关键词: SCXRD crystalline sponges metal–organic frameworks single-crystal X-ray diffraction statistical design of experiments

来  源:   DOI:10.1107/S2052252524004871   PDF(Pubmed)

Abstract:
Investigation of the analyte soaking conditions on the crystalline sponge {[(ZnI2)3(tpt)2·x(solvent)]n} method using a statistical design of experiments model has provided fundamental insights into the influence of experimental variables. This approach focuses on a single analyte tested via 60 experiments (20 unique conditions) to identify the main effects for success and overall guest structure quality. This is employed as a basis for the development of a novel molecular structure grading system that enables the quantification of guest exchange quality.
摘要:
使用实验模型的统计设计对晶体海绵{[(ZnI2)3(tpt)2·x(溶剂)]n}方法的分析物浸泡条件的研究提供了对实验变量影响的基本见解。这种方法侧重于通过60个实验(20个独特条件)测试的单个分析物,以确定成功和整体客体结构质量的主要影响。这被用作开发新型分子结构分级系统的基础,该系统可以量化客体交换质量。
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