resin-based composite

树脂基复合材料
  • DOI:
    文章类型: Case Reports
    保守的修复方法有助于保留被广泛破坏的重要牙齿的剩余牙齿结构。此病例报告描述了一种用于在后牙中放置陶瓷修复体的单预约椅旁技术。一名患者接受下颌右第一磨牙的治疗,具有断裂的树脂基复合修复体。由于重要纸浆的存在,恢复的程度,牙齿上有龋齿,提出了以下治疗方案:放置采用计算机辅助设计/计算机辅助制造工作流程制造的二硅酸锂玻璃陶瓷覆盖物。在牙医移除修复物并进行选择性龋齿去除后,结构分析指导颊尖的减少。立即使用2步自蚀粘合剂系统进行牙本质密封,放置1mm厚的可流动树脂基复合材料层作为树脂涂层。获得了数字印模,镶嵌修复是设计的,研磨二硅酸锂块,随后结晶。当onlay完成时,牙齿准备是喷砂的,选择性蚀刻,并涂有通用粘合剂。清洁并涂上底漆的凹版表面,上嵌体是用双重固化树脂水泥粘结的,并完成了咬合调整。在1个月和4个月的随访检查显示该病例的临床成功。从开始到结束,制作一次预约的椅子旁修复大约需要2.5小时。在这种情况下使用的技术提供了快节奏的工作流程,对于患者来说是舒适和实用的,并且提供了可预测的临床结果,而无需临时修复。
    A conservative approach to restoration assists in preserving the remaining tooth structure of extensively destroyed vital teeth. This case report describes a single-appointment chairside technique for placement of ceramic restorations in posterior teeth. A patient presented for treatment of her mandibular right first molar, which had a fractured resin-based composite restoration. Due to the presence of vital pulp, extent of the restoration, and presence of caries in the tooth, the following treatment plan was proposed: placement of a lithium disilicate glass-ceramic onlay fabricated with a computer-aided design/computer-aided manufacturing workflow. After the dentist removed the restoration and performed selective caries removal, structural analysis guided the reduction of the buccal cusps. Immediate dentin sealing was performed with a 2-step self-etching adhesive system, and a 1-mm-thick layer of flowable resin-based composite was placed as a resin coating. A digital impression was obtained, the onlay restoration was designed, and a lithium disilicate block was milled and subsequently crystallized. When the onlay was completed, the tooth preparation was sandblasted, selectively etched, and coated with a universal adhesive. The intaglio surface of the onlay was cleaned and primed, the onlay was bonded with dual-cure resin cement, and occlusal adjustments were completed. Follow-up examinations at 1 and 4 months revealed the clinical success of the case. From start to finish, it takes approximately 2.5 hours to produce a single-appointment chairside restoration. The technique used in this case offers a fast-paced workflow that is comfortable and practical for the patient and provides a predictable clinical outcome without the need for a temporary restoration.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

    求助全文

  • DOI:
    文章类型: Journal Article
    这项体外研究评估了辐射暴露和材料阴影对树脂基复合材料(RBC)的转化度(DC)和显微硬度的影响。A1E(牙釉质)和A4D(牙本质)的64个RBC标本在1000mW/cm2的校准出射量下光固化5、10、15或20秒,导致5、10、15或20J/cm2的辐射暴露水平。使用傅里叶变换红外光谱法测定DC(每个暴露水平每个阴影n=3)。在每个样品的顶表面和底表面上测量努普硬度值(KHN)(每个暴露水平的每个阴影η=5)。使用2-和3-方差分析和事后Tukey检验(α=0.05)分析数据。红细胞阴影不影响DC(P=0.860),和最低的DC值在5J/cm2的暴露水平下达到(P<0.001)。阴影没有影响顶面的KHN,但是辐射暴露水平确实如此,5J/cm2的应用导致显著更低的值(P<0.05)。对于底部表面,遮荫A1E显示显著高于A4D的KHN值(P<0.001)。辐射暴露的增加导致两种色调的RBC的DC和KHN增加,直到对于A1E和A4D的顶表面达到10J/cm2的饱和点。较暗和更不透明的阴影在2毫米深度处没有充分聚合,即使施加了最高的辐射暴露水平。
    This in vitro study evaluated the influence of radiant exposure and material shade on the degree of conversion (DC) and microhardness of a resin-based composite (RBC). Sixty-four RBC specimens in shades A1E (enamel) and A4D (dentin) were light cured at a calibrated exitance of 1000 mW/cm2 for 5, 10, 15, or 20 seconds, resulting in radiant exposure levels of 5, 10, 15, or 20 J/cm2. The DC was determined using Fourier-transform infrared spectroscopy (n = 3 per shade per exposure level). The Knoop hardness number (KHN) was measured on the top and bottom surfaces of each specimen (n = 5 per shade per exposure level). Data were analyzed using 2- and 3-way analyses of variance and post hoc Tukey tests (α = 0.05). The RBC shade did not affect the DC (P = 0.860), and the lowest DC values were achieved with an exposure level of 5 J/cm2 (P < 0.001). The shade did not affect the KHN on the top surface, but the radiant exposure level did, with the application of 5 J/cm2 resulting in significantly lower values (P < 0.05). For the bottom surface, shade A1E showed significantly higher KHN values than A4D (P < 0.001). An increase in the radiant exposure led to increased DC and KHN for both shades of RBC until reaching a saturation point of 10 J/cm2 for A1E and the top surface of A4D. The darker and more opaque shade was not adequately polymerized at a 2-mm depth, even when the highest radiant exposure level was applied.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

    求助全文

  • 文章类型: Journal Article
    背景:最近的研究已经报道了牙科光固化单元(LCU)发出的光的不均匀性。必须了解这种不均匀的光分布如何影响树脂基复合材料(RBC)在其表面各个点处的物理性能。本研究旨在评估LCU梁的不均匀性对不同色调和厚度的红细胞显微硬度的影响。
    方法:四个身体(A1B,A2B,A3B,和A4B),一个牙本质(A3D),并检查了RBC(FiltekZ350XT)的一个釉质阴影(A3E)。以四种厚度(1、2、3和4mm)制造样品并进行40秒的光固化。在中心点进行维氏显微硬度测试,和从每个样品的底面的中心向左和向右3mm。使用光束轮廓仪对LCU光束轮廓进行了表征,同时使用光谱仪测量样品通过后的辐照度。单因素方差分析(ANOVA)和Tukey的事后检验用于分析色调和厚度对辐照度和显微硬度的影响。分别。单向重复测量ANOVA用于比较不同点的显微硬度。Pearson的相关分析检验了辐照度与显微硬度之间的关系。
    结果:LCU的光束轮廓显示出不均匀的光分布。光辐照度随着样品厚度的增加和较暗的阴影而降低(p<0.05)。显微硬度随着样品厚度的增加而下降(p<0.05),并且在中心点处始终高于外围,特别是在较厚(3和4毫米)和较暗的色调(A3B,A4B,和A3D)。在所有评价点的辐照度和显微硬度之间发现正相关(p<0.05)。
    结论:来自LCU的不均匀光发射显着影响RBC样品的显微硬度,取决于厚度和色调。研究结果强调了在临床环境中考虑LCU束不均匀性以确保RBC的最佳聚合的重要性。
    BACKGROUND: Recent studies have reported the inhomogeneity in the light emitted by dental light-curing units (LCUs). It is essential to understand how this uneven light distribution affects the physical properties of resin-based composites (RBCs) at various points across their surfaces. This study aimed to evaluate the effect of LCU beam\'s inhomogeneity on the microhardness of RBCs with different shades and thicknesses.
    METHODS: Four body (A1B, A2B, A3B, and A4B), one dentin (A3D), and one enamel shade (A3E) of RBC (Filtek Z350 XT) were examined. The specimens were fabricated in four thicknesses (1, 2, 3, and 4 mm) and subjected to a 40-second light-curing. Vickers microhardness testing was performed at the center point, and 3 mm left and right from the center at the bottom surface of each sample. The LCU beam profile was characterized using a beam profiler, while irradiance after specimen passage was measured using a spectrometer. One-way analysis of variance (ANOVA) and Tukey\'s post-hoc tests were used to analyze the effects of shades and thicknesses on irradiance and microhardness, respectively. One-way repeated-measures ANOVA was used to compare the microhardness across different points. Pearson\'s correlation analysis examined the relationship between irradiance and microhardness.
    RESULTS: The beam profile of LCU revealed inhomogeneous light distribution. Light irradiance was decreased with both the increase in thickness and darker shade of the specimens (p < 0.05). Microhardness was found to decline with an increase in sample thickness (p < 0.05), and was consistently higher at the center point compared to the periphery, particularly in thicker (3 and 4 mm) and darker shades (A3B, A4B, and A3D). A positive correlation was found between the irradiance and microhardness across all evaluated points (p < 0.05).
    CONCLUSIONS: Inhomogeneous light emission from LCU significantly influences the microhardness of RBC samples, depending on the thicknesses and shades. The findings underline the importance of considering LCU beam inhomogeneity in clinical settings to ensure optimal polymerization of RBC.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

       PDF(Pubmed)

  • 文章类型: Journal Article
    目的:评估单波和多波光固化单元(LCU)的聚合距离对测量的辐照度的影响,相对于制造商报告的与树脂基复合材料(RBC)的物理性能有关的值。
    方法:使用了四个LCU:一个单波和三个多波。用数字辐射计测量辐照度。根据ISO4049:2019在0mm和5mm的聚合距离下进行固化深度(DC)和挠曲强度(FS)测试。
    结果:所有LCU的辐照度均高于制造商报告的辐照度(>25-64%)。当在0至5mm之间进行聚合时,四个LCU的辐照度降低(配对t检验,P<0.001)。所有组的0mm处的DC相似,但在5mm距离处显著降低(ANOVAP<0.001)。FS在Omm处显示出LCU之间的差异(ANOVAP<0.001),并且受聚合距离的影响。弹性模量不受所使用的LCU或距离的影响(ANOVAP>0.001)。
    结论:在聚合过程中,LCU必须尽可能靠近红细胞,随着距离的增加,固化深度和弯曲强度会产生负面影响。
    OBJECTIVE: To evaluate the influence of the polymerization distance of monowave and polywave light curing units (LCUs) on the measured irradiance relative to the value reported by the manufacturer in relation to the physical properties of resin-based composites (RBCs).
    METHODS: Four LCUs were used: one monowave and three polywave. The irradiance was measured with a digital radiometer. Depth of cure (DC) and flexural strength (FS) tests were performed according to ISO 4049:2019 at polymerization distances of 0 mm and 5 mm.
    RESULTS: The irradiance of all LCUs was higher than that reported by the manufacturer (>25-64%). The irradiance of the four LCUs was reduced when polymerization was performed at between 0 to 5 mm (paired t-test, P < 0.001). The DC at 0 mm was similar in all groups but was significantly decreased at 5 mm distance (ANOVA P < 0.001). FS showed differences among the LCUs at 0 mm (ANOVA P < 0.001) and was affected by the polymerization distance. The elastic modulus was unaffected by the LCU used or the distance (ANOVA P > 0.001).
    CONCLUSIONS: The LCU must be positioned as near as possible to RBCs during the polymerization process, as increased distance negatively affects the depth of cure and flexural strength.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

    求助全文

  • 文章类型: Journal Article
    研究了碱性降解前后通用灯罩和常规牙科树脂基复合材料的双轴弯曲强度。圆盘样品由这些树脂基复合材料制备,将一些样品浸入0.1MNaOH溶液中以产生劣化样品。测量和统计测试在碱性降解试验之前和之后的样品的双轴弯曲强度。使用扫描电子显微镜观察双轴弯曲试验后的断裂表面。结果表明,糊状通用遮阳树脂基复合材料在碱降解前的双轴弯曲强度显著(19%)高于常规型,但在碱降解后的材料之间没有观察到差异。另一方面,可流动的通用遮阳树脂基复合材料的双轴弯曲强度显着(约35%)低于常规复合材料,有或没有退化。虽然,对于糊状材料,碱性降解前,通用树脂基复合材料的双轴弯曲强度高于常规树脂基复合材料,降解后两种材料表现出相似的值。对于可流动材料,无论是否存在降解过程,通用遮阳树脂基复合材料的双轴弯曲强度均低于常规树脂基复合材料。这些结果表明,在决定是否使用可流动的通用遮阳树脂基复合材料填充空腔时应谨慎使用。
    The biaxial flexural strength of universal shade and conventional dental resin-based composites before and after alkaline degradation was investigated. Disk samples were prepared from these resin-based composites, and some of the specimens were immersed in 0.1 M NaOH solution to create deteriorated samples. The biaxial flexural strength of the samples before and after the alkaline degradation test was measured and statistically tested. The fracture surfaces after the biaxial flexural test were observed using a scanning electron microscope. The results showed that the biaxial flexural strength of the paste-type universal shade resin-based composite before alkaline degradation was significantly (19%) higher than that of the conventional type, but no difference was observed between the materials after alkaline degradation. On the other hand, the biaxial flexural strength of the flowable universal shade resin-based composites was significantly (around 35%) lower than that of the conventional composite, with or without degradation. Although, for paste-type materials, the biaxial flexural strength of universal shade resin-based composites was higher than that of conventional resin-based composites before alkaline degradation, after degradation the two materials showed similar values. For flowable materials, the biaxial flexural strength of universal shade resin-based composites was lower than that of conventional resin-based composites regardless of the presence or absence of degradation processes. These results suggest that some caution should be used when deciding whether to use flowable universal shade resin-based composite to fill a cavity.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

       PDF(Pubmed)

  • 文章类型: Journal Article
    目的:评估钡玻璃(BG)填料在3D打印树脂基复合材料中对修复结构的影响。
    方法:实验3D打印树脂基复合材料用UDMA70%wt,Bis-EMA20%wt,和TEGDMA10%wt.使用光引发剂TPO和DFI(2%wt)。BG以40%wt和50%wt并入。0%wt的BG用作阴性对照,VarseoSmileCrownplus(Bego)用作商业对照。使用3D打印机打印样本。随后,将样品洗涤并在FormCure(FormLabs)中以405nm在60ºC下进行2×20分钟的后固化。3D打印树脂基复合材料通过弯曲强度进行评估,转换程度,在溶剂中软化,射线不透性,和对牙龈成纤维细胞的细胞毒性。数据采用单因素方差分析(α=0.05)进行统计学分析。
    结果:BG40%(90.5±5.4MPa)之间的抗弯强度没有显着差异,BG50%(102.0±11.7MPa)和VA(105.2±11.7MPa)。与VA相比,添加40%和50%的BG对转化程度没有影响(p>0.05)。所有组均显示在乙醇中浸渍后在溶剂中软化(p<0.05)。所有组的射线不透性均大于1mmAl。BG50%的射线不透性(2.8±0.3mmAl)显著高于其他组(p<0.05)。细胞毒性评估显示所有组的牙龈细胞活力均高于80%。
    结论:在实验性3D打印树脂基复合材料中添加高达50%wt的钡玻璃显示出长期修复结构的有希望的结果。
    OBJECTIVE: To evaluate the influence of the barium glass (BG) filler in 3D printing resin-based composites for restorative structures.
    METHODS: Experimental 3D printing resin-based composites were formulated with UDMA 70%wt, Bis-EMA 20%wt, and TEGDMA 10%wt. Photoinitiators TPO and DFI (2%wt) were used. BG was incorporated at 40%wt and 50%wt. 0%wt BG was used as negative control and the VarseoSmile Crownplus (Bego) was used as a commercial control. Specimens were printed using a 3D printer. Subsequently, specimens were washed and submitted to post-curing with 405 nm at 60ºC for 2 × 20 min at FormCure (FormLabs). 3D printing resin-based composites were evaluated by flexural strength, degree of conversion, softening in solvent, radiopacity, and cytotoxicity against gingival fibroblasts. Data were statistically analyzed using one-way ANOVA (α = 0.05).
    RESULTS: No significant differences in flexural strength were showed between BG40% (90.5 ± 5,4 MPa), BG50% (102.0 ± 11.7 MPa) and VA (105.2 ± 11.7 MPa). Addition of 40% and 50% of BG showed no influence in the degree of conversion compared to VA (p > 0.05). All groups showed softening in solvent after immersion in ethanol (p < 0.05). All groups showed more than 1mmAl of radiopacity. BG50% showed significantly higher radiopacity (2.8 ± 0.3 mmAl) than other groups (p < 0,05). Cytotoxicity evaluation showed gingival cell viability higher than 80% for all groups.
    CONCLUSIONS: Addition of up to 50%wt of barium glass in experimental 3D printing resin-based composites showed promising results for long-term restorative structures.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

    求助全文

  • 文章类型: Journal Article
    目的:本研究检查了LED多波光固化单元(LCU)的两种光固化方案对水吸附的影响,溶解度,在蒸馏水中老化120d的快速和常规的本体填充树脂基复合材料(RBC)的吸湿性膨胀。
    方法:研究了三种本体填充RBC材料:TetricPowerFill®(快速光聚合复合材料)(TPF),TetricEvoCeram散装填充(EVO),和Grandiosox-tra散装填充(GSO)(常规光聚合复合材料)。在3D打印的树脂模具(直径8毫米x高度4毫米)中制备样品,并仅使用2种模式的多波LCU(Bluephase®PowerCure)从一侧进行光固化:3s模式和20s在“标准”模式中。以固定的时间间隔测量120d蒸馏水的吸水率和溶解度,然后重新调节至干燥以测量解吸75d,全部在37±1°C。以相同的时间间隔记录吸湿性(体积)膨胀,直到120d。使用双向方差分析通过SPSS分析数据,单向方差分析,独立t检验,和Tukey的事后校正检验(p<0.05)。
    结果:TPF,当辐照3s时,显示出最小的吸水率(0.83%),溶解度(1.01μg/mm3),与EVO和GSO相比,体积膨胀最小(1.64%)。虽然EVO在3s时显示出最高的吸水率(1.03%)和溶解度(1.95μg/mm3)。GSO在3s和20s方案中具有最低的吸水率(0.67%)和(0.56%),分别。然而,所有吸附和溶解度数据均在ISO4049范围内。
    结论:对于TPF,快速(3秒)聚合不会增加吸水率或溶解度,与20s照射相比。然而,使用两种可比较的散装填充复合材料,快速固化可使吸水率增加15-25%,溶解度增加一倍以上。这些发现与TetricPowerFill在快速和标准协议下观察到的较小体积膨胀一致。表明其在聚合方案中的相对稳定性。
    OBJECTIVE: This study examines the effect of two light-curing protocols from a LED polywave light curing unit (LCU) on water sorption, solubility, and hygroscopic expansion of fast and conventional bulk-fill resin-based composites (RBCs) aged in distilled water for 120 d.
    METHODS: Three bulk-fill RBCs materials were studied: Tetric PowerFill® (fast photo-polymerised composite) (TPF), Tetric EvoCeram bulk-fill (EVO), and GrandioSo x-tra bulk-fill (GSO) (conventional photo-polymerised composites). Specimens were prepared within a 3D-printed resin mold (8-mm diameter x 4-mm height) and light-cured from one side only with 2 modes of polywave LCU (Bluephase® PowerCure): 3 s mode and for 20 s in \"Standard\" mode. Water sorption and solubility were measured at fixed time intervals for 120 d of distilled water storage, then reconditioned to dry to measure desorption for 75 d, all at 37 ± 1 °C. Hygroscopic (volumetric) expansion was recorded at the same time intervals up to 120 d. Data were analysed through SPSS using Two-way ANOVA, One-way ANOVA, independent t-tests, and Tukey\'s post-hoc correction tests (p < 0.05).
    RESULTS: TPF, when irradiated for 3 s demonstrated minimal water sorption (0.83%), solubility (1.01 μg/mm3), and least volumetric expansion (1.64%) compared to EVO and GSO. While EVO showed the highest water sorption (1.03%) and solubility (1.95 μg/mm3) at 3 s. GSO had the lowest sorption (0.67%) and (0.56%) in 3 s and 20 s protocols, respectively. Nevertheless, all the sorption and solubility data were within the ISO 4049 limits.
    CONCLUSIONS: For TPF, fast (3 s) polymerisation did not increase either water sorption or solubility, compared with 20 s irradiation. However, with the two comparative bulk-fill composites, fast cure increased water sorption by 15-25% and more than doubled solubility. These findings were consistent with the lesser volumetric expansions observed for Tetric PowerFill at both the fast and standard protocols, indicating its relative stability across polymerisation protocols.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

    求助全文

  • 文章类型: Journal Article
    对牙科磨损出版物文献的严格审查强调了三个不同的领域,临床资料,实验室数据和临床情况数据的模拟。来自直接和间接体内方法的临床数据值的不精确使得临床数据充其量受到损害。实验室数据显示,重点是寻找简单的实验室耐磨性研究与已建立的材料科学实验室技术之间的相关性,但没有确定实际的相关性。以口腔磨损模拟器的形式在口腔中复制咀嚼周期更多地集中在磨损测试设备上,而不是磨损量化方法上。因此,需要检查x和y平面中的数据采集变量,以考虑它们如何影响牙科文献中记录的实验室磨损测量的准确性和精确度。目前的方法是使用“前三个问题”中概述的教学工具进行的。
    A critical examination of the literature for dental wear publications highlighted three distinct areas, clinical data, laboratory data and the simulation of the clinical situation data. The imprecision of the clinical data values from direct and indirect in vivo methods renders the clinical data compromised at best. Laboratory data showed a focus on finding a correlation between simplistic laboratory abrasive wear resistance studies and established materials science laboratory techniques, but with no actual correlation identified. Replication of the masticatory cycle in the mouth in the form of an oral wear simulator has focussed more on the wear testing devices rather than the wear quantification methods. As a result, the data acquisition variables in the x- and y-planes need to be examined to consider how they can influence the accuracy and precision of the laboratory wear measurements recorded in the dental literature. The current approach was undertaken using the teaching tool outlined in \"The First Three Questions\".
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

    求助全文

  • 文章类型: Journal Article
    树脂复合材料的主要缺点是它们倾向于积聚微生物生物膜,这可能导致继发性龋齿。这项研究的目的是比较含有接触杀灭抗菌剂的商业树脂基复合材料的机械性能和转化程度,甲基丙烯酸二甲基氨基十六酯(DMAHDM),在不同的浓度下,与氟化物释放复合材料。
    对四组进行了测试:TetricNCeram复合材料(G1),TetricEvoCeram(G2),和TetricNCeram,并添加浓度为3%(G3)和5%(G4)的接触杀灭抗菌剂DMAHDM。机械性能,包括弯曲强度,弹性模量,和维氏显微硬度和转化程度进行了研究。
    添加3%和5%DMAHDM导致与TetricEvoCeram相当的挠曲强度值。TetricNCeram与含3%DMAHDM的组相当(p>0.05)。然而,与TetricEvoCeram(93.3±9.4)和5%DMAHDM(p<0.05)相比,它显着更高。TetricNCeram的弹性模量和维氏显微硬度值均显着高于其他组(p<0.05)。此外,TetricEvoCeram的弹性模量与使用3%和5%DMAHDM的组相似。然而,与5%DMAHDM(0.394±0.021)相比,维氏显微硬度值明显更高(p<0.05),而与3%DMAHDM(0.484±0.016)相当(p>0.05)。各组间转化程度无统计学差别(p>0.05)。
    向TetricNCeram中添加3%DMAHDM导致的弯曲强度值与TetricNCeram和TetricEvoCeram相似。DMAHDM不影响TetricNCeram复合材料的转化程度。
    UNASSIGNED: A major drawback of resin composites is their tendency to accumulate microbial biofilms that can lead to secondary caries. The objective of this study was to compare the mechanical properties and the degree of conversion of commercial resin-based composite materials containing a contact-killing antibacterial agent, dimethylaminohexadecyl methacrylate (DMAHDM), at different concentrations, with a fluoride-releasing composite material.
    UNASSIGNED: Four groups were tested: Tetric N Ceram composite material (G1), Tetric Evo Ceram (G2), and Tetric N Ceram with the addition of contact-killing antibacterial agent DMAHDM at concentrations of 3% (G3) and 5% (G4). The mechanical properties, including flexural strength, elastic modulus, and Vickers microhardness and the degree of conversion were investigated.
    UNASSIGNED: Adding 3 % and 5 % DMAHDM resulted in flexural strength values that were comparable to Tetric Evo Ceram. Tetric N Ceram was comparable to the group containing 3 % DMAHDM (p > 0.05). However, it was significantly greater when compared to Tetric Evo Ceram (93.3 ± 9.4) and 5 % DMAHDM (p < 0.05). Both the elastic modulus and Vickers microhardness values of Tetric N Ceram were significantly higher than those of the other groups (p < 0.05). Furthermore, the elastic modulus of Tetric Evo Ceram showed similar results to groups with 3 % and 5 % DMAHDM. Nevertheless, the Vickers microhardness value is significantly higher when compared to 5 % DMAHDM (0.394 ± 0.021) (p < 0.05) while it was comparable to that of 3 % DMAHDM (0.484 ± 0.016) (p > 0.05). There was no statistically significant difference in the degree of conversion between the groups (p > 0.05).
    UNASSIGNED: Adding 3% DMAHDM to Tetric N Ceram resulted in flexural strength values that were similar to those of Tetric N Ceram and Tetric Evo Ceram. DMAHDM did not affect the degree of conversion of Tetric N Ceram composite.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

       PDF(Pubmed)

  • 文章类型: Journal Article
    目的:这项研究调查了三种光固化单元(LCU)的不同发射模式方案的影响:(i)激光(Monet);(ii)四波(PinkWave);(iii)常规LED(EliparS10)在光固化快速或常规填充树脂基复合材料(RBC)时对温度升高(ΔT)和转换度(DC)的影响。目的是将ΔT和DC相关联,和辐射暴露给红细胞标本。
    方法:用两种批量填充RBC填充4mm深度的3D打印树脂模具:TetricPowerFill®(快速光聚合复合材料)(TPF)或TetricEvoCeram®批量填充(EVO)。使用了三个LCU:(i)Monet激光1s和3s(MONET-1s,MONET-3s);(ii)PinkWave四波在升压模式(PW-3s)中用于3s,在标准模式(PW-20s)中用于20s;(iii)EliparS10用于5s(S10-5s),在标准模式(S10-20s)中用于20s。之前获得了二维温度图,在使用热成像摄像机关闭LCU期间和之后的60s内。在五个深度分析热变化:(距RBC顶面0、1、2、3和4mm)。测定最大温升(Tmax)和平均温升(ΔT)。使用不锈钢分体式模具(4X4mm)从每种材料制备圆柱形样品,并用相同的方案进行光固化。使用傅里叶变换红外光谱(FTIR)在LCU关闭后1小时和120秒内测量DC。数据采用三因素方差分析,单向方差分析,独立t检验,和Tukey事后检验(p<0.05)。
    结果:通过各种辐照方案提供的辐射暴露在4.5-30.3J/cm2之间。MONET-1s和PW-3s的短曝光时间可提供最低的辐射曝光量(分别为4.5和5.2J/cm2),并产生最低的ΔT和DC。PW-20s标准模式下的曝光时间越长,S10-20s,MONET-3产生了最高的Tmax,ΔT,和DC两种复合材料。不同深度的复合材料之间的ΔT范围显着变化(31.7-49.9°C)。TPF的DC介于30-65%之间,EVO介于15.3-56%之间。TPF有更高的Tmax,与EVO相比,所有深度和DC的ΔT,在LCU协议中(p<0.05),除PW-20s和MONET-3s外。修复体的冠状部分(1-2mm)具有最高的ΔT。在120s后,4毫米深度的ΔT和DC之间存在正相关。意义:更长,或标准,与较短或高辐照度方案相比,LCU的暴露时间提供了更大的辐射暴露,并且具有更高的DC和ΔT。当快速光聚合的RBC在短时间(1-5s)内接受高辐照度时,与传统的填充RBC相比,其具有相对优异的热和转化结果。
    OBJECTIVE: This study investigated effects of the different emittance-mode protocols from three light curing units (LCUs): (i) a Laser (Monet); (ii) a quad-wave (PinkWave); (iii) a conventional LED (Elipar S10) on the temperature rise (ΔT) and degree of conversion (DC) when photo-curing fast or conventional bulk-fill resin-based composites (RBC). The aim was to correlate ΔT and DC, and the radiant exposure delivered to RBC specimens.
    METHODS: A 3D-printed resin mold of 4 mm depth was filled with two bulk-fill RBCs: Tetric PowerFill® (fast photo-polymerised composite) (TPF) or Tetric EvoCeram® Bulk-Fill (EVO). Three LCUs were used: (i) Monet laser for 1 s and 3 s (MONET-1 s, MONET-3 s); (ii) PinkWave quad-wave used for 3 s in Boost mode (PW-3 s) and for 20 s in standard mode (PW-20 s); (iii) Elipar S10 for 5 s (S10-5 s) and for 20 s in standard mode (S10-20 s). 2-dimensional temperature maps were obtained before, during and for 60 s after the LCU had turned off using a thermal imaging camera. Thermal changes were analysed at five depths: (0, 1, 2, 3, and 4 mm from the top surface of the RBC). The maximum temperature rise (Tmax) and the mean temperature rise (ΔT) were determined. Cylindrical-shaped specimens were prepared from each material using a stainless-steel split mold (4 × 4 mm) and light-cured with the same protocols. The DC was measured for 120 s and at 1 h after LCU had turned off using Fourier Transform Infrared Spectroscopy (FTIR). Data were analysed using Three-way ANOVA, One-way ANOVA, independent t-tests, and Tukey post-hoc tests (p < 0.05).
    RESULTS: Radiant exposures delivered by the various irradiation protocols were between 4.5-30.3 J/cm2. Short exposure times from MONET-1 s and PW-3 s delivered the lowest radiant exposures (4.5 and 5.2 J/cm2, respectively) and produced the lowest ΔT and DC. The longer exposure times in the standard modes of PW-20 s, S10-20 s, and MONET-3 s produced the highest Tmax, ΔT, and DC for both composites. The ΔT range among composites at different depths varied significantly (31.7-49.9 °C). DC of TPF ranged between 30-65% and in EVO between 15.3-56%. TPF had higher Tmax, ΔT for all depths and DC compared to EVO, across the LCU protocols (p < 0.05), except for PW-20 s and MONET-3 s. The coronal part of the restorations (1-2 mm) had the highest ΔT. There was a positive correlation between ΔT and DC at 4-mm depth after 120 s SIGNIFICANCE: Longer, or standard, exposure times of the LCUs delivered greater radiant exposures and had higher DC and ΔT compared to shorter or high-irradiance protocols. The fast photo-polymerised RBC had comparatively superior thermal and conversion outcomes when it received a high irradiance for a short time (1-5 s) compared to the conventional Bulk-Fill RBC.
    导出

    更多引用

    收藏

    翻译标题摘要

    我要上传

    求助全文

公众号