Review of sample preparation methods for chromatographic analysis of neonicotinoids in agricultural and environmental matrices: From classical to state-of-the-art methods.

• 影响指数: 4.601
• 发表时间: Apr 2021 26
• 来源期刊: J Chromatogr A
• DOI: 10.1016/j.chroma.2021.462042
• PMID: 33761434
• 文章类型: Journal Article
• 作者列表: Watanabe E

关键词: Clean-up; Extraction; Liquid chromatography; Neonicotinoid; Review; Sample matrix

Mesh: Agriculture; Analytic Sample Preparation Methods; Animals; Chromatography / methods; Environmental Pollutants / analysis chemistry; Neonicotinoids / analysis chemistry; Pesticide Residues / analysis

Abstract

This review specifically examines the development of sample preparation methods for residue analyses of neonicotinoid insecticides in agricultural and environmental matrices. Pesticide residue analysis is fundamentally important to ensure the safety of foods and processed foods of plant and animal origin, and to preserve the environment, particularly soil and water. For the development of pesticide residue analysis, the sample preparation process is an important key to maximizing the analytical performance of highly sensitive and accurate chromatographic instruments and to acquiring reliable analytical results. This review outlines sample preparation methods that have been proposed to date for extraction of neonicotinoids that might remain in a complicated sample matrix in quantitatively trace amounts, and for cleaning up, to the greatest extent possible, the interfering components that coexist in the sample extract.