Thermal sterilization

热灭菌
  • 文章类型: Journal Article
    本研究探讨了Curdlan整合和热灭菌对流变特性的影响,结构,浓缩大米淀粉凝胶的质量属性。作为热定形多糖,Curdlan与大米淀粉凝胶建立了双网络凝胶结构,表现出与大米淀粉的强相互作用,通过共聚焦激光扫描显微镜和傅里叶变换红外光谱仪证实。凝乳多糖的添加加速了大米淀粉的凝胶形成,产生更致密的凝胶结构。因此,这个增强的G\',类似固体的行为,纹理属性,和烹饪质量,同时减少频率依赖性。考虑到纯大米淀粉的冷却诱导凝胶化行为,热处理破坏了链间氢键,损害凝胶的结构完整性。这种破坏表现为质地较软,机械性能和烹饪质量下降。值得注意的是,这种下降的力学性能和蒸煮品质的大米淀粉凝胶的掺入可可显着改善,特别是含量≥1.0%。与纯RS相比,包含1.0%的CD显示蒸煮破损率降低了30.69%,硬度提高了38.04%。这项工作为新鲜淀粉凝胶食品的发展提供了有价值的见解,这些食品表现出卓越的质量和延长的保质期。
    This study delves into the effects of curdlan integration and thermal sterilization on the rheological properties, structure, and quality attributes of concentrated rice starch gel. Acting as a heat-set polysaccharide, curdlan established a dual-network gel structure with rice starch gel, displaying strong interactions with rice starch, as confirmed by confocal laser scanning microscopy and Fourier-transform infrared spectroscopy. The addition of curdlan expedited the gel formation of rice starch, yielding a denser gel structure. Consequently, this enhanced G\', solid-like behavior, textural properties, and cooking quality while reducing frequency-dependence. Given the cooling-induced gelation behavior of pure rice starch, thermal treatment disrupted inter-chain hydrogen bonding, compromising the structural integrity of the gel. This disruption manifested in a softer texture and diminished mechanical properties and cooking quality. Notably, this decline in mechanical properties and cooking quality of rice starch gel was markedly ameliorated with the incorporation of curdlan, particularly at a content of ≥1.0 %. Compared with pure RS, 1.0 % CD inclusion showed a reduction in cooking breakage rate by 30.69 % and an increase in hardness by 38.04 %. This work provides valuable insights for the advancement of fresh starch gel-based foods that exhibit exceptional quality and an extended shelf life.
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  • 文章类型: Journal Article
    高温灭菌后肉制品的质地劣化是肉类工业中的紧迫问题。这项研究评估了不同热灭菌温度对即食(RTE)鸡胸肉的质地和多汁性的影响。在这项研究中,通过动态监测鸡肉产品在热灭菌过程中的质地和多汁性,已经观察到,过高的灭菌温度(高于100°C)显着降低剪切力,产品的弹性和保水能力。此外,从肌原纤维蛋白降解的角度来看,分子机制已经阐明,揭示了在121°C/10分钟的热灭菌处理触发肌球蛋白重链和F-肌动蛋白的降解,破坏肌丝的晶格排列,损害肉瘤的完整性,并导致肌原纤维碎裂指数增加约40.66%,从而降低产品的质量特性。本研究揭示了鸡肉产品在热灭菌过程中质量动态变化的潜在机制,从而为开发优质鸡肉产品提供理论指导。
    Texture deterioration of meat products upon high-temperature sterilization is a pressing issue in the meat industry. This study evaluated the effect of different thermal sterilization temperatures on the textural and juiciness of ready-to-eat (RTE) chicken breast. In this study, by dynamically monitoring the texture and juiciness of chicken meat products during the process of thermal sterilization, it has been observed that excessively high sterilization temperatures (above 100°C) significantly diminish the shear force, springiness and water-holding capacity of the products. Furthermore, from the perspective of myofibrillar protein degradation, molecular mechanisms have been elucidated, unveiling that the thermal sterilization treatment at 121°C/10 min triggers the degradation of myosin heavy chains and F-actin, disrupting the lattice arrangement of myofilaments, compromising the integrity of sarcomeres, and resulting in an increase of approximately 40.66% in the myofibrillar fragmentation index, thus diminishing the quality characteristics of the products. This study unravels the underlying mechanisms governing the dynamic changes in quality of chicken meat products during the process of thermal sterilization, thereby providing theoretical guidance for the development of high-quality chicken products.
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  • 文章类型: Journal Article
    研究了不同热灭菌条件对即食对虾品质和消化率的影响。与高温(121°C)和短时间(6分钟和8分钟)灭菌相比,低温(110和115°C)和长时间(>20分钟)灭菌显着促进了美拉德和褐变反应,并改变了RTE虾的颜色。高杀菌温度促进虾仁蛋白氧化,导致羰基增加,二硫键,和自由基含量,而游离巯基含量下降。高温下的氧化和组织破坏导致虾肌肉内的质构特性降低和水分分布改变。然而,在体外模拟消化实验中,灭菌虾表现出优异的消化特性。与低温长时间灭菌相比,高温短时间灭菌更有效地缓解了RTE虾的品质恶化。
    The effects of different thermal sterilization conditions on the quality and digestibility of ready-to-eat (RTE) shrimp were investigated. Compared with the high-temperature (121 °C) and short-time (6 min and 8 min) sterilization, the low-temperature (110 and 115 °C) and long-time (>20 min) sterilization significantly promoted the Maillard and browning reactions and changed the color of the RTE-shrimp. The high sterilization temperature promoted shrimp protein oxidation, resulting in increased carbonyl group, disulfide bond, and free radical content, while the free sulfhydryl group content decreased. This oxidation and tissue destruction at high temperature led to reduced texture properties and altered water distribution within the shrimp\'s muscles. However, sterilized shrimp exhibited superior digestive properties in an in vitro simulated digestion experiment. High-temperature and short-time sterilization is more effective in mitigating the quality deterioration of RTE-shrimp compared to low-temperature and long-time sterilization.
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  • 文章类型: Journal Article
    非挥发物为桃泥(PP)中香气活性成分的形成提供了一些见解,但是仍然需要更深入的调查。热浓缩(PPC)和灭菌(PPCS)过程中PP中关键香气和异味成分的形成途径尚不清楚。因此,采用GC-O-MS结合UPLC-MS/MS对挥发性和非挥发性成分及其形成途径进行鉴定。在36种芳香活性化合物中,γ-十内酯的含量,乙酸己酯,叶醋酸盐,己醛,1-己醇(气味活度值≥1)下降46%,100%,100%,92%,PP和PP+C+S之间的100%,导致“绿色”和“果味”属性的弱化。异味成分,包括1-octen-3-one,异丁酸,异噻唑,和异戊酸在热处理过程中被鉴定。1-Octen-3-one含量通过亚麻酸代谢从PP到PPCS增加了75%,这有助于“煮熟”;异丁酸和异戊酸的形成,异噻唑,通过丝氨酸和亮氨酸代谢导致“酸/腐臭”的增强。
    Non-volatiles offer some insight into the formation of aroma-active components in peach puree (PP), but more depth investigation is still needed. Formation pathways of key aroma-active and off-flavor components in PP during thermal concentration (PP + C) and sterilization (PP + C + S) are unclear. Therefore, GC-O-MS combined with UPLC-MS/MS was used to identify the volatile and nonvolatile components and their formation pathways. Among the 36 aroma-active compounds, the contents of γ-decalactone, hexyl acetate, leaf acetate, hexanal, and 1-hexanol (odor activity value ≥ 1) decreased by 46 %, 100 %, 100 %, 92 %, and 100 % between PP and PP + C + S, causing the weakening of \"green\" and \"fruity\" attributes. Off-flavor components including 1-octen-3-one, isobutyric acid, isothiazole, and isovaleric acid were identified during thermal processing. 1-Octen-3-one content increased by 75 % from PP to PP + C + S through linolenic acid metabolism, which contributed to \"cooked\"; the formation of isobutyric and isovaleric acids, isothiazole, resulted in the enhancement of \"sour/rancid\" via serine and leucine metabolism.
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  • 文章类型: Journal Article
    Yan73(葡萄)是中国栽培的染色葡萄品种。目前,大多数研究集中在花色苷的作用机理或花色苷作为辅助颜色品种对葡萄酒颜色的影响。关于其直接使用或直接加工果汁等产品的研究很少。为了研究不同加工方法对燕73葡萄果汁的影响,物理化学和功能特性,以及果汁的感官指标,通过使用热巴氏灭菌(TP)进行分析,热声处理(TS),TS与乳酸链球菌素(TSN)结合,TS与ε-聚赖氨酸(TSε)结合,辐照(IR),和高静水压力(HHP)。物理化学指标,功能属性,对Smoke73葡萄汁的感官指标进行了测定和分析。研究结果表明,在7种灭菌方法中,除HHP外,所有处理中果汁中的总多酚含量(TPC)均显着增加。TP中TPC最高(3773.33mgGAE/L)。除IR5外,总花色苷含量(TAC)均增加,TSN(1202.67mg/L)的TAC最高。在颜色方面,TP(a*=36.57,b*=19.70,L*=14.81,C*=41.55,h°=28.30,ΔE=5.9)由于高温而促进了花色苷的溶解,这基本上改善了葡萄汁的所有颜色指标,使葡萄汁的颜色更加生动。HHP治疗后,颜色(ΔE=1.72)和香气指标更接近葡萄汁本身。熵权-TOPSIS,批评-局部,和PCA综合质量评价模型表明,所有选择TP为最佳综合质量。
    Yan 73 (Vitis vinifera) is a dyed grape variety cultivated in China. Currently, most studies have focused on the mechanism of anthocyanins or the impact of anthocyanins as auxiliary color varieties on wine color. There is little research on its direct use or direct processing of products such as juice. In order to investigate the effects of different processing methods on the juice of Yan 73 grapes, the physicochemical and functional properties, as well as the sensory indexes of the juice, were analyzed by using thermal pasteurization (TP), thermosonication (TS), TS combined with nisin (TSN), TS combined with ε-Polylysine (TSε), irradiation (IR), and high hydrostatic pressure (HHP). The physicochemical indexes, functional properties, and sensory indexes of Smoke 73 grape juice were determined and analyzed. The results of the study showed that among the seven sterilization methods, total polyphenol content (TPC) in juice was significantly increased in all treatments except HHP. TPC was the highest in TP (3773.33 mg GAE/L). Total anthocyanin content (TAC) was increased except IR5, and TSN (1202.67 mg/L) had the highest TAC. In terms of color, TP (a* = 36.57, b* = 19.70, L* = 14.81, C* = 41.55, h° = 28.30, ΔE = 5.9) promotes the dissolution of anthocyanins because of high temperatures, which basically improves all the color indicators of grape juice and makes the color of grape juice more vivid. After HHP treatment, the color (ΔE = 1.72) and aroma indicators are closer to the grape juice itself. The Entropy weight-TOPSIS, CRITIC-Topsis, and PCA integrated quality evaluation models showed that all selected TP as the best integrated quality.
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  • 文章类型: Journal Article
    灭菌对于即食食品至关重要;然而,它往往会降低产品的质量。探讨抗氧化剂对烤太平洋虾灭菌后食用品质的调节作用,颜色变化,氧化程度,茶多酚处理的烤虾的微观结构和品质,植酸,迷迭香提取物,并对d-异丙磺酸钠进行了研究。茶多酚处理的烤虾灭菌后美拉德中间产物和褐变强度最低;植酸显着降低羰基含量和TBARS值;迷迭香提取物表现出最低的自由基水平。而d-异丙磺酸钠保留了相对完整的肌原纤维结构。相关分析显示,灭菌后烤虾的氧化程度与食用品质呈负相关。因此,抗氧化剂的添加抑制了氧化,提高了烤虾的品质,不同的抗氧化剂对热灭菌后烤虾品质的改善有不同的影响。
    Sterilization is essential for ready-to-eat foods; however, it tends to degrade the quality of the product. To explore the role of antioxidants in regulating the edible quality of roasted Pacific white shrimp after sterilization, color changes, degree of oxidation, microstructure and quality of roasted shrimp treated with tea polyphenols, phytic acid, rosemary extract, and d-sodium erythorbate were investigated. Tea polyphenol-treated roasted shrimp had the lowest Maillard intermediate products and browning strength after sterilization; phytic acid significantly reduced carbonyl content and TBARS value; rosemary extract exhibited the lowest level of free radicals, while d-sodium erythorbate preserved a relatively intact myofibrillar structure. Correlation analysis revealed a negative correlation between the degree of oxidation and the edible quality of roasted shrimp after sterilization. Therefore, the addition of antioxidants inhibited oxidation and improved the quality of roasted shrimp, and different antioxidants had diverse effects on the quality improvement of roasted shrimp after thermal sterilization.
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  • 文章类型: Journal Article
    在栗子罐等果泥罐的生产过程中,由于过度加热,很容易褐变,每年都会造成大量的浪费。通过有限元方法建立了板栗泥的传热传质模型。该模型模拟了温度场的变化过程,板栗泥生产过程中的热流速度场和F值。通过热渗透试验对比确认模型的有效性后,该模型用于调整和优化生产工艺。对于#9121罐,采用两阶段灭菌法。通过10-65-48-14/118-110°C的灭菌方法,在10-86-24/121°C下实现了与原始过程相当的灭菌效果,产品的褐变问题得到缓解,产品质量有所提高。这一实践也可为罐装企业今后调整生产工艺提供参考。
    In the production process of puree cans such as chestnuts cans, it is easy to browning due to excessive heating, which causes a lot of waste every year. The heat and mass transfer model of Chinese Chestnut Puree was established through the finite element method. The model simulated the change process of the temperature field, heat flow velocity field and F value during the production of Chinese Chestnut Puree. After comparing and confirming the effectiveness of the model through the thermal penetration test, the model was used to adjust and optimize the production process. For #9121 cans, the two-stage sterilization method was adopted. Through the sterilization method at 10-65-48-14/118-110°C, a sterilization effect equivalent to that of the original process at 10-86-24/121°C was achieved, the browning problem of the product was alleviated, and the product quality was improved. This practice can also provide a reference for canning enterprises to adjust their production processes in the future.
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  • 文章类型: Journal Article
    热巴氏灭菌(TP)的影响,高温长时间(HTLT),超高温瞬时(UHT),高静水压力(HHP)和热声处理(TS)灭菌的物理化学,研究了黑胡萝卜汁的感官和功能特性。第一次,通过数学建模对灭菌BCJ的综合质量进行量化。UHT是BCJ最不合适的灭菌方法,原因是功能特性最严重。TS对感官和理化性质有不良影响,显着提高了总黄酮和花色苷的含量(p<0.05),表现出最强的抗氧化活性,使其成为营养高价值的加工方法。TP和HHP平衡了感官性能的改善和功能性能的保留,这是最适合BCJ的灭菌方法。本研究确定了BCJ的最佳灭菌方法,为筛选高质量的加工方法提供了科学的解决方案。
    The effect of thermal pasteurization (TP), high temperature long time (HTLT), ultra-high temperature instantaneous (UHT), high hydrostatic pressure (HHP) and thermosonication (TS) sterilization on the physicochemical, sensory and functional properties of black carrot juice (BCJ) were studied. And for the first time, the comprehensive quality of sterilized BCJ was quantified by mathematical modeling. UHT was the least suitable sterilization method for BCJ resulting from the most severe deterioration in functional properties. TS had adverse effects on sensory and physicochemical properties, but significantly increased the total flavonoids and anthocyanins contents (p < 0.05) and showed the strongest antioxidant activity, making it a nutritional high-value processing method. TP and HHP balanced the improvement of sensory properties and the retention of functional properties, which were the most suitable sterilization methods for BCJ. This study determined the optimal sterilization methods of BCJ, and provided a scientific solution for the screening of high quality processing methods.
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  • 文章类型: Journal Article
    在热灭菌的发酵豆奶中,变质的气味是一个问题。本研究旨在阐明腐败气味的生产条件和关键气味。感官评估表明,热灭菌导致酸奶和水果气味的感官强度降低,同时显着增加不良香气,包括豆制品,酸性,煮熟的豆子和变质的气味。变质的气味随着酸度和加热温度的增加而增加。在可滴定酸度为5.4g/kg的发酵豆浆中观察到最强烈的变质气味,90℃灭菌除了豆浆中固有的常见挥发物和乳酸发酵产生的挥发物,2-甲基四氢噻吩-3-酮首次在大豆食品中发现,并被发现会引起变质的气味。在热灭菌发酵豆浆中发现的44种挥发物共同形成了其风味轮。本研究为解决腐臭制约植物性发酵豆乳推广的问题提供了重要的理论支持。
    Spoiled odors are a problem in thermally sterilized fermented soymilk. This study aims to clarify production conditions and key odorants of spoiled odors. The sensory evaluation showed that thermal sterilization caused a decrease in the sensory intensity of yogurt and fruity odors while significantly increasing undesirable aromas including beany, acidic, cooked-beans and spoiled odors. The spoiled odors increased with increasing acidity and heating temperatures. The strongest spoiled odor was observed in fermented soymilk at titratable acidity of 5.4 g/kg, sterilized at 90 °C. Apart from common volatiles that were inherent in soymilk and generated from lactic fermentation, 2-methyltetrahydrothiophen-3-one was found for the first time in soybean foods and was found to cause the spoiled odor. 44 volatiles found in thermally sterilized fermented soymilk were jointly formed its flavor wheel. This study provides important theoretical support for solving the problem of spoiled odor restricting the popularization of plant-based fermented soymilk.
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  • 文章类型: Review
    水果和蔬菜汁(FVJ)含有丰富的营养,所以它们很容易繁殖细菌,导致微生物污染和质量安全的迅速恶化。灭菌是FVJ加工中的重要操作。然而,无论使用热灭菌还是非热灭菌,对FVJ整体质量的影响及其影响强烈依赖于加工参数,微生物物种,和FVJ矩阵。因此,对于不同类型的FVJ,了解不同灭菌技术对果汁整体质量的影响对于设计和优化技术参数以生产增值产品非常重要。本文概述了过去10年中热和非热技术在FVJ加工领域的应用。各种技术对微生物和酶的灭活的操作原理和效果,营养和功能特性,物理化学性质,全面讨论了各种FVJ的感官质量。还详细讨论了不同组合的跨栏技术在FVJ灭菌加工领域的应用。此外,的优势,局限性,并总结了目前不同灭菌技术的应用前景。
    Fruit and vegetable juices (FVJ) are rich in nutrients, so they easily breed bacteria, which cause microbial pollution and rapid deterioration of their quality and safety. Sterilization is an important operation in FVJ processing. However, regardless of whether thermal sterilization or non-thermal sterilization is used, the effect and its impact on the overall quality of FVJ are strongly dependent on the processing parameters, microbial species, and FVJ matrix. Therefore, for different types of FVJ, an understanding of the impacts that different sterilization technologies have on the overall quality of the juice is important in designing and optimizing technical parameters to produce value-added products. This article provides an overview of the application of thermal and non-thermal technique in the field of FVJ processing over the past 10 years. The operating principle and effects of various technologies on the inactivation of microorganisms and enzymes, nutritional and functional characteristics, physicochemical properties, and sensory quality of a wide range of FVJ are comprehensively discussed. The application of different combinations of hurdle technology in the field of FVJ sterilization processing are also discussed in detail. Additionally, the advantages, limitations, and current application prospects of different sterilization technologies are summarized.
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