composite resin

复合树脂
  • 文章类型: Journal Article
    本研究旨在评估使用四种不同的表面处理和不同粘度的复合树脂处理的CAD/CAM树脂纳米陶瓷块的修复微剪切粘结强度。对于目前的研究,从具有低速精密切割锯的CAD/CAM树脂纳米陶瓷块(Cerasmart)在水冷下获得96个尺寸为14×12×2mm的样品。根据表面处理工艺将相关样品随机分为四组:用金刚石钻头研磨,氧化铝空气颗粒磨损,长脉冲激光,和短脉冲激光.在硅烷应用之后,将通用粘合剂应用于所有表面处理的样品并用LED固化10s。根据要使用的修复材料的粘度(n=12),将为修复程序制备的样品分为两个子组(微混合复合材料和可注射复合材料)。修理程序后,注意将样品在37°C的培养箱中在蒸馏水中保持24小时。测试了CAD/CAM树脂纳米陶瓷-复合树脂复合物的修复微剪切粘结强度值(μSBSs)。此外,用扫描电子显微镜检查每组随机选择的样品,以评估表面处理和微剪切粘结强度测试后的表面形貌。通过双向ANOVA和Bonferroni检验分析数据。确定修复方案中优选的表面处理显著影响μSBS值(p<0.001)。虽然短脉冲激光空气照射组获得了最高的μSBS值,在长脉冲激光照射的样品中发现最低的μSBS值。然而,用钻头研磨和空气颗粒磨损的样品显示出相似的μSBS值(p>0.05)。修复程序中优选的复合粘度对μSBS值具有显著影响(p<0.001)。然而,表面处理和修复复合材料的粘度之间的相互作用不会以统计学上显著的方式影响μSBS值(p=0.193)。可能建议临床医生用可注射复合材料或用短脉冲激光治疗后修复CAD/CAM树脂纳米陶瓷修复表面。
    This study aims to evaluate the repair micro-shear bond strength of the CAD/CAM resin nanoceramic block treated using four different surface treatments and composite resins of different viscosities. For the current study, 96 samples with dimensions of 14 × 12 × 2 mm were obtained from a CAD/CAM resin nanoceramic block (Cerasmart) with a low-speed precision cutting saw under water cooling. The relevant samples were randomly divided into four groups according to the surface treatment processes: grinding with diamond bur, aluminum oxide airborne-particle abrasion, long-pulse laser, and short-pulse laser. Following silane application, universal adhesive was applied to all surface-treated samples and cured with an LED for 10 s. The samples prepared for the repair procedure were divided into two subgroups (microhybrid composite and injectable composite) according to the viscosity of the repair material to be used (n = 12). After the repair procedure, care was taken to keep the samples in distilled water in an incubator at 37 °C for 24 h. The repair micro-shear bond strength values (μSBSs) of CAD/CAM resin nanoceramic-composite resin complexes were tested. In addition, randomly selected samples from each group were examined with a scanning electron microscope to evaluate the surface topography after both surface treatments and the micro-shear bond strength test. Data were analyzed by two-way ANOVA and Bonferroni test. It was determined that the surface treatment preferred in the repair protocol significantly affected the μSBS value (p < 0.001). While the highest μSBS value was obtained with the short-pulse laser airradiation group, the lowest μSBS values were found in samples with long pulse laser irradiation. However, samples grinded with a bur and airborne-particle abrasion showed similar μSBS values (p > 0.05). The preferred composite viscosity in the repair procedure has a significant effect on the μSBS value (p < 0.001). However, the interaction between the surface treatment and the viscosity of the repair composite does not affect the μSBS values in a statistically significant way (p = 0.193). It may be recommended to clinicians to repair CAD/CAM resin nanoceramic restoration surfaces with injectable composites or after treatment with short-pulse lasers.
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  • 文章类型: Journal Article
    这项研究评估了牙科修复材料的机械性能和配方,该材料由水葫芦的醋酸纤维素(CA)和白虾壳的壳聚糖(C)组成。研究阶段包括提取,配方,功能组测试,抗菌,毒性,吸水性和溶解性,压缩,剪力,拉伸,硬度,微泄漏,热膨胀,和收缩。实验数据采用probit回归分析,单向方差分析,和Kruskal-Wallis测试.数据显示,CA和C具有microxyl和胺基,可以抑制S.mutans,并且无毒。复合树脂分为九种不同浓度的配方:F1(1%CA+3%C),F2(1%CA+5%C),F3(1%CA+7%C),F4(3%CA+3%C),F5(3%CA+5%C),F6(3%CA+7%C),F7(5%CA+3%C),F8(5%CA+5%C),和F9(5%CA+7%C)。F9的机械强度接近对照组,吸收113.33μg/mm3,80μg/mm3溶解度,32.67Mpa抗压强度,17.18Mpa抗拉强度,没有收缩。这表明F9具有作为生态友好型牙科填充材料的潜力。本研究通过结合水葫芦纤维和虾皮壳聚糖完成了修复材料配方的开发。对合成复合树脂和含有虾皮壳聚糖的水葫芦纤维复合材料的机械性能进行比较分析的结果表明,F9配方(CA5%C7%)表现出以下纤维:吸收,抗压强度,抗拉强度,硬度,和热膨胀。
    This study evaluates the mechanical properties and formulation of dental restoration material comprised of cellulose acetate (CA) from water hyacinth and chitosan (C) from white shrimp shells. The research phases included extraction, formulation, functional group testing, antibacterial, toxicity, water absorption and solubility, compressive, shear, tensile, hardness, microleakage, thermal expansion, and shrinkage. The experimental data were analyzed using probit regression, one-way ANOVA, and Kruskal-Wallis test. The data showed that CA and C had microxyl and amine groups, could inhibit S. mutans, and were non-toxic. Composite resins were divided into nine formulations with different concentrations: F1 (1 % CA + 3 % C), F2 (1 % CA + 5 % C), F3 (1 % CA + 7 % C), F4 (3 % CA + 3 % C), F5 (3 % CA + 5 % C), F6 (3 % CA + 7 % C), F7 (5 % CA + 3 % C), F8 (5 % CA + 5 % C), and F9 (5 % CA + 7 % C). The F9 has mechanical strength close to the control group, with 113.33 μg/mm3 absorption, 80 μg/mm3 solubility, 32.67 Mpa compressive strength, 17.18 Mpa tensile strength, and no shrinkage. It shows that F9 has potential as an eco-friendly dental filling material. The present study completed the development of a formulation for a restoration material by combining water hyacinth fiber and shrimp skin chitosan. The outcomes of a comparative analysis of the mechanical properties of synthetic composite resins and water hyacinth fiber composites containing shrimp skin chitosan revealed that the F9 formulation (CA 5 % + C 7 %) exhibited the following fiber: absorption, compressive strength, tensile strength, hardness, and thermal expansion.
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  • 文章类型: Case Reports
    几十年来,美学一直是牙科与功能性的重要方面,但其重要性达到了历史最高水平。因此,在有助于实现这一目标的技术中,带状冠已经显示出令人信服的结果。然而,它的接受没有达到它的潜力,尤其是在普通牙医中,这可能归因于其技术敏感性。此病例报告阐明了该技术的实用性和可靠性,以及作者在努力提高临床医生提供的治疗质量的同时进行的各种修改。
    Aesthetics has been an important aspect of dentistry along with functionality for decades but its significance is at an all-time high. Hence among techniques that contribute toward this goal, strip crown has shown convincing results. However, its acceptance did not reach its potential, especially among general dentists which could be attributed to its technique-sensitive nature. This case report sheds light on the practicality and reliability of this technique along with various modifications made by authors while striving to improve the quality of treatment provided by the clinician.
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  • 文章类型: Journal Article
    目的:以三氟化镱为填料,配制用于3D打印的实验性甲基丙烯酸酯基可光聚合树脂,并评估其机械性能,物理化学,和生物学特性。
    方法:用60重量%UDMA配制树脂基质,40wt%TEGDMA,1wt%TPO,和0.01wt%BHT。添加浓度为1(G1%)的三氟化镱,2(G2%),3(G3%),4(G4%),和5(G5%)wt%。一组保持不添加填料作为对照(GC)。样品在3D构建器软件中设计并使用UV-DLP3D打印机打印。将样品用异丙醇超声处理并UV固化60分钟。测试树脂的转化度(DC),抗弯强度,努普显微硬度,在溶剂中软化,射线不透性,比色分析,和细胞毒性(MTT和SRB)。
    结果:后聚合增加了所有组的转化程度(p<0.05)。G2%在后聚合后显示出最高的DC。G2%与G1%和GC的抗弯强度没有差异(p>0.05)。所有组在溶剂浸渍后显示硬度降低。射线不透性没有发现统计学差异,在溶剂中软化(ΔKHN%),比色分光光度法,细胞毒性(MTT)(p>0.05)。G1%显示SRB测定的细胞活力降低(p<0.05)。
    结论:可以在不损害机械性能的情况下,添加2%三氟化镱作为填料,生产实验性可光聚合3D打印树脂,物理化学,和生物学特性,与目前的临时材料相当。
    OBJECTIVE: To formulate an experimental methacrylate-based photo-polymerizable resin for 3D printing with ytterbium trifluoride as filler and to evaluate the mechanical, physicochemical, and biological properties.
    METHODS: Resin matrix was formulated with 60 wt% UDMA, 40 wt% TEGDMA, 1 wt% TPO, and 0.01 wt% BHT. Ytterbium Trifluoride was added in concentrations of 1 (G1 %), 2 (G2 %), 3 (G3 %), 4 (G4 %), and 5 (G5 %) wt%. One group remained without filler addition as control (GC). The samples were designed in 3D builder software and printed using a UV-DLP 3D printer. The samples were ultrasonicated with isopropanol and UV cured for 60 min. The resins were tested for degree of conversion (DC), flexural strength, Knoop microhardness, softening in solvent, radiopacity, colorimetric analysis, and cytotoxicity (MTT and SRB).
    RESULTS: Post-polymerization increased the degree of conversion of all groups (p < 0.05). G2 % showed the highest DC after post-polymerization. G2 % showed no differences in flexural strength from the G1 % and GC (p > 0.05). All groups showed a hardness reduction after solvent immersion. No statistical difference was found in radiopacity, softening in solvent (ΔKHN%), colorimetric spectrophotometry, and cytotoxicity (MTT) (p > 0.05). G1 % showed reduced cell viability for SRB assay (p < 0.05).
    CONCLUSIONS: It was possible to produce an experimental photo-polymerizable 3D printable resin with the addition of 2 % ytterbium trifluoride as filler without compromising the mechanical, physicochemical, and biological properties, comparable to the current provisional materials.
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    文章类型: Journal Article
    目的:本研究的目的是评估不同粘合策略对临时树脂基材料粘合到釉质表面以及釉质表面粗糙度的剪切粘合强度(SBS)的影响。
    方法:根据所使用的粘合剂策略,将牛门牙随机分为六组(n&#61;10):BRControl(双丙烯酸树脂);Spot-etch&#43;BR(斑点蚀刻&#43;双丙烯酸树脂);Spot-etchSB2&#43;BR(斑点蚀刻&#43;粘合剂&#43;SBfletch43;粘合剂&#43牙釉质表面粗糙度通过表面速度计测定。在万能试验机上进行了SBS试验,和失效模式在放大下分类。通过单因素方差分析(ANOVA)分析SBS数据。配对t检验用于牙釉质表面粗糙度组内比较,Friedman单向重复测量方差分析用于组间牙釉质表面粗糙度的差异,与Tukey事后检验(A=0.05)。
    结果:BRControl具有最低的SBS值(MPa),与其他组相比有显著差异(P≤0.001)。点蚀刻+BR具有最高的SBS值,但与也使用点蚀刻技术的其他组没有显著差异。所有组的粘合失效模式都是主要的。BRControl具有最低的表面粗糙度差,与所有其他组有显著差异(P=0.001)。
    结论:与没有表面预处理相比,可以应用点蚀刻和其他粘合剂策略来增加牙釉质临时修复的SBS值。然而,粘合策略可能会改变搪瓷表面粗糙度,揭示了清洁牙齿表面的重要性。
    The objective of the present study was to evaluate the influence of different adhesive strategies regarding shear bond strength (SBS) of provisional resin--based materials bonded to the enamel surface as well as on the enamel surface roughness.
    Bovine incisors were randomly divided into six groups (n = 10) according to the adhesive strategy used: BRControl (bis-acrylic resin); Spot-etch+BR (spot-etch + bis-acrylic resin); Spot--etchSB2+BR (spot-etch + adhesive + bis-acrylic resin); Spot-etchZ350Flow+BR (spot-etch + flowable composite resin + bis-acrylic resin); SBU+BR (universal adhesive + bis-acrylic resin); Spot-etchSBMP+Z350 (spot-etch + adhesive + composite resin). The enamel surface roughness was determined by a surface profil-ometer. An SBS test was performed in a universal testing machine, and failure modes were classified under magnification. The SBS data were analyzed by one-way analysis of variance (ANOVA). A paired t test was used for enamel surface roughness intragroup comparisons, and the Friedman one-way repeated meas-ures analysis of variance by ranks was used for differences in enamel surface roughness between groups, with the Tukey post hoc test (a = 0.05).
    BRControl had the lowest SBS values (MPa), with a significant difference (P ≤ 0.001) from the other groups. Spot-etch+BR had the highest SBS values but with no significant differences from the other groups in which the spot-etch technique was also used. Adhesive failure mode was predominant for all groups. BRControl had the lowest surface roughness difference, significantly different (P = 0.001) from all the other groups.
    Spot-etch and other adhesive strategies could be applied to increase the SBS values of provisional restorations to enamel compared with no surface pretreatment. However, the adhesive strategy may change the enamel surface roughness, revealing the importance of cleaning the tooth surface.
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  • 文章类型: Journal Article
    目的:本研究的目的是设计和评估用于患者特定美学颜色分级临时贴面的复合树脂组合物。
    方法:复合结构的各种成分(由Ba2SiO4填料搭配,TiO2颜料,和光引发剂)是通过3sUV曝光(405nm,10W/cm2),每50µm厚的层,然后在制造后进行20分钟的后固化处理。观察每种组分对产生的色调的影响,并与常用的VITA色调指南进行比较。通过干燥下的染色老化处理探索着色,湿,人工唾液环境,咖啡,还有可乐.还评估了机械性能。使用色度计进行颜色测量和比较(亮度(L*),绿红色(a*),和蓝黄色(B*)),变化由CIEDE2000(ΔE00)计算,半透明参数(TP)和白度指数(WID)。然后应用组合物颜色分析结果以产生用于模仿自然外观的颜色分级的临时单板。
    结果:机械,所有组合物导致足够的弯曲强度,最大可达到的强度为111.64MPa。同时,复合颜色受每个成分的影响不同。L*值,这表明复合材料的颜色亮度,被TiO2颜料大大调谐,而Ba2SiO4填料仅引发微小变化。光引发剂浓度显著影响黄度,由增加的b*值表示。对于计算的TP和WID也观察到类似的趋势。基于这些评价,成功生成颜色分级的临时贴面,与VITAA3,A2和B1色调匹配。然而,在大量Ba2SiO4和光引发剂下,复合颜色的稳定性降低。
    结论:该研究提供了一种用于制作临时患者特异性颜色分级贴面的成分指南。它提供了有关组成材料对牙齿美学的影响的见解。
    OBJECTIVE: The aim of this study was to design and assess composite resin composition for patient-specific esthetic color-graded temporary veneer.
    METHODS: Various compositions of composite structures (assorted by Ba2SiO4 filler, TiO2 pigment, and photoinitiator) were prepared via additive manufacturing with 3 s UV exposure (405 nm, 10 W/cm2) per 50 µm thick layer followed by 20 min post-curing treatment after fabrication. The effect of each component on the generated color shades was observed and compared to the commonly used VITA shade guide. The coloration was explored by staining aging treatment under dry, wet, artificial saliva environments, coffee, and cola. The mechanical properties were also evaluated. Color measurement and comparison were done using a colorimeter (lightness (L*), green-red color (a*), and blue-yellow color (b*)), and the changes were calculated by CIEDE2000 (ΔE00), translucency parameter (TP) and whiteness index (WID). The composition color analysis results were then applied to produce a color-graded temporary veneer for mimicking a natural look.
    RESULTS: Mechanically, all composition result in adequate bending strength with maximum achievable strength of 111.64 MPa. At the same time, the composite color was affected by each constituent differently. The L* value, which indicates the color lightness of the composite, was considerably tuned by the TiO2 pigment, whereas Ba2SiO4 filler only triggered minor changes. Photoinitiator concentration significantly affected the yellowness, indicated by the increased b* value. Similar tendency also observed toward the calculated TP and WID as well. Based on these evaluations, color-graded temporary veneer successfully generated, matching the VITA A3, A2, and B1 shades gradation. However, the stability of the composite color decreased at high amounts of Ba2SiO4 and photoinitiator.
    CONCLUSIONS: The study presents a composition guide for fabricating temporary patient-specific color-graded veneer. It provides insights on the effect of the constituent material on dental esthetics.
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  • 文章类型: Journal Article
    这项研究评估了三种类型的复合树脂的重复预热对其颜色稳定性的影响。
    在这项体外研究中,在八组(n=16)中评估了直径为10毫米,高度为2毫米的复合树脂和giomer标本,辉煌的搪瓷微混合,和TetricN-Ceram纳米杂化复合树脂,和BeautifilIIgiomer在室温下以及在55-60°C的水浴中预热40次后使用。准备好标本后,用分光光度计测量它们的颜色参数。将样品浸入茶溶液中3小时/天,持续40天,并再次进行分光光度颜色评估。通过双因素方差分析(α=0.05)计算和分析颜色变化(ΔE)。
    复合树脂类型(P<0.001)和预热(P<0.001)及其交互作用(P<0.001)对ΔE的影响显着。浸泡在茶溶液中导致显著更大的颜色变化(P<0.05)。微填充复合树脂的ΔE明显高于纳米杂化(P=0.003)和微杂化复合树脂(P=0.004)。
    重复预热giomer,微杂交,和纳米杂化复合树脂样品在55〜60°C下40次会对其在茶溶液中的颜色稳定性产生不利影响。giomer的颜色变化明显更大。
    UNASSIGNED: This study assessed the effect of repeated preheating of three types of composite resins and a giomer on their color stability.
    UNASSIGNED: In this in vitro study, 128 composite resin and giomer specimens with a 10-mm diameter and a 2-mm height were evaluated in eight groups (n=16) of Heliomolar microfilled, Brilliant Enamel microhybrid, and Tetric N-Ceram nanohybrid composite resins, and Beautifil II giomer used at room temperature and also after preheating of the tube in a water bath at 55‒60 °C for 40 times. After preparing the specimens, their color parameters were measured by a spectrophotometer. The specimens were immersed in a tea solution for 3 hours/day for 40 days and underwent spectrophotometric color assessment again. The color change (∆E) was calculated and analyzed by two-way ANOVA (α=0.05).
    UNASSIGNED: The effects of composite resin type (P<0.001) and preheating (P<0.001) and their interaction effect (P<0.001) were significant on ∆E. Immersion in a tea solution caused a significantly greater color change in giomer (P<0.05). The ∆E of the microfilled composite resin was significantly higher than that of nanohybrid (P=0.003) and microhybrid composite resin (P=0.004).
    UNASSIGNED: Repeated preheating of giomer, microhybrid, and nanohybrid composite resin specimens to 55‒60 °C for 40 times adversely affected their color stability in the tea solution. The color change was significantly greater for giomer.
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  • 文章类型: Journal Article
    目的:复合材料广泛用于牙科直接牙齿修复。然而,他们对修复过程中使用的工作技术高度敏感。即使是微小的程序错误也会对质量产生重大影响,包括修复的寿命。因此,这项研究的目的是确定材料偏好并分析与牙医队列中直接复合修复相关的临床问题。
    方法:以英语创建了20项在线问卷,并在13个国家/地区管理了1830名普通牙医和专家。问卷的第一部分包括四个问题,以引出人口统计数据,第二部分包括16个问题,重点是保守修复的物质偏好,复合修复体的耐久性,以及牙医在复合修复程序中面临的最具挑战性的阶段。
    结果:受访者决定最常使用复合材料进行牙齿修复(OR997.4,95%CI233.8-4254.8,P值<.001)。大多数受访者表示,复合修复体的耐久性约为7至10年(41.5%)。在影响耐久性的因素中,维持干腔是最常报告的原因(47.1%),也是牙医在复合修复程序中面临的首要挑战(61.0%)。
    结论:我们的研究证实,树脂基复合材料是许多国家最受欢迎的直接修复材料。尽管使用这种材料很困难并且涉及多个步骤,在粘合过程中保持干燥的空腔,和材料应用可能会影响这些修复体的治疗成功和耐久性。临床医生需要注意这个问题,并准备适应他们的决策,并考虑选择替代修复材料,如果合适。
    OBJECTIVE: Composite materials are widely used in dentistry for direct tooth restorations. However, they are highly sensitive to the working technique employed during the restorative procedure. Even minor procedural errors can have a significant impact on the quality including the longevity of the restoration. Hence the aim of this study was to determine the material preferences and analyse the clinical problems associated with direct composite restorations in a cohort of dentists.
    METHODS: A 20-item online questionnaire was created in English and administered 1830 general dentists and specialists in 13 countries. The first section of the questionnaire included four questions to elicit demographic data, and the second section comprised 16 questions focused on material preferences for conservative restorations, durability of composite restorations, and the most challenging stages the dentists faced during the composite restorative procedures.
    RESULTS: Respondents decided most often to use composite materials for the tooth restorations (OR 997.4, 95% CI 233.8-4254.8, P value <.001). Most respondents indicated that the durability of composite restorations was approximately 7 to 10 years (41.5%). Among the factors affecting durability, maintenance of a dry cavity was the most often reported reason (47.1%) and the foremost challenge faced by dentists (61.0%) during the composite restorative procedures.
    CONCLUSIONS: Our study confirmed that resin-based composites are the most popular material for direct restoration in many countries. Although working with this material is difficult and involves multiple steps, maintaining a dry cavity during bonding, and material application may affect the therapeutic success and durability of these restorations. Clinicians need to be attentive to this issue and be prepared to adapt their decision-making and consider opting for alternative restorative materials, if appropriate.
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  • 文章类型: Journal Article
    该研究旨在研究激光激活冲洗对用作根管封闭剂的双固化树脂水泥的渗透和微渗漏的影响。
    将38个提取的上磨牙归因于四个实验组。将根机械扩大并消毒(NaOCl)。对照样品(n=11)用常规针冲洗,其他组(n=9)使用三种不同的激光激活冲洗液:2.94µmEr:YAG激光,9,300µmCO2激光器和808nm二极管激光器,带有改良的黑色涂层激光尖端。每组最后用乙二胺四乙酸(EDTA)进行灌溉,用激光激活的次氯酸钠(NaOCl)和氯化钠(NaCl),而在对照中未激活。然后用红色荧光团(罗丹明B)标记牙本质小管,并用双固化树脂水泥(Paracore)密封根管。水泥将染料固定在密封和渗透的牙本质部分上。为了清除未被水泥固定的罗丹明,然后将根水平切片并浸入过氧化氢(H2O2)中。然后用绿色荧光团(荧光素)标记空的牙本质小管空间,允许通过共聚焦显微镜观察浸润和微渗漏。
    与CO2或二极管激光组相比,对照和Er:YAG激光激活样品的中根三分之一的浸润百分比显着升高。所有实验组均存在微渗漏,但在CO2激光激活后明显减少。
    激光活化灌溉影响树脂水泥渗透和微渗漏,取决于所应用的波长。与CO2和二极管激光器相比,Er:YAG激光激活导致更高的渗透和微泄漏值。
    UNASSIGNED: The study aims to investigate the effects of laser-activated irrigation on infiltration and microleakage of a dual-curing resin cement applied as a root canal sealer.
    UNASSIGNED: Thirty-eight extracted upper molars were attributed to four experimental groups. Roots were mechanically enlarged and disinfected (NaOCl). Control samples (n = 11) were irrigated with conventional needles and three different lasers were used to activate the irrigant in the other groups (n = 9): 2.94 µm Er:YAG laser, 9,300 µm CO2 laser and 808 nm diode laser with a modified black coated laser tip. Final irrigation was performed in each group with ethylenediaminetetraacetic acid (EDTA), sodium hypochlorite (NaOCl) and sodium chloride (NaCl) activated with lasers and in the control without activation.Dentin tubules were then labeled with a red fluorophore (Rhodamine B) and the root canals were sealed with a dual-curing resin cement (Paracore). The cement fixed the dye on the sealed and infiltrated dentin parts. To remove the Rhodamine not fixed by the cement, roots were then sectioned horizontally and immersed in hydrogen peroxide (H2O2). The empty dentin tubules spaces were then labeled with a green fluorophore (Fluorescein) allowing the visualization of infiltration and microleakage by confocal microscopy.
    UNASSIGNED: Percentages of infiltration were significantly higher in the middle root third of the control and Er:YAG laser-activated samples compared to CO2 or diode laser groups. Microleakage was present in all experimental groups but significantly less after CO2 laser activation.
    UNASSIGNED: Laser-activated irrigation impacted resin cement infiltration and microleakage dependent on the applied wavelength. Er:YAG laser activation led to higher values of infiltration and microleakage compared to CO2 and diode lasers.
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  • 文章类型: Journal Article
    高填充3D打印树脂的开发需要用于牙科间接修复的粘合协议,以在胶结后实现最佳的粘合强度。这项研究评估了高填料3D打印材料的剪切粘结强度,用于各种表面处理的永久性修复。罗丹雕塑1.0(50%二硅酸锂填料)和2.0陶瓷纳米杂化物(>60%氧化锆和二硅酸锂填料)进行了测试,以Aelite通用车身复合树脂为对照。准备好样品,固化后,并用氧化铝(25µm)喷砂。使用光学轮廓仪分析表面粗糙度。比较了两种键合方案。首先,使用二硅酸锂硅烷(瓷底漆)或氧化锆底漆(Z-PrimePlus)处理组,或不使用粘合剂进行处理。将梁形树脂水泥(DuoLinkUniversal)试样粘结并储存在37°C水浴中。第二,额外的材料组涂有粘合剂(All-BondUniversal),或者随后施用硅烷或者不处理。然后将这些组类似地与树脂水泥样品一起存储。在24小时之后进行剪切粘结测试。在脱粘之后拍摄SEM图像。进行单向ANOVA和事后Duncan进行统计分析。Rodin1.0与硅烷或氧化锆底漆涂层的粘合失败增加,但显著提高了粘结强度与粘结剂的应用。Rodin2.0显示出一致的粘合强度,无论粘合剂的应用,但内聚失效率随粘结剂和填料涂层的增加而增加。在所有组中,除了罗丹1.0没有粘合剂,硅烷涂层增加了内聚失效率。总之,高填料3D打印材料的最佳剪切粘结强度可以通过硅烷涂层和粘结剂应用来实现。
    The development of high-filled 3D printing resin necessitates a bonding protocol for dental indirect restorations to achieve optimal bond strength after cementation. This study evaluates shear bond strengths of high-filler 3D printed materials for permanent restorations with various surface treatments. Rodin Sculpture 1.0 (50% lithium disilicate fillers) and 2.0 Ceramic Nanohybrid (>60% zirconia and lithium disilicate fillers) were tested, with Aelite All-Purpose Body composite resin as control. Samples were prepared, post-cured, and sandblasted with alumina (25 µm). Surface roughness was analyzed using an optical profilometer. Two bonding protocols were compared. First, groups were treated with lithium disilicate silane (Porcelain Primer) or zirconia primer (Z-Prime Plus) or left untreated without a bonding agent. Beam-shaped resin cement (DuoLink Universal) specimens were bonded and stored in a 37 °C water bath. Second, additional sets of materials were coated with a bonding agent (All-Bond Universal), either followed by silane application or left untreated. These sets were then similarly stored alongside resin cement specimens. Shear bond tests were performed after 24 h. SEM images were taken after debonding. One-Way ANOVA and post hoc Duncan were performed for the statistical analysis. Rodin 1.0 exhibited increased adhesive failure with silane or zirconia primer coating, but significantly improved bond strengths with bonding agent application. Rodin 2.0 showed consistent bond strengths regardless of bonding agent application, but cohesive failure rates increased with bonding agent and filler coating. In all groups, except for Rodin 1.0 without bonding agent, silane coating increased cohesive failure rate. In conclusion, optimal shear bond strength for high-filler 3D printing materials can be achieved with silane coating and bonding agent application.
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