dynamic shear rheometer (DSR)

  • 文章类型: Journal Article
    在应对全球流行病引发的环境紧急情况时,口罩浪费的升级带来了多方面的困境。在这项前卫的研究中,我们揭示了一种新的方法:利用灭菌的切碎的面膜残留物(SMR),主要由100重量组成。%聚丙烯,作为沥青的先驱改性剂。SMR的不同比例(例如,3、6和9wt。%)与新鲜的原始AP-5沥青进行了明智的整合,并接受了广泛的最新检查,包括薄层色谱-火焰离子化检测(TLC-FID),傅里叶变换红外光谱(FT-IR),扫描电子显微镜(SEM),热重分析(TGA),差示扫描量热法(DSC),和特定的流变指标。TLC-FID诊断轨迹突出了SMR对粘合剂的细微差别的恢复影响,由热力学稳定性指数(IC)明显升高而增强的小平面。FT-IR光谱阐明了SMR作为填料的突出作用,否定化学反应性的概念。TGA分析揭示了降解的热开始升高,路标增强了热弹性,而DSC读数在下肢显示出优异的热性能。SEM评估呈现了更清晰的全景图:在升级的SMR合并中,纹理扰动增加,然而,3wt。%混合物显示出最佳效果,相干微纹理与沥青共生。流变学检查揭示了系统的轨迹:渗透率和延展性的下降被软化点和粘度指标的上升所抵消。政变源于DSR分析,明确验证了SMR在减少车辙困扰方面的无与伦比的能力。这项开创性的调查不仅为精致的路面寿命提供了蓝图,而且还倡导了针对大流行废物的可持续对策,体现了环境审慎与基础设施坚韧的融合。
    When navigating the environmental exigencies precipitated by global pandemics, the escalation of mask waste presents a multifaceted dilemma. In this avant-garde research, we unveil a novel approach: harnessing the sterilized shredded mask residues (SMRs), predominantly composed of 100 wt. % polypropylene, as pioneering modifiers for asphalt. Distinct proportions of SMR (e.g., 3, 6, and 9 wt. %) were judiciously integrated with fresh-virgin base AP-5 asphalt and subjected to an extensive suite of state-of-the-art examinations, encompassing thin-layer chromatography-flame ionization detection (TLC-FID), Fourier-transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and specific rheological metrics. The TLC-FID diagnostic trajectories highlighted the nuanced rejuvenating influence of SMR on the binder, a facet reinforced by a pronounced elevation in the thermodynamic stability index (IC). The FT-IR spectra elucidated SMR\'s preeminent role as a filler, negating notions of chemical reactivity. The TGA analyses unveiled an elevated thermal onset of degradation, signposting enhanced thermal resilience, whereas the DSC readings illuminated a superior thermal comportment at lower extremities. The SEM evaluations rendered a clearer panorama: there was heightened textural perturbation at escalated SMR incorporations, yet the 3 wt. % concoction showcased an optimal, coherent microtexture symbiosis with asphalt. The rheological scrutinies revealed a systematic trajectory: a diminishing penetration and ductility countered by ascending softening points and viscosity metrics. The coup de maître stemmed from the DSR analyses, unequivocally validating SMR\'s unparalleled prowess in curtailing rutting distress. This seminal inquiry not only posits a blueprint for refined pavement longevity but also champions a sustainable countermeasure to pandemic-propelled waste, epitomizing the confluence of environmental prudence an d infrastructural fortitude.
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  • 文章类型: Journal Article
    进行了23阶乘设计实验,以研究预热温度(HT)对制造样品的影响,连接温度(BT)到流变仪,使用动态剪切流变仪对来自各种来源的50/70型、70/100型和2型160/220型未改性沥青进行的复合剪切模量(G*)和相位角(δ)和样品的修整状态(Trim)。此外,黑色图和2S2P1D模型用于评估沥青的粘弹性。研究结果表明,G*比δ对变化更敏感。此外,发现8毫米平行板直径对修整状态的灵敏度高于25毫米。被测因素HT一般对被测材料的结果没有统计学上的显著影响,除了160/220_I。在几乎所有测试温度为50/70和160/220_II,通过将系数BT从较低值增加到较高值,G*下降。修剪:BT相互作用对所有材料和温度对G*的影响最大,除了160/220在较低的温度。然而,在δ的情况下,修剪:BT相互作用对70/100和160/220_II具有最显著的影响。黑色图显示没有明显的差异,这可能是变量变化范围有限的结果。
    A 23 factorial design experiment was conducted to study the influence of pre-heating temperature (HT) for manufacturing sample, bonding temperature (BT) onto rheometer, and trimming state (Trim) of the sample on complex shear modulus (G*) and phase angle (δ) using a dynamic shear rheometer on unmodified bitumen of types 50/70, 70/100, and two 160/220 from various sources. In addition, the black diagram and 2S2P1D model were used to evaluate the viscoelastic properties of bitumens. Findings show that the G* is more sensitive to the changes than the δ. Additionally, it was found that the 8 mm parallel plate diameter had a higher sensitivity to the trimming state than the 25 mm. The tested factor HT generally did not have a statistically significant impact on the results of the tested materials, except for 160/220_I. At practically all the temperatures tested for 50/70 and 160/220_II, the G* dropped by increasing the factor BT from a lower to a higher value. The Trim:BT interaction has the greatest impact on all materials and temperatures on G*, except for 160/220 at lower temperatures. However, in the case of δ, the Trim:BT interaction has the most significant effects for 70/100 and 160/220_II. The black diagrams show no discernible differences, which may be a result of the limited range of changes made to the variables.
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  • 文章类型: Journal Article
    就地冷再生(CIR)沥青混合料是修复沥青路面的一种有吸引力的环保方法。然而,由于施工过程中的水分含量,现场沥青混合料通常具有较高的空气空隙,而水分敏感性对于估算道路使用寿命至关重要。因此,本研究的主要目的是根据机械经验(M-E)路面设计来表征水分对aCIR沥青混合料的高温和低温性能的影响,以预测CIR路面破损。通过水分诱导应力测试仪(MIST)模拟水分调节。通过动态模量测试和盘形紧凑型拉伸(DCT)测试估算了CIR沥青混合料(前雾和后雾)的水分敏感性能。此外,采用标准溶剂萃取试验获得再生沥青路面(RAP)和CIR沥青。沥青结合料性能,包括较高的温度和中温性能,通过动态剪切流变仪(DSR)设备进行评估,并通过沥青结合料开裂装置(ABCD)对低温性能进行评估。然后根据路面M-E设计方法对预测的路面裂缝进行了估算。实验结果表明:(1)DCT和动态模量测试对水分调节敏感。在各种温度和频率下,动态模量下降了13%至43%,低温裂解能下降20%。(2)RAP沥青中掺入沥青乳液,降低了抗高温车辙性能,提高了低温抗裂性能和疲劳寿命。M-E设计结果表明,掺入沥青乳液的RAP降低了国际粗糙度指数(IRI)和AC自下而上的疲劳预测,同时增加总车辙和AC车辙预测。CIR路面层中的水分破坏也不会显着影响低交通量的预测困境。总之,CIR技术在项目中的实施改善了沥青路面的低温开裂和疲劳性能。同时,CIR沥青混合料的水分损伤加速了高温车辙和低温开裂,但当用于低流量道路时,它可能是可以接受的。
    Cold in-place recycling (CIR) asphalt mixtures are an attractive eco-friendly method for rehabilitating asphalt pavement. However, the on-site CIR asphalt mixture generally has a high air void because of the moisture content during construction, and the moisture susceptibility is vital for estimating the road service life. Therefore, the main purpose of this research is to characterize the effect of moisture on the high-temperature and low-temperature performance of a CIR asphalt mixture to predict CIR pavement distress based on a mechanistic-empirical (M-E) pavement design. Moisture conditioning was simulated by the moisture-induced stress tester (MIST). The moisture susceptibility performance of the CIR asphalt mixture (pre-mist and post-mist) was estimated by a dynamic modulus test and a disk-shaped compact tension (DCT) test. In addition, the standard solvent extraction test was used to obtain the reclaimed asphalt pavement (RAP) and CIR asphalt. Asphalt binder performance, including higher temperature and medium temperature performance, was evaluated by dynamic shear rheometer (DSR) equipment and low-temperature properties were estimated by the asphalt binder cracking device (ABCD). Then the predicted pavement distresses were estimated based on the pavement M-E design method. The experimental results revealed that (1) DCT and dynamic modulus tests are sensitive to moisture conditioning. The dynamic modulus decreased by 13% to 43% at various temperatures and frequencies, and the low-temperature cracking energy decreased by 20%. (2) RAP asphalt incorporated with asphalt emulsion decreased the high-temperature rutting resistance but improved the low-temperature anti-cracking and the fatigue life. The M-E design results showed that the RAP incorporated with asphalt emulsion reduced the international roughness index (IRI) and AC bottom-up fatigue predictions, while increasing the total rutting and AC rutting predictions. The moisture damage in the CIR pavement layer also did not significantly affect the predicted distress with low traffic volume. In summary, the implementation of CIR technology in the project improved low-temperature cracking and fatigue performance in the asphalt pavement. Meanwhile, the moisture damage of the CIR asphalt mixture accelerated high-temperature rutting and low-temperature cracking, but it may be acceptable when used for low-volume roads.
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  • 文章类型: Journal Article
    In this paper, the possibility of improving the global response of asphalt materials for pavement applications through the use of hydrated lime and Electric Arc-Furnace Steel Slag (EAFSS) was investigated. For this purpose, a set of asphalt mortars was prepared by mixing two different asphalt binders with fine granite aggregate together with hydrated lime or EAFSS at three different percentages. Bending Beam Rheometer (BBR) creep tests and Dynamic Shear Rheometer (DSR) complex modulus tests were performed to evaluate the material response both at low and high temperature. Then, the rheological Huet model was fitted to the BBR creep results for estimating the impact of filler content on the model parameters. It was found that an addition of hydrated lime and EAFSS up to 10% and 5%, respectively, results in satisfactory low-temperature performance with a substantial improvement of the high-temperature behavior.
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