不同型号的砂带反复研磨表面。结果表明,在粗糙度Ra水平为0.4μm至0.2μm时,压缩残余应力随着线速度的增加而减小,并且存在较大的表面形态缺陷。在粗糙度Ra为0.2μm或更小的情况下,磨削改善了表面形貌,压缩残余应力随着进料速率的增加而增加,表面硬度随着线速度的增加而降低。此外,该研究促进了在不同粗糙度条件下影响表面完整性的磨削参数和水平的工程,提供了理论基础和实践参考。
    Titanium alloy materials are used in a variety of engineering applications in the aerospace, aircraft, electronics, and shipbuilding industries, and due to the continuous improvement of the contemporary age, surface integrity needs to be improved for engineering applications. Belt grinding parameters and levels directly affect the surface integrity of titanium alloys (TC4), which further affects the fatigue life of the titanium alloys during service. In order to investigate the surface integrity of titanium alloys at different roughness levels, the surfaces were repeatedly ground with the same type and different models of abrasive belts. The results showed that at roughness Ra levels of 0.4 μm to 0.2 μm, the compressive residual stresses decreased with increasing linear velocity and there were problems with large surface morphological defects. At the roughness Ra of 0.2 μm or less, grinding improves the surface morphology, the compressive residual stress increases with increasing feed rate, and the surface hardness decreases with increasing linear velocity. In addition, the research facilitates the engineering of grinding parameters and levels that affect surface integrity under different roughness conditions, providing a theoretical basis and practical reference.
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  • 文章类型: Journal Article
    在本文中,建立了考虑泰勒因子的铣削力预测模型,并给出了该模型在不同铣削参数下预测的Ti-6Al-4V铣削力。在研究中,对Ti-6Al-4V进行了铣削实验,铣削力由测力计收集,通过EBSD观察了铣削前后铣削表面的微观结构演变。通过对实验结果和模型预测结果的对比分析,验证了本文提出的预测模型的可靠性,并进一步分析了铣削参数对铣削力的影响。最后,根据EBSD观察结果,研究了铣削参数对铣削表面微观结构演变的影响。结果表明,切向铣削力和法向铣削力都随着铣削深度和进给速度的增加而增加。在这项研究中选择的铣削参数中,铣削深度对铣削力的影响最大。铣削力模型预测的切向铣削力和法向铣削力的平均误差小于10%,说明本文建立的考虑泰勒因子的铣削力预测模型适用于Ti-6Al-4V铣削力的预测。随着铣削参数的变化,晶粒结构,晶粒尺寸,晶界分布,相位分布,材料表面的微观结构发生不同程度的变化,铣削表面的塑性变形在很大程度上由滑移协调。
    In this paper, a milling force prediction model considering the Taylor factor is established, and the Ti-6Al-4V milling force predicted by the model under different milling parameters is presented. In the study, the milling experiment of Ti-6Al-4V was carried out, the milling force was collected by the dynamometer, and the microstructure evolution of the milling surface before and after milling was observed by EBSD. Through the comparative analysis of the experimental results and the model prediction results, the reliability of the prediction model proposed in this study was verified, and the influences of the milling parameters on the milling force were further analyzed. Finally, based on the EBSD observation results, the effects of the milling parameters on the microstructure evolution of the milling surface were studied. The results show that both the tangential milling force and normal milling force increase with the increase in the milling depth and feed rate. Among the milling parameters selected in this study, the milling depth has the greatest influence on the milling force. The average errors of the tangential milling force and normal milling force predicted by the milling force model are less than 10%, indicating that the milling force prediction model established in this paper considering Taylor factor is suitable for the prediction of the Ti-6Al-4V milling force. With the change in the milling parameters, the grain structure, grain size, grain boundary distribution, phase distribution, and micro-texture of the material surface change to varying degrees, and the plastic deformation of the milling surface is largely coordinated by the slip.
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  • 文章类型: Journal Article
    由于SLM的高成本以及对工艺和材料专业知识的需求,确定通过选择性激光熔化(SLM)制造的Ti-6Al-4V零件的质量仍然是一个挑战。为了了解SLMedTi-6Al-4V零件的相对密度与工艺参数的对应关系,本文使用GridsearchCV方法使用超参数优化开发了优化的极端梯度增强(XGBoost)决策树模型。特别是,检验了用于模型训练和测试的数据集大小对模型预测准确性的影响。结果表明,随着数据集大小的减少,所提出的模型的预测精度降低,但是整体精度可以保持在相对较高的精度范围内,与实验结果吻合良好。基于一个小数据集,优化后的XGBoost模型与人工神经网络(ANN)和支持向量回归(SVR)模型的预测精度进行了比较,结果发现,优化后的XGBoost模型具有较好的平均绝对误差等评价指标,均方根误差,和决定系数。此外,优化后的XGBoost模型可以很容易地扩展到预测更多的金属材料的力学性能由SLM工艺制造。
    Determining the quality of Ti-6Al-4V parts fabricated by selective laser melting (SLM) remains a challenge due to the high cost of SLM and the need for expertise in processes and materials. In order to understand the correspondence of the relative density of SLMed Ti-6Al-4V parts with process parameters, an optimized extreme gradient boosting (XGBoost) decision tree model was developed in the present paper using hyperparameter optimization with the GridsearchCV method. In particular, the effect of the size of the dataset for model training and testing on model prediction accuracy was examined. The results show that with the reduction in dataset size, the prediction accuracy of the proposed model decreases, but the overall accuracy can be maintained within a relatively high accuracy range, showing good agreement with the experimental results. Based on a small dataset, the prediction accuracy of the optimized XGBoost model was also compared with that of artificial neural network (ANN) and support vector regression (SVR) models, and it was found that the optimized XGBoost model has better evaluation indicators such as mean absolute error, root mean square error, and the coefficient of determination. In addition, the optimized XGBoost model can be easily extended to the prediction of mechanical properties of more metal materials manufactured by SLM processes.
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