Three-point bending test

三点弯曲试验
  • 文章类型: Journal Article
    测量诸如氧化锆的修复材料的弯曲强度对于为临床应用提供适当的适应症和预测性能至关重要。在实验室之间,用于弯曲强度测量的样品制备存在很大差异。目的是评估处理方法,表面处理,和试样的测试方法影响氧化锆的抗弯强度。氧化锆样品(VITAYZHT)(n=270)使用CAD/CAM进行处理,或使用三种不同的表面处理(机加工,地面,抛光),并通过三点弯曲(非倒角/倒角)或双轴弯曲强度测试进行测量。进行了威布尔统计。平均抗弯强度值范围为612MPa(常规,机械加工,三点弯曲非倒角)至1143MPa(CAD/CAM,打磨,双轴弯曲强度)。当使用CAD/CAM进行完全可控的处理并随后进行抛光来制备标本时,可实现最高的可靠性。使用双轴弯曲强度测试方法可以获得更高的强度值,因为相对于有效体积的应力集中较小。抛光减少了表面微裂纹,因此增加了强度值。
    Measuring the flexural strength of restorative materials such as zirconia is crucial for providing proper indications for clinical applications and predicting performance. Great variations in specimen preparation for flexural strength measurements exist among laboratories. The aim was to evaluate how the processing method, surface treatment, and test method of the specimens affect the flexural strength of zirconia. Zirconia specimens (VITA YZ HT) (n = 270) were processed using CAD/CAM or were conventionally milled with three different surface treatments (machined, ground, polished) and were measured with three-point bending (non-chamfered/chamfered) or biaxial flexural strength test. Weibull statistics were conducted. The mean flexural strength values ranged from 612 MPa (conventional, machined, three-point bending non-chamfered) to 1143 MPa (CAD/CAM, polished, biaxial flexural strength). The highest reliability is achieved when specimens are prepared using thoroughly controllable processing with CAD/CAM and subsequently polished. Higher strength values are achieved with the biaxial flexural strength test method because the stress concentration in relation to the effective volume is smaller. Polishing reduces surface microcracks and therefore increases the strength values.
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  • 文章类型: Journal Article
    本文介绍了由四轴玻璃纤维织物和环氧树脂制成的复合材料的三点弯曲测试的实验结果。测试了两种复合材料,一个有8层,另一个有16层;两者具有相同的基质(环氧树脂)。进行了测试,使用五种不同的测试速率从10毫米/分钟到1000毫米/分钟。记录并计算了以下参数:杨氏模量,弯曲应力,挠曲应变,能源,力,四个都是第一峰。实验数据显示,根据测试速率,这些材料没有灵敏度,至少在分析范围内;但是,较厚的复合材料的特征,有16层织物,略低于较薄的复合材料,8层。结果指出,对于相同厚度的复合材料,某些特征,比如第一峰的应力,弯曲模量,应变在第一个峰值,和能量在第一个峰值,对10-1000mm/min范围内的测试速率不敏感。16层复合材料与8层复合材料相比,第一峰的能量是两倍,但是比能量(作为横截面积的能量)具有接近的值:8层复合材料的103.47kJ/m2和16层复合材料的106.51kJ/m2。结果推荐这种复合材料用于抗弯曲组件或低速冲击保护的应用。
    This paper presents experimental results from three-point bending tests for a composite made of quadriaxial glass fiber fabrics and an epoxy resin. Two composites were tested, one with 8 layers and the other with 16 layers; both had the same matrix (the epoxy resin). Tests were carried out, using five different test rates from 10 mm/min to 1000 mm/min. The following parameters were recorded and calculated: Young\'s modulus, flexural stress, flexural strain, energy, force, and all four for the first peak. The experimental data reveal no sensitivity for these materials based on the test rates, at least for the analyzed range; but, the characteristics for the thicker composite, with 16 layers of fabric, are slightly lower than those for the thinner composite, with 8 layers. The results pointed out that, for the same thickness of composite, certain characteristics, such as stress at the first peak, the flexural modulus, strain at the first peak, and energy at the first peak, are not sensitive to the test rate in the range 10-1000 mm/min. The energy at the first peak is double for the 16-layer composite compared to the 8-layer composite, but the specific energy (as energy on cross-sectional area) has close values: 103.47 kJ/m2 for the 8-layer composite and 106.51 kJ/m2 for the 16-layer composite. The results recommend this composite for applications in components with resistance to bending or for low-velocity impact protection.
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  • 文章类型: Journal Article
    挤出聚苯乙烯(XPS)经常用于构造许多不同的结构。因此,有必要适当地表征其机械性能以确保所述结构的安全性。在可用的表征测试中,静态弯曲试验简单,易于执行;由于这些特点,它们应该比其他测试更频繁地进行。在XPS上的静态弯曲试验中,由于XPS的高度灵活性,有几个挑战,所选择的测试方法和样品配置影响表征的准确性。对于泡沫塑料,包括XPS,三点弯曲(TPB)测试方法分别由国际标准化组织(ISO)和日本工业标准(JIS)标准化,如ISO1209-2:2007和JISK7221-2:2006,其中确定样本配置。因此,已经基于这些标准化方法常规地进行了泡沫塑料的TPB测试以表征弯曲性能。相比之下,由于这些标准化方法的存在,对测试方法和样本配置的影响的调查往往被忽略。然而,为了准确表征XPS的弯曲性能,必须详细检查测试方法和样品配置的效果。在这项研究中,三种弯曲性能(杨氏模量,比例极限应力,和弯曲强度)使用三点弯曲(TPB)确定从XPS面板上切下的样品,四点弯曲(FPB),和压缩弯曲(CB)测试,以5的间隔从5到50的不同样品跨度/深度比,并进行统计分析以确定测试的相关性。当TPB中的跨度/深度比范围为25-50、25-50和15-50时,样品配置对杨氏模量的影响可以降低。FPB,和CB测试,分别,而在TPB中,在5-50、20-50和15-50的跨度/深度比范围内,比例极限应力降低了,FPB,和CB测试,分别。此外,在TPB中,当跨度/深度比范围为5-50、20-50和5-50时,对弯曲强度的影响减小,FPB,和CB测试,分别。因此,这些结果表明,当跨度/深度比分别确定为25-50和15-50时,TPB和CB测试比FPB测试更可行。然而,在这些测试中确定的样品弯曲性能中观察到明显的差异。根据这些发现,应该进行进一步的研究来阐明这些差异。
    Extruded polystyrene (XPS) is frequently used in the construction of many different structures. Therefore, it is necessary to appropriately characterize its mechanical properties to ensure the safety of said structures. Among the available characterization tests, static bending tests are simple and easy to perform; owing to these characteristics, they should be performed more frequently than other tests. In static bending tests on XPS, there are several challenges owing to the high flexibility of XPS, and the chosen testing method and sample configuration affect the accuracy of characterization. For cellular plastics, including XPS, three-point bending (TPB) test methods are standardized by the International Organization for Standardization (ISO) and Japanese Industrial Standards (JIS) as in ISO 1209-2:2007 and JIS K 7221-2:2006, respectively, where the sample configurations are determined. Therefore, TPB tests of cellular plastics have been conventionally performed based on these standardized methods to characterize the bending properties. In contrast, investigations on the effects of testing methods and sample configurations have often been neglected due to the existence of these standardized methods. However, to characterize the bending properties of XPS accurately, the effects of the testing method and sample configuration must be examined in detail. In this study, three bending properties (Young\'s modulus, proportional limit stress, and bending strength) of samples cut from an XPS panel were determined using three-point bending (TPB), four-point bending (FPB), and compression bending (CB) tests with varying sample span/depth ratios from 5 to 50 at intervals of 5, and statistical analyses were performed to determine the relevance of the tests. The effect of sample configuration on Young\'s modulus could be reduced when the span/depth ratio range was 25-50, 25-50, and 15-50 in the TPB, FPB, and CB tests, respectively, whereas that on the proportional limit stress was reduced in the span/depth ratio range of 5-50, 20-50, and 15-50 in the TPB, FPB, and CB tests, respectively. Additionally, the effect on the bending strength was reduced when the span/depth ratio range was 5-50, 20-50, and 5-50 in the TPB, FPB, and CB tests, respectively. Therefore, these results suggest that the TPB and CB tests were more feasible than the FPB test when the span/depth ratio was determined as being 25-50 and 15-50, respectively. However, clear differences were observed in the sample bending properties determined in these tests. In light of these findings, further studies should be conducted to elucidate these differences.
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  • 文章类型: Journal Article
    最近,已开发出一组通用的单阴影树脂基复合材料(RBC),以简化阴影选择过程。优异的机械和物理性能对于修复体的最终成功和临床寿命至关重要。因此,评估单阴影红细胞的特性是当务之急。这项研究旨在确定通用单色调红细胞的弯曲强度(FS)和转化度(DC)。
    在这项研究中,使用了四种商业红细胞;三种通用单色泽红细胞;全色(OC),Charisma®DiamondONE(CD),和VittraAPSUnique(VU),和用作对照的常规纳米杂化复合材料Filtek™Z250XT(FT)。FS和DC使用了60个复合梁和40个复合圆盘,分别。具有三点弯曲试验的通用试验机用于测量FS,而DC是使用傅里叶变换红外光谱仪(FTIR)测量的。使用扫描电子显微镜对每个树脂复合材料组的三个断裂试样进行定性分析。
    ANOVA用于比较四个RBC中FS和DC的平均值(OC,CD,VU,和FT)。在平均FS和DC值(F=673.043,p<0.001和F(=782.4,p<0.0001)中观察到高度显着差异,分别。CD组FS最高,其次是FT和VU组;OC组观察到最低值。此外,发现DC值存在统计学显著差异.在VU中观察到最高的DC值,其次是OC和CD,在FT中观察到最低的DC值。
    通用单阴影红细胞表现出良好的FS,除了OC,表现出显著的低FS。通用单阴影红细胞的DC高于常规纳米杂化复合修复材料。
    UNASSIGNED: Recently, a group of universal single-shade resin-based composites (RBCs) has been developed to simplify the process of shade selection. Excellent mechanical and physical properties are crucial for the ultimate success and clinical longevity of restorations. Therefore, evaluating the properties of the single-shaded RBCs is imperative. This study aimed to determine the flexural strength (FS) and degree of conversion (DC) of universal single-shade RBCs.
    UNASSIGNED: In this study, four commercial RBCs were used; three universal single-shade RBCs; Omnichroma (OC), Charisma® Diamond ONE (CD), and Vittra APS Unique (VU), and a conventional nanohybrid composite Filtek™ Z250 XT (FT) which was used as a control. Sixty composite beams and 40 composite discs were used for FS and DC, respectively. A universal test machine with a three-point bending test was used to measure the FS, whereas the DC was measured using a Fourier-transform infrared spectrometer (FTIR). Three fractured specimens from each resin composite group were qualitatively analyzed using scanning electron microscopy.
    UNASSIGNED: ANOVA was used to compare the mean values of FS and DC among the four RBCs (OC, CD, VU, and FT). Highly significant differences were observed in the mean FS and DC values (F = 673.043, p < 0.001 and F (=782.4, p < 0.0001), respectively. The highest FS was observed in the CD group, followed by FT and VU groups; the lowest value was observed in the OC group. In addition, a statistically significant difference was identified in DC values. The highest DC value was observed in VU, followed by OC and CD, and the lowest DC value was observed in FT.
    UNASSIGNED: Universal single-shade RBCs demonstrated a good FS, except for OC, which exhibited a significantly low FS. The DC of the universal single-shade RBCs was higher than that of the conventional nanohybrid composite restorative material.
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  • 文章类型: Journal Article
    为了探索和比较故障模式,变形行为,以及用碳纤维增强聚合物(CFRP)和钢筋加强的单边缺口(SEN)梁的承载能力,静态和动态三点弯曲试验对两种类型的混凝土梁进行了这项研究。在静态测试期间,电液伺服电机用作加载装置,向CFRP梁和钢筋混凝土(RC)梁施加压力。在冲击实验中,通过调整落锤的高度赋予不同的冲击速度。因此,关于裂纹扩展的信息,能量吸收,并获得了变形。静态测试的结果表明,RC梁主要经历剪切破坏。相比之下,CFRP梁主要表现为弯曲剪切破坏,归因于钢筋和混凝土之间的粘结强度相对较弱。在这项研究中,在三种不同的速度下进行了冲击测试。随着撞击速度的增加,两种类型的混凝土梁都从弯曲破坏过渡到弯曲剪切破坏。在最低速度下,在弯曲过程中,用不同材料增强的梁之间的能量吸收差异不大。然而,以最高的速度,CFRP梁比RC梁吸收更少的能量。结构冲击破坏模式及其力学特性的研究为结构的防撞设计和防护提供了有价值的参考。
    To explore and compare the failure modes, deformation behaviors, and load-bearing capacities of single-edge notched (SEN) beams strengthened with carbon fiber-reinforced polymer (CFRP) and steel bars, static and dynamic three-point bending tests on both types of concrete beams have been carried out in this study. During the static tests, the electro-hydraulic servo machine served as a loading device to apply pressure to CFRP beams and reinforced concrete (RC) beams. During the impact experiments, different impact velocities were imparted by adjusting the drop hammer\'s height. Thus, information regarding crack propagation, energy absorption, and deformation was obtained. The results from the static tests showed that the RC beams predominantly experienced shear failure. In contrast, the CFRP beams primarily exhibited bending-shear failure, attributed to the relatively weaker bond strength between the bars and the concrete. Impact tests were conducted at three different velocities in this study. As the impact velocity increased, both types of concrete beams transitioned from bending failure to bending-shear failure. At the lowest velocity, the difference in energy absorption between beams reinforced with different materials was insignificant during the bending process. However, at the highest velocity, CFRP beams absorbed less energy than RC beams. The study of structures\' impact failure modes and their mechanical characteristics offers valuable references for the anti-collision design and protection of structures.
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  • 文章类型: Journal Article
    本文的主要目的是评估在高速率载荷(冲击)下,由于纤维饱和点的水分含量(MC)变化而引起的Linden的机械性能。为了评估绿色木材的机械性能,主要是干燥木材的数据不适用,因为水分含量会极大地影响木材的机械性能。通过测试干燥和高水分含量的木材,我们可以理解水分含量对木材冲击行为的影响的一般观点。几个测试样品是由不同含水率为11%的菩提树木材制成的,60%和160%。落锤式冲击机测试了样品,以测量在非常短的冲击时间内锤子的反作用力。测试的结果是参数,例如力-时间图,裂纹萌生所需的最大力,冲击弯曲强度(IBS)和裂纹萌生所需的功。结果表明,MC的增加会降低最大力,裂纹萌生和IBS所需的工作。然而,当MC超过光纤饱和点(FSP)时,对力模式和最大所需力没有进一步影响。
    The article\'s main aim is to assess the mechanical behaviour of linden under high-rate loadings (impact) and its change due to changes in moisture content (MC) over fibre saturation point. For assessing the mechanical properties of green wood, mainly the data of the dried wood is not applicable since the moisture content can drastically affect the mechanical properties of the wood. By testing both dried and high-moisture-content wood, we can understand a general viewpoint toward the effect of the moisture content on the impact behaviour of the wood. Several test samples were made of linden wood with different moisture content levels of 11%, 60% and 160%. A drop-weight impact machine tested the specimens to measure the reaction force of the hammer during a very short impact period. The results of the tests were parameters such as force-time chart, the maximum force required for crack initiation, the impact bending strength (IBS) and the work needed for crack initiation. The results indicated an increase in MC decreases the maximum force, work required for crack initiation and IBS drastically. However, when MC exceeded the fibre saturation point (FSP), there was no further influence on the force pattern and maximum required force.
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  • 文章类型: Journal Article
    将椰子纤维(CF)掺入磷酸镁水泥(MPC)中可以有效地改善其高脆性和易开裂性。在实际工程中,椰子纤维增强磷酸镁水泥(CF-MPC)可能会在寒冷的环境中工作。因此,了解各种类型的低温固化对CF-MPC性能的影响至关重要,但是这方面的研究很少。在这项研究中,静态压缩和三点弯曲试验用于检查不同CF含量和不同负固化温度下CF-MPC的压缩和弯曲特性。通过扫描电子显微镜(SEM)和X射线衍射(XRD)观察了低温维持对样品结构和水化反应的影响。结果表明,CF-MPC低温固化在压缩和弯曲过程中更容易产生裂纹,适量的CF可以增强其塑性变形能力。CF-MPC的抗压强度和抗弯强度随固化温度的降低而下降。此外,随着CF含量的增加,样品的抗压强度也趋于下降,弯曲强度的变化有一个临界点。此外,MPC的主要水化产物(MgKPO4·6H2O)随固化温度的降低而降低,CF-MPC出现较多的孔洞和裂缝。
    The incorporation of coconut fiber (CF) into magnesium phosphate cement (MPC) can effectively improve upon its high brittleness and ease of cracking. In practical engineering, coconut fiber-reinforced magnesium phosphate cement (CF-MPC) will likely work in cold environments. Therefore, it is essential to understand the effects of various types of low-temperature curing on CF-MPC performances, but there are very few studies in this area. In this study, the static compression and three-point bending test were utilized to examine the compressive and flexural characteristics of CF-MPC with various CF contents and different negative curing temperatures. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were conducted to observe the impact of low-temperature maintenance on the structure and hydration reaction of the specimens. The results indicate that CF-MPC curing at low temperatures was more prone to cracks during compression and bending, while the appropriate amount of CF could enhance its plastic deformation capability. The CF-MPC\'s compressive and flexural strength declined as the curing temperature dropped. Moreover, with the rise in CF content, the samples\' compressive strength also tended to fall, and there was a critical point for the change in flexural strength. In addition, MPC\'s primary hydration product (MgKPO4·6H2O) decreased with a drop in curing temperature, and more holes and fractures appeared in CF-MPC.
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  • 文章类型: Journal Article
    采用粉末冶金轧制法,可以生产在泡沫芯和面板之间具有冶金结合的铝泡沫夹层(AFS)面板。在这项研究中,通过控制发泡温度和持续时间,AFS面板制造有不同的核心密度和厚度,所有保持面板厚度接近1毫米。通过三点弯曲试验,这项研究深入研究了核心密度如何影响这些AFS面板的力学行为。很明显,核心密度的增加积极影响面板的弯曲强度和破坏载荷,但反过来影响其总能量吸收效率。不同的核心密度带来了不同的破坏模式:低密度样品主要显示面板压痕和核心剪切破坏,而高密度的显示面板屈服和断裂。此外,该研究提供了对不同故障模式的初始故障载荷的预测,并介绍了全面设计的故障图,为AFS面板的生产奠定了基础理论。
    Using the powder-metallurgy rolling method, aluminum foam sandwich (AFS) panels with a metallurgical bond between the foam core and the panel can be produced. In this study, by manipulating the foaming temperature and duration, AFS panels were fabricated with varying core densities and thicknesses, all maintaining a panel thickness close to 1 mm. Through the three-point bending test, this research deeply delved into how core density influences the mechanical behaviors of these AFS panels. It became evident that a rise in core density positively affects the bending strength and failure load of the panels but inversely impacts their total energy absorption efficiency. Differing core densities brought about distinct failure patterns: low-density samples primarily showed panel indentation and core shear failures, whereas those of high density demonstrated panel yield and fractures. Furthermore, the research offers predictions on the initial failure loads for different failure modes and introduces a comprehensively designed failure diagram, laying a foundational theory for the production of AFS panels.
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  • 文章类型: Journal Article
    氧化锆和聚醚醚酮(PEEK)是两种被广泛研究的生物材料,可替代口腔修复中的金属。为了获得适当的生物力学行为,假体生物材料必须确保良好的抗载荷能力,因为这是一个关键的特性,使其在牙科应用中的使用。这项研究的目的是研究实验环境中不同生物材料的抗断裂性差异:固定局部义齿(FPDs)拧在仿生下颌骨的原型中。10个FPD样品分为2组(A和B):A组(n=5)涉及氧化锆陶瓷中的FPD,B组(n=5)涉及PEEK复合材料中的FPD。通过三点弯曲机械测试对样品进行加载,并且已经评估了断裂载荷,生成了逐点图形(速度/载荷和时间/变形)。通过微计算机断层扫描(micro-CT)进一步分析样品,并在实验负载条件下进行描述。氧化锆陶瓷FDP是报告最差结果的样品,显示相对于基于PEEK的样本的较低的垂直位移值。Micro-CT结果进一步证实了先前描述的初步结果。这项体外研究旨在提供有关PEEK作为用于修复治疗的可靠且坚固的生物材料的可靠性的分析数据。
    Zirconia and polyetheretherketone (PEEK) are two biomaterials widely investigated as substitute for metals in oral prosthetic rehabilitation. To achieve a proper biomechanical behavior, the prosthetic biomaterials must ensure a good resistance to loads, as this is a crucial characteristic enabling their use in dental applications. The aim of this study was to investigate differences in the fracture resistance of different biomaterials in an experimental environment: fixed partial dentures (FPDs) screwed in a prototype of biomimetic mandible. 10 Samples of FPDs were allocated in 2 groups (A and B): Group A (n=5) involved FPDs in zirconia-ceramic, and Group B (n=5) involved FPDs in PEEK-composite. The samples were loaded by means of a three-point bending mechanical test, and the load to fracture has been evaluated generating a point-by-point graphics (speed/load and time/deformation). The samples were further analyzed by micro-computed tomography (micro-CT) and described under experimental loading conditions. Zirconia-ceramic FDPs were the samples reporting the worst results, showing a lower value of vertical displacement with respect to PEEK-based samples. The micro-CT results have further confirmed the preliminary results previously described. This in vitro study aims to give analytic data on the reliability of PEEK as a reliable and strong biomaterial for prosthetic treatments.
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  • 文章类型: Journal Article
    在这里,评价掺入表面预反应的玻璃离聚物(S-PRG)填料的自聚合树脂的机械性能。为此,将粒径为1μm(S-PRG-1)和3μm(S-PRG-3)的S-PRG填料以10、20、30和40wt%混合,以制备实验树脂粉末。将粉末和液体(粉末/液体比=1.0g/0.5mL)捏合并填充到有机硅模具中以获得矩形样品。通过三点弯曲试验记录挠曲强度和模量(n=12)。S-PRG-1在10wt%(62.14MPa)和S-PRG-3在10和20wt%(68.68和62.70MPa,分别)是足够的(>60兆帕)。含S-PRG-3的试样的弯曲模量明显高于含S-PRG-1的试样。弯曲后样品断裂表面的扫描电子显微镜观察表明,S-PRG填料紧密嵌入并分散在树脂基体中。维氏硬度随着填料含量和尺寸的增加而增加。S-PRG-3的维氏硬度(14.86-15.48HV)高于S-PRG-1的维氏硬度(13.48-14.97HV)。因此,S-PRG填料的粒径和含量影响实验自聚合树脂的机械性能。
    Herein, the mechanical properties of an auto-polymerizing resin incorporated with a surface pre-reacted glass ionomer (S-PRG) filler were evaluated. For this, S-PRG fillers with particle sizes of 1 μm (S-PRG-1) and 3 μm (S-PRG-3) were mixed at 10, 20, 30, and 40 wt% to prepare experimental resin powders. The powders and a liquid (powder/liquid ratio = 1.0 g/0.5 mL) were kneaded and filled into a silicone mold to obtain rectangular specimens. The flexural strength and modulus (n = 12) were recorded via a three-point bending test. The flexural strengths of S-PRG-1 at 10 wt% (62.14 MPa) and S-PRG-3 at 10 and 20 wt% (68.68 and 62.70 MPa, respectively) were adequate (>60 MPa). The flexural modulus of the S-PRG-3-containing specimen was significantly higher than that of the S-PRG-1-containing specimen. Scanning electron microscopy observations of the specimen fracture surfaces after bending revealed that the S-PRG fillers were tightly embedded and scattered in the resin matrix. The Vickers hardness increased with an increasing filler content and size. The Vickers hardness of S-PRG-3 (14.86-15.48 HV) was higher than that of S-PRG-1 (13.48-14.97 HV). Thus, the particle size and content of the S-PRG filler affect the mechanical properties of the experimental auto-polymerizing resin.
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