{Reference Type}: Journal Article
{Title}: Static Solid Relaxation Ordered Spectroscopy: SS-ROSY.
{Author}: Boutis GS;Kausik R;
{Journal}: Int J Mol Sci
{Volume}: 20
{Issue}: 23
{Year}: Nov 2019 24
{Factor}: 6.208
{DOI}: 10.3390/ijms20235888
{Abstract}: A two-dimensional pulse sequence is introduced for correlating nuclear magnetic resonance anisotropic chemical shifts to a relaxation time (e.g., T1) in solids under static conditions. The sequence begins with a preparatory stage for measuring relaxation times, and is followed by a multiple pulse sequence for homonuclear dipolar decoupling. Data analysis involves the use of Fourier transform, followed by a one-dimensional inverse Laplace transform for each frequency index. Experimental results acquired on solid samples demonstrate the general approach, and additional variations involving heteronuclear decoupling and magic angle spinning are discussed.