{Reference Type}: Journal Article
{Title}: Statistical optimization of guest uptake in crystalline sponges: grading structural outcomes.
{Author}: Carroll RC;Coles SJ;
{Journal}: IUCrJ
{Volume}: 11
{Issue}: 0
{Year}: 2024 Jul 1
{Factor}: 5.588
{DOI}: 10.1107/S2052252524004871
{Abstract}: Investigation of the analyte soaking conditions on the crystalline sponge {[(ZnI2)3(tpt)2·x(solvent)]n} method using a statistical design of experiments model has provided fundamental insights into the influence of experimental variables. This approach focuses on a single analyte tested via 60 experiments (20 unique conditions) to identify the main effects for success and overall guest structure quality. This is employed as a basis for the development of a novel molecular structure grading system that enables the quantification of guest exchange quality.