flexural strength

弯曲强度
  • 文章类型: Journal Article
    混合纤维增强自密实混凝土(HFR-SCC)的使用最近由于其与普通混凝土相比具有显着的优势而升级,例如延展性增加。抗裂性,并消除了压实等的需要。确定火灾事件后HFR-SCC的残余强度特性的过程需要严格的实验工作和大量的资源。因此,这项研究提出了一种新的方法来开发使用基因表达式编程(GEP)算法可靠预测HFR-SCC的抗压强度(cs)和抗弯强度(fs)的方程。这些模型是使用从国际出版的文献中获得的数据开发的,这些文献有八个输入,包括水灰比,温度,纤维含量等.和两个输出参数,即,cs和fs。此外,不同的统计误差度量,如平均绝对误差(MAE),决定系数(R2)和目标函数(OF)等。用于评估已开发方程的准确性。误差评估和外部验证都批准了开发模型预测剩余强度的适用性。此外,对方程进行了灵敏度分析,揭示了温度,水灰比,和高效减水剂是一些预测残余压缩和弯曲强度的主要贡献者。
    The use of hybrid fibre-reinforced Self-compacting concrete (HFR-SCC) has escalated recently due to its significant advantages in contrast to normal concrete such as increased ductility, crack resistance, and eliminating the need for compaction etc. The process of determining residual strength properties of HFR-SCC after a fire event requires rigorous experimental work and extensive resources. Thus, this study presents a novel approach to develop equations for reliable prediction of compressive strength (cs) and flexural strength (fs) of HFR-SCC using gene expression programming (GEP) algorithm. The models were developed using data obtained from internationally published literature having eight inputs including water-cement ratio, temperature, fibre content etc. and two output parameters i.e., cs and fs. Also, different statistical error metrices like mean absolute error (MAE), coefficient of determination ( R 2 ) and objective function (OF) etc. were employed to assess the accuracy of developed equations. The error evaluation and external validation both approved the suitability of developed models to predict residual strengths. Also, sensitivity analysis was performed on the equations which revealed that temperature, water-cement ratio, and superplasticizer are some of the main contributors to predict residual compressive and flexural strength.
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  • 文章类型: Journal Article
    丙烯酸树脂广泛用作可移除正畸矫治器的主要组分。然而,口腔卫生差和正畸矫治器的维护为病原微生物的生长提供了合适的环境。在这项研究中,锶改性磷酸盐基玻璃(Sr-PBG)以0%(对照)添加到正畸丙烯酸树脂中,3.75%,7.5%,和15重量%,以评估新型材料的表面和理化性质及其对白色念珠菌的体外抗真菌作用(C.albicans).表面显微硬度和接触角在对照组和3.75%Sr-PBG组之间没有变化(p>0.05),试验组抗弯强度低于对照组(p<0.05),但Sr-PBG含量无差异(p>0.05)。与对照组相比,所有实验组在24和48小时均显示出抗真菌作用(p<0.05)。这项研究表明,3.75%Sr-PBG对白色念珠菌具有抗真菌作用以及合适的理化性质,这可能有助于将与有害微生物生活在可移动正畸矫治器上相关的不利影响的风险降至最低,并促进各种材料的使用。
    Acrylic resins are widely used as the main components in removable orthodontic appliances. However, poor oral hygiene and maintenance of orthodontic appliances provide a suitable environment for the growth of pathogenic microorganisms. In this study, strontium-modified phosphate-based glass (Sr-PBG) was added to orthodontic acrylic resin at 0% (control), 3.75%, 7.5%, and 15% by weight to evaluate the surface and physicochemical properties of the novel material and its in vitro antifungal effect against Candida albicans (C. albicans). Surface microhardness and contact angle did not vary between the control and 3.75% Sr-PBG groups (p > 0.05), and the flexural strength was lower in the experimental groups than in the control group (p < 0.05), but no difference was found with Sr-PBG content (p > 0.05). All experimental groups showed an antifungal effect at 24 and 48 h compared to that in the control group (p < 0.05). This study demonstrated that 3.75% Sr-PBG exhibits antifungal effects against C. albicans along with suitable physicochemical properties, which may help to minimize the risk of adverse effects associated with harmful microbial living on removable orthodontic appliances and promote the use of various materials.
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  • 文章类型: Journal Article
    这项研究调查了AISI以外的箱式集管轨道的弯曲强度,仅考虑单个频道的容量。实验和有限元都使用,并将结果与AISI进行比较。研究结果强调了轨道在整体弯曲能力中的重要作用。发现AISI保守的比例为34%至152%。故障模式不同于单通道的代码理论预期。紧固件紧密间距边际提高了容量,虽然侧面紧固件提供了显着的增强,但是轨道加宽限制了这种增强。考虑到轨道强度,建议对AISI进行修改,结果显示出良好的准确性。
    The study investigates the bending strength of tracks of box headers beyond AISI, which considers the capacity of individual channels alone. Both experimental and FEM are used, and the results are compared to AISI. The findings highlight tracks\' significant role in the overall bending capacity. AISI is found to be conservative by 34% to 152%. Failure mode is different from code theoretical expectations for a single channel. Fastener close spacing marginally improves the capacity, while side fasteners offer significant enhancement, but track widening limits this enhancement. A modification to AISI is proposed considering track strength, with outcomes showing good accuracy.
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  • 文章类型: Journal Article
    制造实验性光固化图案树脂以生产具有足够尺寸稳定性的图案树脂材料。光固化图案树脂由聚(甲基丙烯酸正丁酯)或聚(甲基丙烯酸异丁酯)(PiBMA)聚合物和甲基丙烯酸酯单体组成。物理性质,燃烧后的残余灰分量,维氏硬度,抗弯强度,测定每种材料的体积聚合收缩率。将制备的树脂获得的数据与市售图案树脂的数据进行比较,帕拉维特G(PG)。与PG相比,一些制备的树脂观察到较低量的残余灰分。所有实验树脂的维氏硬度和弯曲强度值均低于PG。所有基于PiBMA的实验树脂的体积聚合收缩率均低于PG。这些结果表明,基于PiBMA的丙烯酸光固化树脂材料可用于焊接过程中的图案化和索引。
    Experimental light-curing pattern resins were fabricated to produce pattern resin materials with adequate dimensional stability. The light-curing pattern resins consisted of poly(n-butyl methacrylate) or poly(iso-butyl methacrylate) (PiBMA) polymers and methacrylate monomers. The physical properties, amount of residual ash after burning, Vickers hardness, flexural strength, and volumetric polymerization shrinkage of each material were determined. The data obtained for the prepared resins were compared with those of a commercially available pattern resin, Palavit G (PG). A lower amount of residual ash was observed for some of the prepared resins than for PG. The Vickers hardness and flexural strength values of all experimental resins were lower than those of PG. The volumetric polymerization shrinkage of all the experimental resins based on PiBMA was lower than that of PG. These results suggest that acrylic light-curing resin materials based on PiBMA may be useful for patterning and indexing during soldering.
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  • 文章类型: Journal Article
    最近,已开发出一组通用的单阴影树脂基复合材料(RBC),以简化阴影选择过程。优异的机械和物理性能对于修复体的最终成功和临床寿命至关重要。因此,评估单阴影红细胞的特性是当务之急。这项研究旨在确定通用单色调红细胞的弯曲强度(FS)和转化度(DC)。
    在这项研究中,使用了四种商业红细胞;三种通用单色泽红细胞;全色(OC),Charisma®DiamondONE(CD),和VittraAPSUnique(VU),和用作对照的常规纳米杂化复合材料Filtek™Z250XT(FT)。FS和DC使用了60个复合梁和40个复合圆盘,分别。具有三点弯曲试验的通用试验机用于测量FS,而DC是使用傅里叶变换红外光谱仪(FTIR)测量的。使用扫描电子显微镜对每个树脂复合材料组的三个断裂试样进行定性分析。
    ANOVA用于比较四个RBC中FS和DC的平均值(OC,CD,VU,和FT)。在平均FS和DC值(F=673.043,p<0.001和F(=782.4,p<0.0001)中观察到高度显着差异,分别。CD组FS最高,其次是FT和VU组;OC组观察到最低值。此外,发现DC值存在统计学显著差异.在VU中观察到最高的DC值,其次是OC和CD,在FT中观察到最低的DC值。
    通用单阴影红细胞表现出良好的FS,除了OC,表现出显著的低FS。通用单阴影红细胞的DC高于常规纳米杂化复合修复材料。
    UNASSIGNED: Recently, a group of universal single-shade resin-based composites (RBCs) has been developed to simplify the process of shade selection. Excellent mechanical and physical properties are crucial for the ultimate success and clinical longevity of restorations. Therefore, evaluating the properties of the single-shaded RBCs is imperative. This study aimed to determine the flexural strength (FS) and degree of conversion (DC) of universal single-shade RBCs.
    UNASSIGNED: In this study, four commercial RBCs were used; three universal single-shade RBCs; Omnichroma (OC), Charisma® Diamond ONE (CD), and Vittra APS Unique (VU), and a conventional nanohybrid composite Filtek™ Z250 XT (FT) which was used as a control. Sixty composite beams and 40 composite discs were used for FS and DC, respectively. A universal test machine with a three-point bending test was used to measure the FS, whereas the DC was measured using a Fourier-transform infrared spectrometer (FTIR). Three fractured specimens from each resin composite group were qualitatively analyzed using scanning electron microscopy.
    UNASSIGNED: ANOVA was used to compare the mean values of FS and DC among the four RBCs (OC, CD, VU, and FT). Highly significant differences were observed in the mean FS and DC values (F = 673.043, p < 0.001 and F (=782.4, p < 0.0001), respectively. The highest FS was observed in the CD group, followed by FT and VU groups; the lowest value was observed in the OC group. In addition, a statistically significant difference was identified in DC values. The highest DC value was observed in VU, followed by OC and CD, and the lowest DC value was observed in FT.
    UNASSIGNED: Universal single-shade RBCs demonstrated a good FS, except for OC, which exhibited a significantly low FS. The DC of the universal single-shade RBCs was higher than that of the conventional nanohybrid composite restorative material.
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  • 文章类型: Journal Article
    目的:义齿口炎和假体断裂是老年人佩戴可摘义齿时面临的常见问题。为了克服这一点,通过添加抗微生物剂来改进义齿材料而不损害原始性能的若干尝试。这项研究的目的是评估自固化的聚甲基丙烯酸甲酯(PMMA)义齿基托树脂的弯曲强度和显微硬度添加越橘(通常称为蔓越莓)后,提取物作为抗菌剂,在不同的比例。
    方法:体外实验研究。
    方法:在水性溶剂的存在下对冷冻的蔓越莓果实进行提取过程。将冻干提取物以0、0.5、1.0、1.5和2.0干重/重量%的比例添加到自固化PMMA义齿基托树脂的聚合物中。基于蔓越莓的包容,该研究包括一个对照组(0%)和四个实验组(0.5%-2%),共100个样本.对50个研究样品(n=10)进行了弯曲强度的三点弯曲测试。使用扫描电子显微镜(SEM)分析断裂样品的表面。使用维氏硬度试验测定显微硬度。
    方法:进行单向统计ANOVA检验以发现组间差异,其次是Tukey的事后测试,用于多个成对比较。
    结果:弯曲强度范围为66.80至69.28MPa,组间差异无统计学意义(P>0.05)。SEM评估显示蔓越莓提取物在PMMA基质中均匀分散。浓度越高,看到的空隙较少。添加2%蔓越莓的维氏显微硬度值从对照组的15.96显著下降至14.57(P<0.05)。
    结论:将蔓越莓提取物掺入自固化PMMA义齿基托树脂中,高达2干重%,弯曲强度没有下降。然而,与对照组(0%蔓越莓夹杂物)相比,维氏显微硬度值显着降低。
    OBJECTIVE: Occurrence of denture stomatitis and prosthesis breakage are common problems faced by elderly people wearing removable dentures. To overcome this, several attempts are made to improve the denture material by addition of antimicrobials without compromising original properties. The aim of the study was to evaluate flexural strength and microhardness of self-cured polymethyl methacrylate (PMMA) denture base resin after addition of Vaccinium macrocarpon (commonly called as cranberry), extract as antimicrobial, at varying proportions.
    METHODS: Experimental in vitro study.
    METHODS: Frozen cranberry fruits were subjected to extraction process in the presence of aqueous solvents. Lyophilized extract was added in proportions of 0, 0.5, 1.0, 1.5, and 2.0 dry wt/wt % into polymer of self-cure PMMA denture base resin. Based on cranberry inclusion, the study comprised one control (0%) and four test groups (0.5%-2%) with total of 100 samples. A three-point bending test for flexural strength was done for fifty study samples (n = 10). Surface of fractured samples was analyzed using a scanning electron microscope (SEM). Microhardness was determined using Vickers hardness test.
    METHODS: One-way statistical ANOVA test was done to find the difference between groups, followed by Tukey\'s post hoc test for multiple pairwise comparison.
    RESULTS: Flexural strength ranged from 66.80 to 69.28 MPa, and a statistically insignificant difference was observed between groups (P > 0.05). SEM evaluation showed uniformly dispersed strands of cranberry extract in PMMA matrix. With higher concentration, less voids were seen. Vickers microhardness value significantly decreased from 15.96 in the control group to 14.57 with 2% cranberry addition (P < 0.05).
    CONCLUSIONS: Incorporation of cranberry extract into self-cure PMMA denture base resin, up to 2 dry wt %, did not decline the flexural strength. However, there was a significant decrease in Vickers microhardness values when compared against the control group (0% cranberry inclusion).
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  • 文章类型: Journal Article
    目的:评估义齿清洁剂对白色念珠菌粘附的功效及其对表面的影响,光学,和常规树脂的机械性能,碾磨,和3D打印义齿基托。
    方法:共制备了240个树脂样品,120用于测试白色念珠菌的附着力,光学稳定性(ΔE00),粗糙度(Ra),亲水性(°),表面自由能(Owens-Wendt)和120个用于测试白色念珠菌粘附的样品,表面显微硬度(努普),三点试验中的弯曲强度和弹性模量,其中将它们分为3组假牙树脂(n=40)和5组假牙清洁剂(n=8)。数据通过双向方差分析和Tukey检验进行多重比较(α=0.05)。
    结果:使用碱性溶液和稀酸成分的义齿清洁剂在减少白色念珠菌方面表现出最大的效果(P<0.001),然而1%NaOCl显著影响树脂的性能(P<0.05)。3D打印义齿显示,所有清洁剂的表面显微硬度均显着降低(P<0.05)。
    结论:李斯特林在减少白色念珠菌方面表现出优异的疗效,对义齿性能的影响最小,而1%NaOCl对性能有显著的负面影响。对于所有义齿清洁剂,3D打印树脂的机械性能明显低于其他树脂。
    结论:正在出售义齿基托材料以适应CAD/CAM系统,增加使用该系统制造的假牙的用户数量。尽管如此,关于微生物的粘附能力和光学,假牙的表面和机械性能,因此需要进一步调查。
    OBJECTIVE: Evaluate the efficacy of denture cleaners on the adhesion of Candida albicans and their effects on the surface, optical, and mechanical properties of resins for conventional, milled, and 3D-printed denture bases.
    METHODS: A total of 240 resin samples were made, 120 for testing Candida albicans adhesion, optical stabilities (ΔE00), roughness (Ra), hydrophilicity (°), surface free energy (Owens-Wendt) and 120 samples for testing Candida albicans adhesion, surface microhardness (Knoop), flexural strength and modulus of elasticity in a three-point test, in which they were divided into 3 groups of denture resin (n = 40) and subdivided into 5 cleaners of dentures (n = 8). Data were evaluated by two-way ANOVA and Tukey\'s test for multiple comparisons (α = 0.05).
    RESULTS: Denture cleaners with an alkaline solution and dilute acid composition were those that showed the greatest effectiveness in reducing Candida albicans (P < 0.001), however 1% NaOCl significantly affected the properties of the resins (P < 0.05). Denture 3D-printed showed that the surface microhardness was significantly lower for all cleansers (P < 0.05).
    CONCLUSIONS: Listerine demonstrated superior efficacy in reducing Candida albicans with minimal effect on denture properties, whereas 1% NaOCl had a significant negative impact on the properties. The mechanical properties were significantly lower in 3D-printed resin than in other resins for all denture cleansers.
    CONCLUSIONS: Denture base materials are being sold to adapt to the CAD/CAM system, increasing the number of users of dentures manufactured with this system. Despite this, there is little investigation into denture cleaners regarding the adhesion capacity of microorganisms and the optical, surface and mechanical properties of dentures, thus requiring further investigation.
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  • 文章类型: Journal Article
    背景:在牙科,玻璃离聚物水泥(GIC)广泛用于一系列应用。GIC的独特性质包括氟离子释放和再充电,化学键合到牙齿的硬组织,生物相容性,像牙釉质和牙本质一样的热膨胀系数,和可接受的美学。它们的高溶解度和差的机械质量是它们的限制之一。E-玻璃纤维通常用于增强聚合物基质,并通过其较高的二氧化硅含量来识别。
    目的:研究的目的是评估在传统GIC中添加(10wt%和20wt%)硅烷处理的E-玻璃纤维对其机械性能(抗压强度,抗弯强度,和表面硬度)和溶解度。
    方法:通过XRF实现E-玻璃纤维填料的表征,SEM,PSD。通过将E-玻璃纤维填料以按重量计10%和20%添加到传统GIC中来制备样品,形成两个创新群体,并与未修饰的GIC(对照组)进行比较。检查物理性质(膜厚度和初始凝固时间)以确认混合后的可操作性。通过评估抗压强度来进行增强GIC的评估,抗弯强度,硬度,和溶解度(每个测试n=10个样品)。进行单因素方差分析和Tukey检验进行统计分析(p≤0.05)。
    结果:传统的GIC显示出最小的抗压强度,抗弯强度,硬度,和最高的溶解度。虽然用20wt%E玻璃纤维增强的GIC显示出最高的抗压强度,抗弯强度,硬度,和最小的溶解度。同时,用10wt%增强的GIC显示出中等结果(P≤0.05)。
    结论:使用20wt%的E-玻璃纤维作为传统GIC的填料提供了增强作用和降低的溶解度。
    BACKGROUND: In dentistry, glass-ionomer cements (GICs) are extensively used for a range of applications. The unique properties of GIC include fluoride ion release and recharge, chemical bonding to the tooth\'s hard tissues, biocompatibility, a thermal expansion coefficient like that of enamel and dentin, and acceptable aesthetics. Their high solubility and poor mechanical qualities are among their limitations. E-glass fibers are generally utilized to reinforce the polymer matrix and are identified by their higher silica content.
    OBJECTIVE: The purpose of the study was to assess the impact of adding (10 wt% and 20 wt%) silane-treated E-glass fibers to traditional GIC on its mechanical properties (compressive strength, flexural strength, and surface hardness) and solubility.
    METHODS: The characterization of the E-glass fiber fillers was achieved by XRF, SEM, and PSD. The specimens were prepared by adding the E-glass fiber fillers to the traditional GIC at 10% and 20% by weight, forming two innovative groups, and compared with the unmodified GIC (control group). The physical properties (film thickness and initial setting time) were examined to confirm operability after mixing. The evaluation of the reinforced GIC was performed by assessing the compressive strength, flexural strength, hardness, and solubility (n = 10 specimens per test). A one-way ANOVA and Tukey tests were performed for statistical analysis (p ≤ 0.05).
    RESULTS: The traditional GIC showed the least compressive strength, flexural strength, hardness, and highest solubility. While the GIC reinforced with 20 wt% E-glass fibers showed the highest compressive strength, flexural strength, hardness, and least solubility. Meanwhile, GIC reinforced with 10 wt% showed intermediate results (P ≤ 0.05).
    CONCLUSIONS: Using 20 wt% E-glass fiber as a filler with the traditional GIC provides a strengthening effect and reduced solubility.
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  • 文章类型: Journal Article
    本研究旨在评估弯曲强度(FS),表面磨损,以及经受不同后打印条件的3D打印牙科树脂的光学性能。使用树脂材料3D打印了总共240个标本(2×2×25mm²),用于永久(VaresoSmileCrownPlus)VSC和临时(VaresoSmileTemp)VST修复。样品经历五种印刷后条件:没有印刷后固化;在FormCure固化单元中进行后固化;Visioβ真空;IvoclarTargis;或热固化(150°C)30分钟。每组样品(n=24)在后固化后直接进行测试,干燥储存24小时后,或在沸水中水热加速老化16小时。三点弯曲试验用于评估FS。对50个圆盘形试样(n=5/组)进行了两体磨损试验。测量永久性VSC样品的表面光泽度和半透明性(n=5/组)。进行SEM/EDS和统计分析。成形固化装置产生最高的FS和最低的磨损深度(p<0.05)。水热老化显著降低了FS。经受相同印刷后条件的材料之间的FS和磨损值没有统计学差异。VSC组在不同的印刷后处理中表现出相似的光学性质。打印后处理条件对3D打印树脂的FS和磨损有重大影响,而光学性能不受影响。
    This study aimed to evaluate the flexural strength (FS), surface wear, and optical properties of 3D-printed dental resins subjected to different post-printing conditions. A total of 240 specimens (2 × 2 × 25 mm³) were 3D-printed using resin materials for permanent (VaresoSmile Crown Plus) VSC and temporary (VaresoSmile Temp) VST restorations. Specimens underwent five post-printing conditions: no post-printing cure; post-cured in a Form Cure curing unit; Visio Beta Vacuum; Ivoclar Targis; or heat-cured (150 °C) for 30 min. Each group of specimens (n = 24) was tested either directly after post-curing, after 24 h of dry storage, or following hydrothermal accelerated aging in boiling water for 16 h. The three-point bending test was used to evaluate the FS. The two-body wear test was performed on 50 disc-shaped specimens (n = 5/group). Surface gloss and translucency were measured for permanent VSC specimens (n = 5/group). SEM/EDS and statistical analyses were performed. The Form Cure device yielded the highest FS and lowest wear depth (p < 0.05). Hydrothermal aging significantly reduced FS. There were no statistical differences in FS and wear values between materials subjected to same post-printing conditions. VSC groups exhibited similar optical properties across different post-printing treatments. Post-printing treatment conditions had a significant impact on the FS and wear of the 3D-printed resin, while optical properties remained unaffected.
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  • 文章类型: Journal Article
    本文显示了复合材料的三点弯曲强度分析,该复合材料由聚酰胺掺杂短切碳纤维并通过材料挤出(MEX)增材制造技术生产的连续碳纤维增强。作为比较,生产了两种类型的样品:使用碳纤维的未增强和连续纤维增强(CFR)。以确保最高强度性能的两个方向制造样品。强度分析补充了额外的数字图像相关(DIC)分析,可以识别标本中具有最大应变的区域。利用光学显微镜可以对样品的断裂表面进行分形检查。这项研究的结果表明,连续碳纤维增强对材料的刚度和强度都有有益的影响,弯曲强度从未增强复合材料的77.34MPa增加到连续碳纤维增强复合材料的147.03MPa。
    This paper shows the three-point bending strength analysis of a composite material consisting of polyamide doped with chopped carbon fiber and reinforced with continuous carbon fiber produced by means of the material extrusion (MEX) additive manufacturing technique. For a comparison, two types of specimens were produced: unreinforced and continuous fiber-reinforced (CFR) with the use of carbon fiber. The specimens were fabricated in two orientations that assure the highest strength properties. Strength analysis was supplemented by additional digital image correlation (DIC) analysis that allowed for the identification of regions with maximum strain within the specimens. The utilization of an optical microscope enabled a fractographic examination of the fracture surfaces of the specimens. The results of this study demonstrated a beneficial effect of continuous carbon fiber reinforcement on both the stiffness and strength of the material, with an increase in flexural strength from 77.34 MPa for the unreinforced composite to 147.03 MPa for the composite reinforced with continuous carbon fiber.
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